Microstructure and Microhardness of Friction Stir Processed AZ31b-H24 Magnesium Alloy

The effect of welding speed on the microstructure of friction stir processed (FSPed) AZ31B-H24 magnesium alloy was studied using light microscopy, image analysis, and microhardness tests. The grain size of the magnesium alloy was observed to increase after FSP from about 3.5 µm in the base alloy to about 8 µm in the stir zone. The aspect ratio decreased from 1.60 to 1.55 towards the center of the stir zone. The changes in the grain size and shape caused the microhardness of the samples to drop significantly across the FSPed region from 75 HV in the base alloy to below 55 HV in the stir zone. Decreasing the welding speed increased the grain size due to a greater input of heat energy. The faster heating rate due to the lower welding speed caused a deeper penetration of the annealing effects of FSP. It was also observed that the annealing effects caused by FSP were less pronounced with increasing distance from the interface between the sample and pin tool shoulder. The Hall-Petch type relationship of the micro-indentation hardness as a function of the grain size was observed to hold true after FSP.