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By D. E. Kirby

The electrochemical reduction of AlC13 was investigated as a process for the production of aluminum. An externally heated, single-compartment cell with a rammed refractory lining was used with molten KCl-NaCl-AlC13 electrolyte. Aluminum was deposited qt 700° to 760° C with a current of 100 to 200 amperes on a molten aluminum cathode. Chlorine was evolved at a graphite anode and collected and measured to provide a quantitative evaluation of the AlC13 reduction. Aluminum was removed from the cell by siphoning or ladling. Granular AlC13 was added periodically to replenish that depleted from the electrolyte. Concentrations of 7.5 to 17.5 percent AlC13 in the electrolyte were optimum for operation. Anode current efficiencies of 83 to 85 percent were attained, using anode current densities of 5.9 amperes per square inch and an anode-cathode distance of 4 inches. The chemically bonded, alumina liner was resistant to attack by aluminum and chlorine but susceptible to erosion at the surface of the electrolyte. Titanium diboride proved suitable for the electrical connection to the molten aluminum cathode. Aluminum of a purity equal to or better than 1100 series metal was electrowon continuously from commercial AlC13 for a period of 4-1/2 months.

Jan 1, 1970

By Mariana Sizenando Lyrio, Fernanda Nascimento Moreira, Weslley Luiz da Silva Assis, Harison da Silva Ventura, Gabriella Maria Silveira de Sá, Ana Gabriella Conceição dos Santos

surgimento de fases intermetálicas em aços é matéria de grande interesse devido ao caráter nocivo que elas podem conferir às propriedades mecânicas do material. No presente trabalho, foi estudado o efeito do surgimento da fase sigma em um aço inoxidável duplex através de modelamento numérico-computacional. A microestrutura duplex foi obtida via simulação, sendo, então utilizada como matriz para a nucleação e crescimento da fase sigma, também via simulação. O método do Cone Causal foi utilizado para o desenvolvimento da microestrutura e os resultados foram comparados com a metodologia da cinética formal de JMAK para fins de validação do modelo. Os resultados da simulação permitem obter, através da Regra das Misturas, predições sobre as propriedades mecânicas do material, no caso, o limite de resistência à tração, que foi comparado com os dados encontrados na literatura. Foi possível constatar o aumento do limite de resistência à tração para maiores frações volumétricas de sigma, o que traz como resultado a diminuição da ductilidade para o aço.

Nov 17, 2019

"The first SkimAir flash flotation cell was installed in Outokumpu’s Hammaslahti Copper Concentrator in 1982 to prevent overgrinding of soft sulphides in the milling circuit. Since this first installation the popularity of the flash flotation has fluctuated depending on metal market conditions and regional preferences. Units have been installed in many commodities including copper, lead, gold, PGMs, silver and nickel. Though it has been successfully employed in many operations around the world, flash flotation technology is still not well understood by many in the mining industry. This paper will discuss aspects of flash flotation flowsheet development along with some of the metallurgical and engineering considerations required to successfully incorporate flash flotation into new or existing milling circuits. This paper will also try and debunk some of the myths that exist around flash flotation cells and their operation. Case studies of flash flotation implementation will be discussed.IntroductionModern flash flotation technology was developed several decades ago by Outokumpu, with the first commercial installation of this technology being at the Hammaslahti concentrator in Finland in 1982 (Kallioinen & Niitti, 1985). This was a relatively modestly sized SK80 cell producing final grade copper concentrate directly from the flash flotation cell operating in the grinding circuit. Since that time the size and number of flash flotation cells installed globally has grown considerably to the point where today, it is a widely known application of flotation technology for amenable ores. Owing to their long history in developing the technology, Outotec are the market leader with their SkimAir range of flash flotation cells. Though there is a general awareness of flash flotation process in the mineral processing industry, there is a lack of detailed understanding of the process and the benefits it can provide to new and existing operations."

Jan 1, 2017

A shortage of technical skills in all areas of the mining industry is being experienced worldwide. This has significant consequences for design, operations, productivity and safety and, therefore, needs to be seriously addressed, both in the short and longer term. It is therefore both a strategic and a tactical issue. Importantly, however, since mining is a long-term business, the shortage of skills must be dealt with from a strategic point of view to ensure the supply of the necessary skills for future mining. This paper will deal specifically with the provision of high level technical skills, that is, university graduates in mining engineering, and the outlook for the institutions that are currently producing such graduates.

Jan 1, 2009

By Claude MacDonald, John H. Ashburn

"IntroductionIndustrial growth and technological change over recent years had been accompanied by two major sources of concern to management and employees: (a) increase in occupational injury and illness and the resultant costs involved; and (b) equipment damage and breakdowns in concentrated production lines causing more extensive loss potential.Due to economic factors, management attention has focussed more on production and quality than on safety, health and related loss potential sources. As a result , occupational safety and health activism has grown, government legislation of compensation and occupational safety and health standards have progressively developed and stronger liability attitudes have been taken by courts of law.To improve efficiency and allow development in more competitive markets, rising labour costs, equipment costs and safety related financial losses have dictated that attention be given to conservation of all resources. Conservation of resources, people, equipment, material and environment, can no longer be addressed in isolation but must be managed integrally with production and quality. To this end, systems have developed utilizing sound management principles applied with equal intensity to production, quality and loss potential"

Jan 1, 1987

By Marcos Natan da Silva Lima

O aço com alto manganês tem sido estudado como alternativa mais barata em substituição às ligas de aço mais utilizadas, devido as suas propriedades de resistência, ductilidade e tenacidade. Foi alterada a composição de manganês para teores acima dos teores dos aços Hadfield, visando sua aplicação em temperaturas criogênicas. Foram obtidas ligas de aço com alto teor de Manganês através do processo de fundição. O objetivo é avaliar as alterações provocadas pelo aumento do Manganês no aço fundido. Através do estudo realizado no Thermo-Calc®, as amostras da liga fundida foram submetidas à laminação a quente e posterior tratamento térmico de solubilização a 700 ºC, com o intuito de manter a microestrutura austenítica. As mesmas foram analisadas quanto à microestrutura por microscopia ótica (MO) e microscopia eletrônica de varredura (MEV). Os ensaios de dureza realizados confirmaram a elevada dureza das ligas, bem como a variação entre as ligas no estado fundido e solubilizado.

Oct 30, 2017

By Anderson Rosa Pereira

A constante busca pela excelência na qualidade do material produzido tem gerado demanda para métodos precisos e de determinação on-line das características do material. Os métodos hoje utilizados para coleta de dados de rugosidade superficial geram amostras randômicas ou concentradas no início ou fim da bobina, o que não necessariamente mostra com precisão a rugosidade de todo o material produzido, e impossibilitam uma intervenção mais direta, precisa e automática nos parâmetros de laminação, objetivando um melhor aproveitamento dos cilindros, redução de custos e controle sobre este importante parâmetro de qualidade. Esta publicação descreve o funcionamento e a aplicação do sistema de medição de rugosidade on-line EMGSORM 3plus no controle automático de rugosidade desenvolvido para um skin pass mill. Assim, a linha principal deste artigo mostra através de um exemplo prático a aplicação de um sistema de medição de rugosidade on-line e seus benefícios.

Aug 16, 2017

By Diego Canez Fernandes, Henriquison Bottrel Reis, Mauricio Covcevich Bagatini

As técnicas que visam aumentar a densidade de carga possibilitam elevar a produtividade da coqueria e, além disso, permitem utilizar carvões com menor poder coqueificante. O aumento de densidade pode contribuir ainda para a obtenção de um coque de melhor qualidade, o que contribui para a redução do coke rate no alto-forno. Uma alternativa para aumentar a densidade de carga é a adição de óleo na mistura de carvões, o que reduz a tensão superficial da água, permitindo uma maior aproximação entre as partículas e favorecendo o contato efetivo durante a fase plástica. Neste contexto, o presente trabalho teve como objetivo avaliar o efeito da adição de óleo na densidade de carga para diferentes condições de granulometria e umidade do carvão empregado. Para isso foram realizados ensaios para medir a densidade de carga em três níveis de umidade (8%, 10% e 12%) e granulometria (82%, 85% e 88% < 2,83 mm). Posteriormente, foram realizados ensaios de coqueificação em escala piloto, e o coque produzido foi avaliado quanto ao DI15/150 (drum index), CRI (coke reactivity index) e CSR (coke strenght reaction). Os resultados mostraram que a adição gradativa de óleo promoveu aumento na densidade de carga enquanto a elevação da umidade do carvão e seu afinamento provocou a redução desse parâmetro. A qualidade metalúrgica do coque aumentou com a elevação da densidade de carga demostrando que essa é uma técnica com potencial de uso em plantas industriais.

Oct 1, 2019

By R. Biss

"Niobium or columbium, as usually called in North America is becoming a more and more important metal in the industrial world because of its attractive properties.Eventhough discovered in the early nineteenth century, it was not until the 1930's that its use became more widespread. The discovery of large commercial deposits in the late 1950's and the demand of industry for steel with high strength and toughness further promoted its use. To assure its adequate supply new or-e processinr technologies had to be developed. So, beside the traditional gravity concentration, the flotation process was employed for the partial upgrading of pyrochlore concentrate at S8ve (Norway) plant in 1953. The flotation process was equally used at St-Lawrence Columbium plant in the province of Quebec, Canada. The new plants at Araxa and Catalao in Brazil and at St-Honore, Canada, which supply almost of all niobium used today in the non-Communist world, also adopted the flotation process. The processes using long chain aliphatic rnonoarnines, diamines or sulfonates as collectors proved to be difficult especially on weathered types of ores or on those having a substantial content of silicate gangue minerals. They almost completely failed in case of alkaline intrusive rocks as syenites, nepheline syenite, ijolites and pyroxenites, composed almost entirely of silicate minerals. A lot of effort was devoted all around the world on research of new, more efficient flotation processes. So in 1982, Les Services T.M.G. Inc. (Niobec), sole producer of pyrochlore concentrate in North America, developed the direct pyrochlore flotation process from carbonatites. In 1983, at about the same time, the Quebec Department of Natural Resources Laboratories and Les Services T.M.G. Inc. announced a successful recovery of niobium Minera1s from a low grade nenheline syenite ore."

Jan 1, 1984

By M. J. Ferrante

The Bureau of Mines investigated the applicability of the freeze-drying technique for preparing dispersion-strengthened tungsten powders suitable for conversion by powder metallurgy into materials which might have improved high-temperature strength. Extruded rods from compacts of tungsten-5 vol pct thoria had at 1,650° C a tensile strength of 30,300 psi and a 10-hour stress-rupture strength of 12,700 psi, These are slightly below those measured for swaged rods of commercial tungsten-3.7 vol pct thoria. Only those tungsten-thoria dispersions containing a stoichiometric deficiency of oxygen yielded a significant strengthening effect. A low-melting eutectic formed in extruded tungsten dispersions containing either zirconia or yttria, which caused a lowering of the tensile strengths. These tensile strengths were only slightly higher than strengths of elemental tungsten made from commercial powder having a particle size of 2.4 microns (Fisher subsieve). Sheet made from this commercial tungsten had a slightly higher tensile strength than tungsten made by freeze drying, but the freeze-dried tungsten sheet had a lower recrystallization temperature, a lower ductile-to-brittle transition temperature, and a higher purity.

Jan 1, 1971

By V. Vekris

A diverse patent portfolio and an effective intellectual property strategy are vital in today’s small business world. Not only does a diverse patent portfolio enable a company to secure a monopoly within the market, it greatly increases the value of a company’s intangible assets and keeps competitors at bay. An overview of the patenting process as it pertains specifically to the materials science-related start-ups will be given, together with a summary of some general patenting strategies and a review of some patenting errors to be avoided, such as premature disclosure of the invention to the public. Additionally, a review of new “green technology” initiatives recently adopted by Patent Offices around the world is also provided. These initiatives are expected to greatly benefit patent applicants in the fields of metallurgy and mining, where research efforts are often directed to environmentally-friendly products and processes. INTRODUCTION Patents are playing an increasingly significant role in the business world. A diverse patent portfolio can enable a company to secure a monopoly within the market, which can provide a competitive advantage over competitors. At the same time, patent portfolio of any size can greatly contribute to the total value of a company’s intangible assets. As an example, Nortel entertained bids in 2011 for its portfolio of about 4000 patents, a large portion of which were directed to 3G- and 4G-mobile communication technologies. The portfolio was eventually sold for $4.5 billion to a consortium including Apple, EMC, Ericsson, Microsoft, Research in Motion, and Sony. Copper mining, and indeed the global mining industry as a whole, is facing challenges. Ore deposits are increasingly low grade, complex, and deeper in the ground, rendering copper mining operations more difficult and costly. Production costs are increasing. According to one study, the cost of producing copper has increased by an average of 10% per year since 2005 (Cantallopts, 2017). To illustrate, the cost of producing a pound of copper in 2005 was 90 cents, but had increased to 217 cents by 2014.

Jan 1, 2019

By G. Swartz, R. J. Brison, R. A. Wyman, J. P. Vandenhoeck, S. E. Khalafalla

Magnetic fluids are commonly composed of ultrafine submicron particles of magnetite (Fe3O4) dispersed in either a kerosene or a water carrier medium with oleic acid as a protective colloid. The unique property of these fluids is that when the magnetic particles are attracted to a magnet the carrier medium moves along with the particles so that the liquid also appears magnetic. The availability of a fluid whose gross behavior changes sharply in a magnetic field without affecting its rheologic characteristics is becoming critical for many technologic applications. About two gener¬ations ago suspensions of relatively large, micron-sized ferromagnetic particles in oil proved useful in clutches, brakes, and dashpots. These were called magnetic clutch materials, and their viscosities were highly dependent upon the applied magnetic field, in contrast to true mag¬netic fluids which retain their fluidic characteristics under all applied fields and field gradients. While the term "ferrofluid" was used by Rosensweig and Kaiser&apos; to designate a magnetic colloid composed of a dispersed magnetic ferrous material, the more general term, "mag¬netic fluid," is preferred. This is because these fluids may contain ferro- or ferrimagnetic substances, such as cobalt, nickel, gadolinium, dysprosium, or magnetic ferrites in carrier liquids, such as hydrocar¬bons (kerosene), silicones, water, fluorocarbons, etc. Preparation of Magnetic Fluids Magnetic fluids were first prepared by Papell and Faber, at the NASA Lewis Research Center, Cleveland, Ohio, by tumbling ferrite materials for several weeks in a carrier medium (such as kerosene) and a dispersing agent (such as oleic acid) with steel balls. Rosensweig et al.1 compared the stability of their ferrofluids obtained from both metallic iron and the magnetic oxides of iron, Fe3O4 and yFe2O3. They found that, although the saturation magnetization of iron is 3.5 times greater than that of magnetite, its colloidal solutions deterio¬rated much more rapidly. The iron particles were undoubtedly rapidly oxidized to a nonmagnetic state due to the enormous surface area of these colloidal particles. Because the properties of these fluids are highly dependent on particle size and may acquire opposite characteristics by small incre¬ments in that size, more controllable methods of preparation have been developed recently by Khalafalla and Reimers.6 In one method metastabilized pyrophoric wiistite is ground to colloidal size in a kerosene oleic acid mixture, and then it is disproportionated to colloi¬dal magnetite and iron at temperatures just below the eutectoidal temperature of wüstite stability (570°C); thus, t < 570°C 4 FeO t > 570°C Fe + Fe30, (1) Because of its antiferromagnetic characteristics, the precursor wüstite is much easier to grind than magnetite. Another method3 avoids grinding entirely and utilizes a peptiza¬tion technique from ferrous materials in the molecular state of aggrega¬tion. This latter procedure has resulted in preparation of strong fluids at considerable savings in cost.

Jan 1, 1985

This chapter summarizes data on crude mineral production for the United States, its island possessions, and the Common- wealth of Puerto Rico. Included also are tables that show the principal mineral commodities exported from and imported into the United States and that compare world and U.S. mineral production. The detailed data from which these tables &apos;were derived are contained in the individual commodity chapters of volume I and in the State chapters of volume II of this edition of the Minerals Yearbook. Although crude mineral production may be measured at any of several stages of extraction and processing, the stage of measurement used in this chapter is what is normally termed "mine output." It usually refers to minerals or ores in the form in which they are first extracted from the ground, but customarily includes the production of auxiliary processing at or near the mines.

Jan 1, 1978

By J. Kempken, R. Degel, J. Kunze, R. König

The FeNi technology is currently dominated by high-power submerged arc furnaces, often designed as smelter as "two-inline-solution". To achieve the intended high efficiency, state-of-the-art design in good correlation with ores and reductants and an integrated layout of the whole plant is of great importance. An introduction will be given to general aspects in the production FeNi, plus a detailed overview of design principles for large FeNi smelters and finally some examples of innovations and research projects concerning Fe-Ni.

Jan 1, 2007

By Larry R. Powell

The Bureau of Mines, in cooperation with the Illinois Mine Subsidence Insurance Fund, is monitoring the response of two foundations to ground movements induced by subsidence from high extraction mining in southern Illinois. The objectives of the monitoring program are to study the inter- action between the ground surface and a foundation during a subsidence event and to determine the capability of the tiltmeter to detect and monitor subsidence movements. Tiltmeter data were obtained on two foundations constructed near Sesser, IL. One of the 30-by 40- ft foundations was constructed with a typical poured concrete footing, the other with a rein- forced-concrete footing poured on top of pol yethylene sheeting placed over a compacted layer of sand. Soil-filled bins were placed on the perimeters of both foundations to simulate superstructure loads. Monitoring pins and tiltplates were installed on the corners and midpoints of the footing. Additional survey points were established on the five-acre site to track the mining advance. This paper describes the monitoring instrumentation and techniques as they relate to the mining and site conditions. The capability of a tilt- meter to detect and follow the tilt of the foundations is demonstrated.

Jan 1, 1986

By Richard C. Holmquist

Some of you may be old enough to remember -- as I do -- the early days of World War II. A highly prepared, well-equipped Japanese striking force had moved like lightning across the South Pacific islands and Southeastern Asia. As the invasion force pushed its way down the Malaysian Peninsula, Singapore stood serene and beautiful, protected by its natural moat of water, busy as ever with its commercial pursuits. One can see its captains of trade and industry now, sitting com¬fortably on the veranda of the "Singapore Country Club", sipping scotch between cricket games, convinced that the weary, logistically extended Japanese force couldn&apos;t possibly cross over to their island which had been so secure for a hundred&apos; years or more. No need to remind you what happened. The brave men in their ships at sea and in the gun emplacements ashore were hopelessly out-gunned and out-maneuvered.

Jan 1, 1979

By Dirceu da Silva Junior

Os compósitos poliméricos com fibras naturais são geralmente fabricados com a técnica de moldagem por compressão a frio ou a quente, na qual as fibras são as compactadas com resina em um molde. Em geral, a matriz deve ser feita de um aço resistente à fratura, à fadiga e dureza adequada, pois grandes esforços são utilizados na prensagem do material entre 100 a 300°C. Neste contexto, o objetivo deste trabalho foi avaliar a influência da temperatura na dureza dos aços SAE 8620 e SAE 8640. Amostras foram submetidas ao tratamento térmico de têmpera a 900oC e revenimento na faixa de 150 a 650ºC. Posteriormente foram lixadas e polidas conforme os métodos convencionais de preparação metalográfica. Na revelação da microestrutura utilizou-se o reagente Nital 2%. Para avaliar a influência da temperatura foram feitas medidas de dureza Rockwel C e análises microestruturais das amostras. Os resultados mostraram que os materiais apresentam uma microestrutura típica de martensita revenida após têmpera e revenido. No entanto, a dureza é superior a 45 RC somente para o aço SAE 8640 até revenimento de 350°C. Conclui-se, portanto, que apenas o aço SAE 8640 é adequado para fabricação de moldes para moldagem a quente de compósitos poliméricos.

Aug 16, 2017

By W. T. Benson

The Bureau of Mines has undertaken investigations to examine selected deposits of beryllium throughout the United States. The beryllium deposit about 6 miles southeast of Lone Pine in the Owens Valley region of Inyo County, Calif., was among those selected for study. In 1960, field work was conducted on the Inyo Beryl claim to determine the extent and character of the beryl-bearing deposit. This report describes the work that was done. In the area investigated, the beryl occurs disseminated in granite and limestone and as stringers. Apparently, the stringers are related to nearby pegmatite dikes, inasmuch as some appear to contain fine-Grained pegmatite. Granitic rocks enclose most of the stringers, which occur as fracture fillings, ranging from thin seams to 4 inches in thickness. The stringers are of muscovite, quartz, albite, and beryl. Some also include epidote and fluorite. For the most part, they are widely spaced. Therefore, mining of substantial tonnages averaging better than 0.2 percent beryl does not appear feasible.

Jan 1, 1962

By G. W. Imholz

A number of interesting wells were drilled in north central Texas during 1940. The Shell Oil Company&apos;s Smith well in scc. 143, block I, H. and T. C. survey, Stonewall County, was completed for an initial production of 581 bbl. per day from the Mississippian limestone, with a total depth of 6065 ft. The same company&apos;s Patterson well, sec. 393, block D. H. and T. C. survey, Stonewall County, tested the Ellenburger limestone and was abandoned as a dry hole with a total depth of 6760 feet. In Nolan County the Tex-Harvey Oil Co. drilled a well in sec. 43, near the Tipton well, which was completed as a small producer in the Strawn section. The Tex-Harvey well tested this producing horizon but was abandoned as a dry hole with a total depth of 5210 feet. The Montour-Haggart well, sec. 184, block 2, H. and T. C. survey, Fisher County, tested the Strawn and was abandoned with a total depth of 5664 feet. The Georgian Oil Company&apos;s Blach, sec. 309, T. R. and L.. Shackelford County, encountered the top of the Ellenburger limestone at 4725 ft. After being plugged back to 3915 It. from a total depth of 4825 ft., the well tested 10 bbl, of oil per day and 300 bbl. of water. The W. I. Sothern No. 2 Carlisle well in sec. 293 was deepened to the Cambrian. The top of the Ellenburger was encountered at 6540 fcet. A wildcat well in Fisher County, the E. A. Stephenson-Maberry, apparently opened a new pool when the well encountered sand from 3298 lo 3302 ft. and was completed for 50 bbl. per day in the Cook sand horizon. In Jones County, the King Oil Company&apos;s Olsen well, sec. 158, B. B. B. and C. survey, extended the Avoca-Olander pool. The well was completed for 263 bbl. in 8 1/2 hr. from the Palo Pinto limestone, from 3298 to 3302 ft. Ungren-Frazier extended the Akard pool with No. I Akard, in the D. &apos;T. Bruce survey. The well was completed for 83 bbl. per day from the Cook sand, encountered from 2109 to 2126 feet.

Jan 1, 1941

By G. W. Imholz

A number of interesting wells were drilled in north central Texas during 1940. The Shell Oil Company&apos;s Smith well in scc. 143, block I, H. and T. C. survey, Stonewall County, was completed for an initial production of 581 bbl. per day from the Mississippian limestone, with a total depth of 6065 ft. The same company&apos;s Patterson well, sec. 393, block D. H. and T. C. survey, Stonewall County, tested the Ellenburger limestone and was abandoned as a dry hole with a total depth of 6760 feet. In Nolan County the Tex-Harvey Oil Co. drilled a well in sec. 43, near the Tipton well, which was completed as a small producer in the Strawn section. The Tex-Harvey well tested this producing horizon but was abandoned as a dry hole with a total depth of 5210 feet. The Montour-Haggart well, sec. 184, block 2, H. and T. C. survey, Fisher County, tested the Strawn and was abandoned with a total depth of 5664 feet. The Georgian Oil Company&apos;s Blach, sec. 309, T. R. and L.. Shackelford County, encountered the top of the Ellenburger limestone at 4725 ft. After being plugged back to 3915 It. from a total depth of 4825 ft., the well tested 10 bbl, of oil per day and 300 bbl. of water. The W. I. Sothern No. 2 Carlisle well in sec. 293 was deepened to the Cambrian. The top of the Ellenburger was encountered at 6540 fcet. A wildcat well in Fisher County, the E. A. Stephenson-Maberry, apparently opened a new pool when the well encountered sand from 3298 lo 3302 ft. and was completed for 50 bbl. per day in the Cook sand horizon. In Jones County, the King Oil Company&apos;s Olsen well, sec. 158, B. B. B. and C. survey, extended the Avoca-Olander pool. The well was completed for 263 bbl. in 8 1/2 hr. from the Palo Pinto limestone, from 3298 to 3302 ft. Ungren-Frazier extended the Akard pool with No. I Akard, in the D. &apos;T. Bruce survey. The well was completed for 83 bbl. per day from the Cook sand, encountered from 2109 to 2126 feet.

Jan 1, 1941