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By Berenice B. Mitchell

THE STATISTICAL tables in this chapter present, country by country, the mineral production of the world in 1949-50. The figures are on a mine basis, unless otherwise indicated, except for cement, coke, and steel, which are measured at the processing plant. The tables are essentially a retabulation, by countries, of the 53 commodity world tables appearing in the various chapters of this volume. For lack of comprehensive information, data for the following minerals are excluded: Andalusite, aplite, asphalt, boron, bromine, calcite (optical), calcium chloride (natural), carbon dioxide, clay, columbium (niobium), diatomite (kieselguhr), dumortierite, emery, garnet (abrasive), gem stones (other than diamonds), germanium, greensand, grindstones, helium, indium, iodine, kyanite, lithium, magnesium compounds (other than magnesite), meerschaum, mineral pigments, monazite, natural gas, natural gasoline, oil shale, olivine, perlite, pumice, quartz crystal, radium, sand and gravel, selenium, sillimanite, sodium salts (other than common salt), stone, strontium, sulfur (byproduct), tantalum, tellurium, thallium, topaz (industrial), tripoli) uranium, vermiculite, wollastonite, and zirconium. In addition, a few minor geographic areas for which no statistics are available, are also omitted from the tabulation; it is believed that no significant quantities of minerals are mined in any of these areas. The statistics in these tables were derived principally from questionnaires sent, in cooperation with the United States Department of State, to the governments of each country. Supplementary sources were United States consular reports, the Imperial Institute's Statistical Summary of the Mineral Industry of the British Commonwealth and Foreign Countries, other official publications of various countries, the United Nations Statistical Yearbook, the Year Book of the American Bureau of Metal Statistics, Minerais et Metaux, business magazines, and company reports. Where official data were not available, esti-

Jan 1, 1953

By R. C. Gabler

Laboratory tests on a combined nitrogen roast--two-stage leach--electro-winning approach show promise as a possible process for recovering copper, sulfur, iron oxide, and valuable minor metals (gold, silver, and molybdenum) with a minimum impact on the environment. During the nitrogen roast at 800° C, 15 to 20 percent of the sulfur together with a significant fraction of the volatile elements, such as arsenic, bismuth, lead, and zinc, are removed from the chalcopyrite concentrate. The resulting calcine, consisting of 8-chalcopyrite, troilite, and a bornitelike structure, is leached with hydro-chloric acid to remove 70 to 85 percent of the iron. The digenite in the leach residue is dissolved in an oxygen-saturated, spent sulfate electrolyte. Using a graphite 'anode plus sulfur dioxide to reduce interference from ferric iron, copper of 99.99+ purity is electrowon at current efficiencies of 88 to 92 percent and a cell voltage of 0.4 to 0.5 volt. Copper recovery for the overall process is 98 to 99 percent. Sulfur is obtained in the elemental form from the roasting and leaching steps. Iron can be recovered from the hydro-chloric acid leach solution. Gold, silver, and molybdenum are concentrated in the silica residue from the spent electrolyte leach.

Jan 1, 1975

By Sarkis G. Ampian

The Bureau of Mines has developed a method for identifying fine particles of beryl in mineral samples by preferentially staining the beryl grains. The sample is first subjected to a heated sodium hydroxide solution to etch the beryl particles, which are subsequently stained an intense blue color in a boiling alkaline solution of quinalizarin. Positive identification of beryl grains permits quantitative analyses by microscopic techniques. INTRODUCTION Beryl, a beryllium aluminum Silicate, is the principal ore mineral of beryllium. The only known commercial concentrations of this mineral are found in pegmatite dikes of granitic composition. Normally beryl is associated with muscovite mica, quartz, and the sodium-and potassium-bearing feldspars (orthoclase, microcline, and albite). Other beryllium-bearing minerals which are found occasionally in minor amounts with beryl are phenacite, a beryllium silicate, and chrysoberyl, a beryllium aluminate.

Jan 1, 1962

By S. D. Maksirnovic, Fred N. Kissell

The use of vertical surface degasification boreholes with bleeder systems and the use of a timbered bleeder system to degasify gob areas were studied by (the Bureau of Mines. This report describes three gob degasification studies ,conducted in the Pittsburgh coalbed. One study was conducted to determine the number of panels degasified with one large borehole . The study showed that the borehole provided degasification for three panels. Another study was conducted during the retreat of a 35-acre panel with a single-entry and a two-entry bleeder system and a large surface borehole. A major portion of methane emitted from the panel was carried away by the bore- hole, leaving the bleeder entries relatively free of methane. The last study was made to determine the effectiveness of a timbered bleeder system. The bleeder entries successfully degasified the gob area when enough entries were available and adequate pressure was available to force the air through roof falls.

Jan 1, 1980

By P. D. Kovscek

High-pressure streams of water, known as water jets, can be used to improve the cutting efficiency of mechanical bits. During prior testing by the Bureau of Mines, the cutting performance of a longwall shearer, equipped for water-jet-assisted cutting, was evaluated. The performance of the shearer did not improve while using water jet assist because the pressure of the water delivered to the rock surface was inadequate. The study, described in this report, resulted in a determination of the major cause of water pressure loss on the shearer, and an evaluation of the techniques for increasing the water pressure at the rock surface. The results show that the major pressure loss, which occurred between the nozzle and rock surface, is directly affected by the amount of fluid turbulence that develops just upstream from the nozzle. Preventing a sudden change in the direction of the flow channel can increase the stagnation pressure as much as 400 pct. Smoothing the surface of the flow channel in the shearer bit block would increase the stagnation pressure delivered to the rock surface by 35 pet.

Jan 1, 1989

By W. R. Wrzensinski

This report presents the findings from a l-yr Bureau of Mines program in which sulfur concrete reinforcing materials were tested and evaluated to determine their resistance to corrosion. It also summarizes the permeation characteristics of sulfur concrete and the exemplary performance of precast, reinforced sulfur concrete structures in various industrial environments. The Bureau is furthering the development of sulfur concrete technology as part of a larger effort to find uses for the Nation's plentiful sulfur resources in construction materials. Sulfur concrete is a corrosion-resistant material that can be used in acid and salt environ-ments where conventional materials fail. Penetration of corrosion-inducing agents is minimized because of the low permeation characteristics of sulfur concrete.

Jan 1, 1988

By F. Chase, D. Pappas

Pillar recovery has been associated with nearly one third of roof fall fatalities in underground coal mines during the past decade. Safe pillar recovery requires global stability and local stability. Global stability is addressed primarily through pillar design. The local stability risk factors include cut sequence, the final pillar stump, supplemental supports (timbers vs. Mobile Roof Supports (MRS)), roof bolting, and many others. The National Institute for Occupational Safety and Health (NIOSH) has evaluated each of these factors through field research and analysis of accident statistics. The paper discusses design methods and technologies that have been transferred to the mining community and implemented.

By R. D. Brown

There are techniques for separating aluminum alloys from mixed scrap, but there are no efficient ways to separate wrought aluminum from cast aluminum. This Bureau of Mines report describes a novel technique for separating mixed aluminum alloy scrap into cast and wrought aluminum alloy fractions. The technique, which uses conventional heating, fragmentizing, and screening equipment, exploits differences in the mechanical properties of cast and wrought aluminum alloys at elevated temperatures. The cast alloys become brittle at high temperatures owing to intergranular melting of regions of eutectic composition. This melting begins to occur as the solidus temperature for each alloy is reached. Solidus temperatures for casting alloys generally range from 520° to 580° C, but are above 600° C for most wrought alloys. Thus, the casting alloys are easily fragmented while the wrought alloys remain ductile in the proper temperature range. Starting with a mixture containing approximately 80 pct cast and 20 pct wrought alloys, fractions of 100 pct cast and 98 pct wrought have been produced.

Jan 1, 1985

By John S. Berber

Tar produced as a byproduct from low-temperature carbonization of coal contains only small amounts of valuable lower boiling tar acids but relatively high percentages of high-boiling tar acids. These high-boiling tar acids are characterized by a high degree of alkylation and can be converted into the lower boiling homologs by catalytic treatment to remove the alkyl groups or decrease their chain lengths.

Jan 1, 1965

By Stephen D. Cramer

The solubility of methane, carbon dioxide, and oxygen was measured in brines at temperatures from 0° to 300° as part of Federal Bureau of Mines research on the corrosion of metals in high-temperature geothermal and mineral processing environments. Solubilities were measured by the technique of extracting pure gas, dissolved at pressures where Henry's law was applicable, from known volumes of brine. The results were smoothed with respect to temperature. The solubility, expressed in terms of the Henry's law constant, reaches a maximum at temperatures ranging from 60° to 100° C for methane and oxygen, and from 160° to 170° C for carbon dioxide. The Henry's law constant increases, that is, gases are salted out of the brines, in the presence of dissolved salts. Salting-out coefficients are strongly dependent upon temperature. The temperature dependence of the Henry's law constant for geothermal brines is different from that for sodium chloride brines owing to the more complex chemistry of the geothermal brines. The solubility of oxygen and carbon dioxide in brines exposed to air saturated with water vapor and at a total pressure of 760 mm Hg is reported for temperatures from 0° C to the normal boiling point.

Jan 1, 1982

By Paul E. Loustaunau, Devah Galloway, Catherine Wetherby

This report describes a project in which Development of a Supervisory and Management Training Program for the Underground Coal Mining Industry was developed and evaluated. The project was carried out in two phases. The first phase was a research effort to develop specifications for the program. The second phase was a development and evaluation effort. In the second phase, training programs for first-line supervisors (section foremen) and for middle managers (mine/shift foremen and mine superintendents) were prepared in accordance with the specifications and evaluated by members of the industry. This report describes the project and presents the conclusions drawn there from.

Jan 5, 1983

By Je M. Oh

The Bureau of Mines is conducting research to determine the high temperature oxidation resistance of substitute stainless steels (SS) containing two less strategic elements, Al and Si, instead of Cr. Chromium is considered to be a critical and strategic metal. Although the Cr content was reduced to 8 wt pct, the alloys showed better oxidation resistance than did 304 SS containing 18 wt pct Cr. Specifically, the alloys that contained Fe-8Cr-16Ni with combinations of Al and Si showed excellent oxidation resistance even at temperatures up to 1,000° C. In this study, the effects of the alloying elements on oxidation kinetics and morphology of oxides were investigated using a Cahn Rg electrobalance, scanning electron microscopy, an energy-dispersive X-ray analyzer, X-ray diffraction, and an electron microprobe. Aluminum and silicon additions in combinatin were more effective in providing oxidation resistance than either element was alone.

Jan 1, 1986

By James S. Browning

Domestic production of lithium minerals, source of the lightest metallic element, has increased from an average of 1,327 short tons of concentrate in the 1935-39 period to approximately 37,830 short tons in 1954. This rather phenomenal growth in production and use reflects growing industrial interest in the metal and its salts. This information circular has been prepared to summarize for the casual technical reader the reserve, mining, processing, and consumption situation pertaining to the mineral spodumene - the principal source of lithium. A relatively complete bibliography is included for those who may need more detailed information.

Jan 1, 1958

By Wilson Blake

The Bureau of Mines used a mathematical model based on the finite element method of stress analysis to calculate stresses and displacements surrounding an open pit mine in a gravity-loaded rock mass. Comparison of the finite element solution for a semicircular notch in a gravity-loaded plate with the theoretical solution for a semicircular notch in a plate under uniform compression parallel to the free boundary demonstrates the inapplicability of the latter method to openings at the free surface of a gravity-loaded medium. High stress concentrations are formed at irregularities along the boundary of an open pit in a gravity-loaded continuous competent rock; however, for this type of rock the magnitudes of the stresses are too low to be considered a major factor in open pit slope stability. High stress magnitudes will occur if, in addition to the gravity stress field, a large horizontal stress field exists.

Jan 1, 1967

By D. W. Frommer

As one phase of a general problem of recovering sulfide slimes, mineral-dressing research was conducted on flotation tailing from the St. Joseph Lead Co., Bonne Terre, Mo., mill to recover a significant portion of the residual, finely divided galena. Production of a high-grade concentrate was not part of the immediate objective. Only a reasonable ratio of concentration of lead sulfide slime was sought, since the problem of upgrading by mechanical or extractive processes would be considered in the later stages of this study. The results show that, from a feed material averaging 0.20 percent lead (about 70 percent finer than 400-mesh), a recovery of up to 45 percent could be effected by flotation in rougher concentrate analyzing up to 6.5 percent Pb. These results were obtained by using larger quantities of various xanthates and sodium sulfide than used customarily in mills. Sodium sulfide, which is ordinarily detrimental to flotation of galena, was beneficial in this case.

Jan 1, 1959

By Michael G. Zabetakis

The process of ?gasfreeing? has been defined3/ as "* * * the removal of oil and vapors from tanks, pipelines, and compartments to render such spaces safe for the intended work," Generally, part or all of a vessel is gasfreed for one of several reasons: Periodic cleaning; tank inspection or repairs; shipyard overhaul or major repairs; or change of cargo, Curing the gas- freeing, flammable or explosive4/ mixtures (mixtures through which a flame can propagate after ignition by an open flame, heated object, electrical charge, or other means) may be produced. These mixtures create an explosion hazard, as the pressures produced after their ignition are often great enough to completely demolish the vessel and kill all those aboard, This paper outlines a study by the Federal Bureau of Mines of the gas explosion hazards likely to be encountered while gasfreeing a vessel compartment. To better understand these hazards it will first be necessary to review the language used in gas- explosions work. This language is considered in the following sections. Inert gases such as carbon dioxide, nitrogen, water vapor, and others can be used to decrease the range of combustible-vapor concentrations in which flammable mixtures are formed. Sufficient quantities of such gases can often be added to cause a mixture that originally was flamable to become nonflammable. Unfortunately, the use of water vapor in this application is complicated by the fact that elevated temperatures are required to keep the water in the vapor state. In practice, it may be difficult to maintain these elevated temperatures throughout the space (such as a cargo tank) to be inerted for any length of time. Accordingly, where other inert gases are not available, it may be desirable to gasfree a Lank by using heated air. To do this, the combustible vapors should be flushed as quickly as possible from the space to be gasfreed. In a properly designed system, large tanks were gasfreed with a littlee as 6 volumes of air per volume of tank capacity.

Jan 1, 1961

By Jr. Hardy, H. Warren Shen

"A study is presently underway by the authors to investigate the character of the bit-coal interaction during coal cutting and its influence on the size and shape distributions of the generated dust. An important aspect of this on-going project is the development of acoustic emission (AE) criteria which would make it possible to carry out remote monitoring of coal cutting operations. The on-going AE studies are fundamental in form and were undertaken to evaluate the general feasibility of AE monitoring techniques using simplified coal breakage and cutting procedures. The present paper will focus on the test facilities, experimental techniques, and results associated with linear, single-bit cutting. An AE-transducer, attached directly to the bit, detected AE signals during the cutting process.Experiments have been carried out on seven specimens of coal obtained from the USBM experimental mine at Bruceton, Pennsylvania. Three separate cuts were made for each of two bit angles (10 and 45 degrees) and two bit velocities (0.085 and 0.169 cm/sec), for a total of 12 separate cuts. Data associated with resulting particle size distribution and AE characteristics (major dominant frequency components) will be discussed. Data analysis has also been underway using a computer-based pattern recognition system known as ICEPAK (Intelligent Classifier Engineering Package). This program is able to evaluate over 100 features of an AE event and to make objective comparisons between AE signals associated with different loading or cutting parameters. The results to date show that AE generated during some of the test conditions can be recognized by ICEPAK with a recognition rate of 90% and higher while other conditions cannot at present be separated with a suitable recognition rate. Further analysis of the experimental data is presently underway.The reduction of the severity, and eventual elimination, of Coal Workers' Pneumoconiosis (CWP) depends on gaining fundamental understanding in a number of major areas. These include dust generation and entrainment, transportation, suppression, medical effects of dust, and possible treatment. At present a project is underway by the authors to investigate the character of the bit-coal interaction during coal cutting and its influence on the size and shape distributions of the generated dust. An important aspect of this on-going project is the development of acoustic emission (AE) criteria which would make it possible to carry out remote monitoring of coal cutting operations. Suitable on-line analysis of monitored AE data would allow engineers to evaluate factors such as shearer bit conditions and cutting efficiency, and to quantify the particle size and shape distribution of the generateddust. The on-going AE studies are fundamental in form and were undertaken to evaluate the general feasibility of AE monitoring techniques using simplified coal cutting procedures. To date experiments have been carried out on coal under uniaxial compression, linear single-bit cutting, and cutting using a laboratory-scale, single-bit shearer. A brief outline of the overall study has been presented in an earlier paper (Hardy, Shen and Kimble, 1995). This paper will consider the linear single-bit cutting studies in more detail.It is generally accepted today that most solids emit low-level seismic signals when they are stressed or deformed. In this paper this phenomenon will be referred to as acoustic emission (Hardy 1972, 1981, 1989). In essence, the measurement of AE activity in a field or laboratory structure is relatively simple. A suitable transducer is attached to the structure, the output of the transducer is connected to an associated monitoring system, and the AE signals occurring in the structure, due to internal or external stress, deformation, and failure are suitably acquired, pre¬processed and recorded."

Jan 1, 1998

By R. E. Head

At the microscopic laboratory of the Bureau of Mines Intermountain Experiment Station, Salt Lake City, Utah, efforts are being made to devise methods of differentially coloring finely crashed minerals as a means for their identification. Staining would facilitate sight recognition of minerals under the microscope and would be of great value in the study of crushed ores, concentrates, and tailings. Since the treatment of ores for their beneficiation is primarily based on the recovery of the minerals containing the clements of value, it is extremely important that these minerals should be known and that a method for quickly determining them when in minute fragments should be available. Herein lies one of the greatest uses for color methods. In many cases it is a difficult matter for even the trained petrographer and mineralogist to identify finely crushed minerals quickly. Although ordinary petrographic methods are accurate, they are often time--consuming and are not suitable to the needs of millmen who require, especially in the examination of tailings a method for determining minerals by inspection.

Jan 1, 1929

By A. R. Rule

Research was conducted by the Bureau of Mines to develop a process for utilization of Idaho kyanite. A continuous gravity-flotation separation process was applied successfully to recover kyanite-group minerals from an Idaho ore containing about 21 percent combined kyanite, andalusite, and sillimanite. Dry magnetic separation of the concentrate resulted in a product containing about 90 percent kyanite at a recovery of 63 percent of the kyanite-group minerals in the ore, Alumina and silica analyses were within the range generally accepted for conversion to mullite, and the finished products had a pyrometric cone equivalent of more than 38. A recovered garnet coproduct may be of commercial value.

Jan 1, 1973

By John Nagy

The Bureau of Mines examined explosion development in a closed spherical vessel, mathematically correlating flame travel, pressure, and time with parameters defining the reaction. The model assumes that burnt and unburnt zones are separated by a thin, radially moving flame front. Isothermal and adiabatic systems are considered. Correlation with gas and dust explosion data is better for the adiabatic system, but the isothermal development is simpler and in reasonably good agreement. Interpretation of the explosion phenomena is facilitated by expressing the rate of mole change in the flame front in terms of elementary parameters. This expression is developed by examining the components of spatial-flame velocity.

Jan 1, 1969