Search Documents

By Mônica Aline Magalhães Gurgel

O presente trabalho estudou a evolução microestrutural durante o recozimento no campo intercrítico de um aço baixo carbono com micro-adição de nióbio e molibdênio, laminado a frio, destinado a indústria automobilística, sendo este material da classe dos aços bifásicos. Com o intuito de verificar se os parâmetros utilizados no processo de fabricação (laminação a quente e a frio em função de uma determinada composição química) foram definidos de forma eficaz para obtenção da microestrutura esperada para um material “Dual Phase”. Os estudos foram suportados pelas análises da evolução microestrutural durante o processo de recozimento em escala laboratorial e análise dilatométrica, com o objetivo de determinar a faixa de temperatura no tratamento de recozimento em que as melhores propriedades foram atingidas. As caracterizações microestruturais e mecânicas foram avaliadas por Microscopia Óptica, Microscopia Eletrônica de Varredura (MEV) e ensaios de dureza Vickers.

Jul 30, 2018

By Susan Brink

The U.S. Bureau of Mines is investigating the potential of in situ leach mining a variety of Cu, Mn, and Au-Ag ores. Geologic characterization of ore samples from laboratory leaching experiments is conducted both prior to and after leaching to assess the effects of leaching on the chemistry, mineralogy, and texture of the rocks. The identification and chemical compositions of ore, gangue, and reaction products are determined by a combination of techniques such as reflected and transmitted light microscopy, X-ray diffraction, electron diffraction, electron microprobe analysis, and backscattered electron imaging with scanning electron microscopy. The distribution of the desired metal in various mineral phases can be illustrated using elemental X-ray maps. The potential of reactive gangue minerals to rob Cu from leach solutions is investigated with the aid of transmission electron microscopy. Porosity and permeability are measured to determine how effectively the host rock can transmit leach solution. Textural relationships between ore, gangue, secondary reaction products, and fluid channelways are determined by petrographic examination and are documented by optical photomicrographs and secondary electron imaging. Representative sample selection is described, and several epoxy impregnation and sample mounting techniques are discussed.

Jan 1, 1991

By Robert D. Gunn, John E. Boysen, Dennis D. Fischer

The second underground coal gasification experiment conducted by ERDA's Laramie Energy Research Center at a site near Hanna, Wyo., was completed on Jul. 30, 1976. During the experiment production reached 0.32 blm3/d (12 M cu ft/d) of 6.9 w/m3 gas (175 Btu per cu ft). Approximately 6100 tonnes (6700 tons) of coal were gasified during the experiment. Energy return ratios of 4.5 to 5.3, coal gas thermal efficiencies of 76 to 89%, and overall process efficiencies of 65 to 74% were achieved during the second Hanna experiment. This paper describes the experiment and the results obtained with emphasis given to the determination of the energy recovered relative to energy consumed in conducting the test. Data from this determination are compared with previously published data from the first test conducted at Hanna during 1973-74.

Jan 1, 1978

Coal Division Mineral Industry Education Division Industrial Minerals Division Minerals Beneficiation Division Mineral Economics Division Mining, Geology and Geophysics Division Council R C Stephenson, Chairman (Ind Min Div), M D Cooper (Coal), H F Yancey (Coal), S D Michaelson (MBD), Will Mitchell, Jr (MBD), J R Van Pelt, Jr (MIED), S S Cole (Ind Min Div), J D Forrester (MGGD), L E Shaffer (MIED), E L Clark (MGGD), C W Merrill (MED), E H Robie, Acting Secretary, 29 West 39 Street, New York 18, New York

Jan 1, 1955

By Fábio de Oliveira Braga

Blindagens cerâmicas são frequentemente utilizadas para proteção contra projéteis de alta energia, como os de calibre 7,62 mm e 5,56 mm. Recentemente, foi demonstrado que a modificação da geometria da face de impacto, de plana para convexa, possibilita uma melhor distribuição das tensões geradas pela interação do projétil com o alvo. Este efeito provocaria um aumento na absorção de energia do projétil, proporcionando uma maior segurança ao usuário. No presente trabalho caracterizou-se uma blindagem com a face cerâmica convexa, por meio da metodologia da norma NIJ-0101.06 (2008), ou seja, pelo ensaio balístico com medição do trauma em um material de referência que simula a consistência do corpo humano. Este ensaio visa a aplicação do material em coletes balísticos. Foi observada uma melhora significativa no desempenho balístico após a modificação da geometria.

Oct 30, 2017

By Gustavo Estrela da Silva

O presente trabalho tem por objetivo avaliar a influência da taxa de resfriamento durante a solidificação na formação de diferentes microestruturas de ferros fundidos. Para tal, uma liga de ferro fundido com pequena adição de Si foi fundida em forno de indução e vazada em molde de areia, gerando um corpo de prova dotado de regiões com diferentes espessuras de parede, impondo ao metal líquido vazado diferentes taxas de resfriamento. Foi possível constatar que o aumento da taxa de resfriamento aumenta a tendência de formação de ferro fundido branco, respeitando-se o equilíbrio metaestável Fe-cementita, e que menores taxas de resfriamento priorizam a formação de ferro fundido cinzento (respeitando o equilíbrio estável Fe-grafita). Estudos macrográfico e micrográfico detalham as regiões de ferro fundido branco, mesclado e cinzento, e relacionam as diferentes morfologias obtidas com as taxas de resfriamento impostas.

Aug 8, 2018

By G. Cailletaud, I. Guillot, D. Larouche, R. Martinez, D. Massinon

The precipitation of Al2Cu particles in a 319 T7 aluminum alloy has been modeled. A theoretical approach enables the concomitant computation of nucleation, growth and coarsening, based on an implicit scheme using the finite differences. The equation of continuity is discretized in time and space in order to obtain a matricial form. The inversion of a tridiagonal matrix allows us to determine the evolution of the size distribution of Al2Cu particles at t + dt. The fluxes of solute in-between the boundaries, as well as the ones at the boundaries, are computed in order to respect the conservation of the mass of the system. The main results of the model are compared to TEM measurements. Simulations provide quantitative features on the impact of the cooling rate on the size distribution of Al2Cu particles in good agreement with the TEM measurements. This metallurgical model is integrated into FEA software in order to perform mechanical computations. This kind of multiscale approach allows new perspectives to be investigated in the process of designing cylinder heads. It enables a more precise prediction of the microstructure, its evolution as a function of continuous cooling rates and its impact on the integrity of the structure.

Jan 1, 2015

By Frank J. Perzak

This report describes a U.S. Bureau of Mines study on the hazards of large-scale conveyor belt fires in underground coal mines, as a function of both air velocity and distance from belt surface to gallery roof. The fire hazards considered were smoke obscuration, toxic effects of carbon monoxide (CO), and elevated air temperatures downstream of the fire. All of these hazards scale with the ratio of fire intensity to ventilation airflow. These hazards were all found to be greater at the lower belt-to-roof distance, owing to the greater fire intensities that resulted. The hazards of smoke obscuration and elevated CO levels were greater at lower air velocities. Smoke obscuration was found to be the earliest hazard, reaching critical levels before the stage of belt flame spread. Critical levels of CO and downstream air temperatures were not reached until the later stages of flame spread. Fire growth rates during rapid flame spread were much greater than rates measured during the early stages of belt burning. Data were analyzed to determine the early-warning capability of fire sensors. Smoke sensors provided the earliest warning, followed closely by CO sensors. Thermal sensors did not exhibit any early warning capability.

Jan 1, 2010

By M R. Asef

Although generation of environmentally harmful hydrogen sulfide is considered to be related to sour gas fields, sweet gas reservoirs and waste fluids, travertine springs and geothermal fields may also produce acid gas (H2S and CO2) under certain conditions. The potential parameters influencing such a possibility need to be fully investigated to evaluate the extent of the consequences and predict hydrogen sulfide generation accordingly. Reports on hydrogen sulfide production at different regions and fields were gathered worldwide for the cases when some of them did not have such a problem previously. In order to inspect different aspects of these case studies, some other regions with no hydrogen sulfide content were selected as control. In all cases water samples were taken carefully for chemical analysis in the laboratory. Besides, mineral compositions were characterised in some cases for better evaluation. In order to give a thorough prospect of hydrogen sulfide production, a geochemical model was prepared. In situ engineering geological conditions, especially pressure and temperature, were assigned in the model to investigate the possibility of H2S generation using PHREEQC software. The results of modelling revealed that although many similarities existed between mineral compositions of the cases, certain formations were particularly prone to hydrogen sulfide generation. For better evaluation, important exchangeable cation ratios such as potassium/sodium, calcium/magnesium and ion proportions like sulfate and chloride were calculated as trends of the formations. As expected, the model could successfully monitor a higher ratio of SO42- and Cl- in potential H2S generator formations. Wide variation in percentage of HCO3- was considered as a secondary observatory parameter for better estimation. In addition, it was noticed that higher anion content created an environment ready to absorb any cations and this makes H2S generation easier. Finally, using correlations between predictors and estimators for low depth and deep samples defined the degree of effectiveness for every sample.

Sep 26, 2011

By Fábio Yamada, Ruano Araujo, Marcelo Fugihara, Matheus Sousa Reis

A evolução internacional do mercado de alumínio requer capacidade das empresas de atender uma demanda crescente e para isso se faz necessária uma gestão logística eficiente. O presente trabalho tem como objetivo avaliar o fluxo de veículos em uma fábrica de processamento de alumínio através da simulação dinâmica de processos e tecnologia de modelagem. Com isto, propõe-se avaliar a gestão de recursos (equipamentos e operadores), capacidade de estoques, fluxos internos e movimentações de carga na fábrica; assim, pode-se avaliar a necessidade de novos investimentos nestes quesitos. A análise envolve o cenário atual bem como a demanda futura projetada com o acréscimo de um modal logístico anexo à fábrica, que aumentará o fluxo de produtos na empresa. Em síntese, este artigo relaciona-se com os temas: logística, modelagem matemática de processos e melhorias em produtividade.

Oct 1, 2019

By M. J. Sinnott, W. R. Kiessel

The creep characteristics of commercially pure titanium sheet in the annealed state, cold-worked state, and cold-worked and recovered state in the temperature range from 75' to 750°F have been determined. Titanium has been found to exhibit strain aging characteristics. The effect of strain aging on creep has been determined. A possible explanation for the poor creep properties of titanium is proposed. THE metal titanium exhibits many desirable properties but results on its creep properties have been somewhat disappointing. The creep strength is low even though the material has a very high melting point.' The present work was undertaken to determine the creep strength of titanium in various conditions; annealed, cold-worked, and cold-worked and recovered and to determine why titanium shows such relatively poor creep properties. The general procedure followed in this research consisted in obtaining the usual mechanical prop- erties such as creep strength, short time tensile strengths, and hardness on materials treated to a controlled degree of internal strain, as determined by X-ray diffraction measurements, and their subsequent interpretation in terms of this internal strain. The material used in this work was sheet stock taken from one heat of commercially pure titanium. As-received, this sheet was 0.060 in. thick. The analysis was given as 0.037 pet C, 0.023 pet Si, 0.50 pct W, 0.063 pct Ni, 0.08 pct Fe, and the remainder titanium. The oxygen and nitrogen were unreported but generally are about 0.2 pct in commercial heats. In order to put the material in a state of minimum internal strain all the sheet was given an anneal in a static argon atmosphere for 1 hr at 1600°F prior to processing and testing. The microstructure of the material after this treatment was essentially a single-phase solid solution of uniform equiaxed grains. For the studies on the cold-worked sheet, the material was reduced by rolling in a two high, 5 in. mill. Rolling was done at room temperature in passes

Jan 1, 1954

By Anna Carolina Cerqueira Neves

Muito se tem estudado sobre materiais alternativos, como os compósitos de matriz polimérica reforçados por fibras lignocelulósicas. Isso se justifica pelo fato das fibras naturais terem vantagens no que tange ao meio ambiente, bem como relativo baixo custo. Além disso, a fibra natural apresenta características de interface com a matriz polimérica que favorecem as propriedades mecânicas pela estrutura do compósito. Esse presente trabalho objetiva analisar as propriedades de tração de compósitos de matriz de poliéster reforçados com 10,20 e 30% em fração volumétrica de fibras de cânhamo, que foram preparados alinhando as fibras em moldes e deixando-os curar por 24 horas em temperatura ambiente. Os corpos de prova foram testados numa máquina de ensaios Instron e os resultados mostraram um aumento na tensão máxima de ruptura com o aumento da porcentagem de fibra incorporada.

Aug 17, 2017

The LeadtZinc Concentrator at Mount lsa treats all the lead-zinc-silver ore from the Mount Isa Mine and some of the ore from the Hilton Mine. This concentrator was commissioned in June 1966 and total lead-zinc-silver ore treatment was transferred from the Mount rsa's original No 1 Concentrator in May 1967. Plant capacity is around 5 x 106 t/y.There have been three phases of major plant modifications since commissioning:1. replacement and upgrading of the flotation section in 1979; 2. upgrading of the crushing plant and installation of a heavy medium hydrocyclone plant in 1983 for ore preconcentration, and; 3. doubling ball milling capacity and a further upgrading of the flotation section in 1992.Other developments have included the installation of flotation columns and Jameson cells.The evolution of milling practice since 1955 has been reported by Davey and Slaughter (1970), Bartrum, Dobrowolski and Schache (1977), Fiedler and Munro (1984) and Espinosa-Gomez el al (1989).Lead concentrate is smelted in Mount Isa while zinc concentrate and bulk concentrate (locally called Low Grade Middlings or LGM) are railed to Townsville and shipped to custom electrolytic zinc plants and ISP smelters.

Jan 1, 1993

By Alexandre Keunecke Hardt

Nesse trabalho são abordadas as características de um barramento de serviços de manufatura, um software que promove a integração dos diferentes sistemas presentes no ambiente de TI industrial com o nível corporativo. O cenário atual de crescente competitividade e dinamismo da indústria siderúrgica e de mineração apresenta uma tendência cada vez mais forte de aumento da eficiência operacional. Isso demanda a gestão de ambientes de TI cada vez mais complexos que incluem desde sistemas especialistas a sistemas legados de fusões e aquisições. A integração dessas aplicações com os sistemas corporativos (ERP) resultam em um ambiente com intensas trocas de informações em que a operação se torna dependente do funcionamento sincronizado dessas comunicações. Este trabalho tem como objetivo discutir uma solução de arquitetura de integração manufaturacorporativa por meio de um barramento de serviços e apresentar um estudo de caso.

Aug 16, 2017

By Anna Carolina Cerqueira Neves

Atualmente, materiais alternativos têm sido pesquisados, sendo os compósitos dematriz poliméricas reforçados com fibras naturais um desses tipos de materiais. Ofato que torna as fibras naturais uma ótima opção são suas vantagens ambientais eseu relativo baixo custo. No caso do eu eucalipto, este também possui um altocultivo no Brasil. Além disso, as fibras naturais apresentam características deinterface com a matriz polimérica que favorecem as propriedades mecânicas pelaestrutura do compósito. Esse presente trabalho analisa as propriedades de tração docompósito de matriz poliéster reforçado com a incorporação de fibras de eucaliptoem 10,20 e 30% em fração volumétrica, que foram preparados alinhando as fibrasnas matrizes e curadas por 24 horas em temperatura ambiente, por volta de 25ºC.Os corpos de prova foram testados numa máquina Instron e os resultadosmostraram um aumento na resistência à tração conforme o aumento do volume defibras incorporadas.

Aug 17, 2017

By Enid C. Plante, K. L. Sutherland

Practical metallurgists are unanimous in stating that oxidation of mined sulphide ore adversely affects separation of the constituent minerals under standard conditions in a mill. Frequently, the need for different operating conditions in different plants is attributed either to the extent of oxidation of the mineral surfaces or to soluble oxidation products. The investigations reported in this paper study the effect of oxidation on the primary condition necessary for flotation, namely that of adhesion of an air bubble to the mineral. Oxidation Products from Sulphide Minerals Weinig and Carpenter1 state that the relative rates of oxidation of some sulphides are: FeAsS > FeS2 > CuFeS2 > ZnS > pbS > Cu2S tetrahedrite. They also show that oxidation is rapid at first, that sulphides of older geological formations are more stable than those of recent date and that mixtures oxidize more rapidly than any one mineral alone. The more rapid oxidation of mixtures is borne out by results of Gottschalk and Buehler2 who found that PbS, zns and cus oxidized 8 to 20 times faster when pyrite was present. Only the end products of oxidation, sulphate and the metal ion, were identified in these tests. Gaudin3 states that pyrite is difficult to oxidize in the laboratory. Winchell,4 using pyrite containing 99.98 pct FeS2, allowed water to percolate through a bed of this ground material. At the end of three months only a trace of Fe+++and So4- were found. Even after 10 months the quantity of Fe+++ was only 7.8 mg and SO4- 25.5 mg per liter of percolating solution. Car-michael5 confirmed Winchell's results on the slow oxidation of pyrite. Usually the oxidation of sulphide surfaces has been conducted in neutral or acid solutions, the acidity being caused by the oxidation products. Eliseev and Nagir-nyaka found that treatment of pure pyrite with lime gave only thiosulphate, but considered it possible that thiosulphate was obtained not by oxidation of the pyrite itself, but by oxidation of calcium disul-hide. Mitrofanov7 suggested that thiO~ulphate was formed by the following process: oxidation of sulphide to give free sulphur (this frequently happens with marcasite), followed by oxidation of the sulphur to sulphur dioxide and reaction of the sulphur dioxide with sulphur to give thiosulphate. Ferric and ferrous hydroxides, or similar compounds, were shown to be present. The Research Staff of the United Verde Copper Co.8 treated ore from the United verde mine with lime. Thiosulphate, sulphide and polysulphides were stated to be

Jan 1, 1949

By J. V. Scalera

Because of U.S. dependency on imported critical metals, the Bureau of Mines has conducted research to evaluate the possible substitution of nitrided low-alloy steels for higher chromium-containing alloys. The corrosion data for nitrided steels are limited primarily to the Soviet literature. The objective of this study was to determine the corrosion properties of six commercially nitrided low-alloy steels in a 5-wt % NaCl solution at pH 4. Weight-loss tests indicated that, in deaerated test solutions, most of the nitrided steels were less corrosion resist-ant than nontreated steels. However, electrochemical tests indicated that under more oxidizing conditions, nitrided materials are converted to a passive state with a significantly reduced corrosion rate. Elec-trochemical tests performed in an aerated environment confirmed the passivity of the samples in an oxidizing environment.

Jan 1, 1984

By C. Samuelsson, G. Carlsson

Characterization of dust from Boliden Mineral AB’s copper-plant in Sweden was carried out using chemical analysis, X-ray diffraction analysis, energy dispersive analysis and wave length analysis using electron microprobe equipment. Dust from four different locations was characterized: the electrostatic precipitator (ESP) after the roasting furnace; the ESP after the copper smelting furnace; from the copper converter ventilation bag house filter; and from the bag house filter collecting dust from the settling furnace and tap gas ventilation. The results showed that the dust is composed of small solid and/or liquid particles from the furnace reactor which have been transported with the process gas to the dust collecting devices. This portion of the dust is mechanically formed. It also contains compounds that have been vaporized in the process and then condensed from the process gas at lower temperature, chemically formed dust. The proportion of mechanical and chemical dust varies with the process generating the dust.

Jan 1, 2001

By Daniel Adolfsson, Ryan Robinson, Fenwei Su, Jelena Blagojevic

"Cold bonded briquetting of steel plant by-products has proven to be a viable recycling alternative concerning technology, economy and environment in both the traditional blast furnace route and the direct reduction process. A critical parameter in cold bonded briquettes is the type and amount of binder used during production. The binder material must meet certain quality requirements concerning low and high temperature strength, chemistry and economy. Currently, SSAB Tunnplåt uses ordinary Portland cement (OPC) as binder in their cold bonded briquettes. In order to improve binder quality and possibly decrease OPC dependency, a binder feasibility study has been conducted concerning an internal by-product, ladle slag, as a supplement and/or partial substitute for OPC. Several characterization techniques have been used to study the behaviour of ladle slag, these include: XRD, XRF, SEM, glass content analysis, calorimetric analysis, particle size distribution and thermochemical stability considerations concerning the CaO-Al2O3-SiO2 system.IntroductionRecently, a project was initiated at SSAB Tunnplåt AB, in Sweden, which aimed at reducing the amount of ordinary Portland cement (OPC) as hydraulic binder in cold bonded briquettes by partly replacing it with ladle slag. OPC is traditionally used within civil engineering, and widely accepted as a hydraulic binder in a number of different applications. OPC consists of four major crystalline phases, i.e. C3S, C2S, C3A and C4AF. Tricalcium aluminate as well as the ferrite phase in OPC reacts very quickly with water, for this reason gypsum is added to the clinker in order to retard these reactions. The fact that gypsum is present in the system limits the recycling of briquettes to the BOF, since the presence of gypsum during steelmaking results in a significant amount of sulphur emissions. The latter along with the expense that follows, makes it worthwhile to consider alternatives for OPC as binder in cold bonded briquettes."

Jan 1, 2008

By Terence M. Gordon, Mati Raudsepp, Gregory M. Dipple

Four methods of measuring mineral abundance in a rock are examined for their potential in assaying for high-tech industrial minerals. One method uses X-ray powder-diffraction data and the other three rely on whole rock chemical data and information on mineral assemblages and mineral compositions. All four methods were employed to estimate wollastonite content in diamond drill core of skarn collected as part of an exploration program and are compared to visual estimates of wollastonite content from core logs. These techniques for assaying wollastonite span a considerable range ofaccuracy and expense, and combined, define a non-linear relationship between these variables. Accuracy increases rapidly relative lo expense up to total costs of about $50 per analysis. Assay methods in the $50-100 per analysis range have associated errors of 5-10% relative and probably suffice for most exploration programs. Improvements in accuracy above this level require a much larger investment. The most expensive assay technique (-$300 per analysis) yields the most accurate measurement of grade (relative error -1%). Its application may best be limited to periodic checks on other assay techniques and for fine-tuning ofmineral separation procedures.

Jan 1, 2001