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By Miguel Becerra, Daniel Jordán, Jorge Soto, Luis Torres

"Most SAG grinding operations currently use ball sizes between 5.5 and 6 inch maximum size. However, in most cases the use of this ball sizes hasn’t been justified by a phenomenological analysis of the real effect on the grinding process, but rather by trial and error. The analysis of the influence of ball sizes in SAG grinding hasn’t been developed in detail by considering the effect on process parameters inside the mill, grinding efficiency or internal classification. Historically a conventional grinding reference has been made on the empirical procedure developed by Azzaroni (1980). Further to Azzaroni’s methodology, Sepulveda (Sepúlveda, 2007) developed the SPEC methodology, incorporating the ball size effect on the grinding efficiency parameters using a population balance model included on Molycop tools spreadsheets.This paper demonstrates a detailed analysis at pilot scale of the ball size employed in SAG grinding and scaling that exists between the different levels. This analysis includes assessing the effect of balls sizes on parameters associated with grinding efficiency and its effect on the total fill level, product size distribution and specific energy consumption, among others. In a complementary way it develops a technical - economical evaluation from industrial data comparing two different ball sizes and its effect on the grinding process analysed integrally."

Jan 1, 2014

By Robert Hochscheid

A patent issued to J.N.J. Leeman (1957) described the change in performance that takes place when a cyclone is installed in the horizontal position rather than the vertical position. Although this patent was directed more toward improvements that could be realized in the heavy medium cleaning of coal, it contained specific references to reducing the quantity of fine solids that would report in the underflow, and an example for fine sand classification is also included. The three cyclone installations for which data is given in this paper demonstrate that horizontal mounting of large cyclones can improve classification efficiency, eliminate some operational difficulties, and reduce cyclone maintenance requirements in closed circuit grinding installations. Cyclone Experience at Serrana S.A. Each of four grinding circuits at the Serrana S.A. de Mineracao Apatite flotation plant in Brazil have a 2.7 X 4.6 meter (9 X 15 foot) rod mill and each originally operated in closed circuit with two vertically mounted Model D20B (500m nominal diameter) Krebs Cyclones. New feed size is 25mm. The Apatite is liberated at a relatively coarse 35 to 28 mesh grind, but the 500mm cyclones had to be fed at 66 pct. solids in order to obtain an overflow analyzing 12 pct. coarser than 42 mesh. Because dilution water in the cyclone feed had to be limited, classification was inefficient, and there were other significant circuit difficulties as summarized in a recent article by C. A. Busnardo (1984):

Jan 1, 1985

Sherwood?s Minto Project ? High grade copper copper-gold deposit ? Yukon Territory, Canada ? Development underway ? Permitted ? Production by mid mid-2007 ? 40 40-50m lbs Cu plus Au/Ag by by-products ? Parallel exploration program underway ?Discover more high grade resources ?But what kind of deposit is it?

May 1, 2006

By J. D. McKay

The Bureau of Mines devised a column flotation technique using either fine or coarse bubbles and compared it with conventional flotation on a Montana chromite ore. On deslimed ore, fine-bubble column flotation produced a 44.7-pct-Cr203-grade rougher concentrate with 87-pct recovery, compared with 43.8- and 43.5-pct-Cr203-grade rougher concentrates with 85- and 77-pct recovery for coarse-bubble column flotation and conventional flotation, respectively. On undeslimed ore, coarse-and fine-bubble column flotation produced rougher concentrates containing approximately 41.5-pct-Cr203 with 95-pct recovery, exceeding conventional flotation which produced 35.6-pct-Cr203-grade concentrates with 87-pct recovery.

Jan 1, 1985

By F. E. Steigert, A. H. Geisler

THE permanent magnet alloy comol, which contains 17 pct Mo, 12 pct Co, balance Fe, exhibits a precipitation reaction analogous to that at the iron end of the binary Fe-Mo system. The equilibrium precipitate, (P,), has a structure isomorphous with Fe,Mo, which is rhombohedra1 with parameters a = 8.97A and a = 3038.6&apos; according to the work of Arnfelt and Westgren.&apos; In the ternary alloy the parameters are a = 8.87A and a = 31°0.5&apos;. Oscillating crystal patterns of a single matrix crystal, M, in which P, was precipitated by slow cooling from 1300°C, showed that the orientation relationship of the two lattices is as follows: (110)P3 // (110)* (111)p3 // (110)m There are crystallites of P, in 12 different orientations in a single crystal of the parent solid solution. Microscopic examination shows that the crystallites are generally plate-like with their lateral dimensions parallel to (110) matrix planes. When precipitation in a supersaturated alloy quenched from 1300°C progressed isothermally at temperatures between 600" to 800°C, the evolution of the P, structure could be traced. Diffuse diffraction effects in Laue patterns provided early evidence of the precipitation process. Analyses of these by a previously described technique2 showed that they corresponded to rod-like elements parallel to <110> matrix directions in reciprocal space. With further aging to promote growth of the precipitate, the rod-like elements contracted to points in reciprocal space for normal Bragg reflection from the precipitate as shown by the left diagram in Fig. 1. Thus the diffuse scattering was attributed to the small thickness of the plate-like particles which was inadequate for sharp diffraction. When the precipitate particles were first thick enough to give normal diffraction their structure was different from that of the equilibrium precipitate, P,. The first structure, P1, presumably is a coherent transition struc-

Jan 1, 1952

By S. J. Rothman, L. T. Lloyd

S. J. Rothman and L. T. Lloyd (Argonne National Laboratory)— Hagel&apos;s paperz0 discusses the question of the mechanism for self-diffusion in bcc transition metals. Recent work21"23 has led us to agree with him in reabandoning the ring mechanism in favor of a defect mechanism, most likely vacancies. On the other hand, we think that Hagel&apos;s attempt to group together all self-diffusion in bcc transition metals is wrong. We prefer the scheme of Peart, Graham, and omlin," who separate them into two groups. One group contains the anomalously behaved metals P titanium,&apos;, y uranium, and perhaps zirconim.&apos; The other group contains a iron," this alloy was held at 1800°C for 2 hr before quenching, its structure was all a. B. C. Giessen, I. Rump, and N. J. Grant (Authors&apos; reply)—We very much appreciate the discussion by Deardorff and Kato regarding the a to /3 transformation temperature of hafnium. In the W-Hf program, as well as in a current study of the system Cr-Hf, standard precautions were exercised against contamination, including vacua of less than 10"5 mm Hg and a weight control check of all specimens to insure an impurity rise of less than 100 ppm. Following receipt of the above discussion, a revision was made in the annealing process. Arc-cast specimens were etched with a 10 pct HF-90 pct HNO solution until 1 mm of surface, including a possible oxide film, was removed. Annealing was done in a hafnium container which provided a long diffusion path for gaseous contaminants. Finally, the heat treating time was shortened. Structural changes were noted to occur quite slowly. A 99.5 at. pct Hf alloy showed 70 pct /3 after 30 min at 1700°C and was 100 pct /3 after 10 min at 1715°C. After 24 hr at 1740C, the alloy was found to be 10 pct/3. This change is due to contamination; it was estimated that it corresponds to an increase of 60°C in the transformation temperature over a 24 hr period. The corresponding change in 30 rnin would be slight. Using the same hafnium as in the above publication, and three new alloys at 98, 99, and 99.5 at. pct Hf, the transformation temperature was indicated to be 1715" 15°C. Since this hafnium contained 4.4 at. pct Zr, a correction of 40 5C, based on an assumed approximately linear transformation temperature curve, must be made for pure hafnium. This yields a value of 1755 20°C in good agreement with Deardorff and Kato&apos;s value. Because the slope of the boundary is small, this permits a good extrapolation, and we regard the W-Hf alloys as well suited to check the Hf transformation temperature. niobirn,&apos;&apos; and molybdenum,22 whose activation energies correlate with the melting temperature and whose Do values follow Zener&apos;s predictions.28 We have no quarrel with Hagel&apos;s placing chromium into the second group; we disagree with his interpreting our data to make uranium fit into that group. Hagel considers that the measurements of self-diffusion in uranium below about 950°C represent combined volume and grain boundary diffusion. This contention is based on the curvature of the penetration plot for our 891°C run,4 which also has a nearly straight line plot of log c vs x. Hagel has extrapolated these characteristics to our 803.5C run and fitted his Arrhenius plot for self-diffusion in y uranium to our four highest temperature points only. We think this is wrong for the following reasons.

Jan 1, 1963

By J. Budac, J. Dennett, D. Mayne, P. Nawrocki

"The Nickel/Cobalt operation in Fort Saskatchewan, Alberta has successfully used an oxidative ammonia leach process to refine a variety of feeds into high quality nickel and cobalt products for over 60 years. Fundamental changes to the refining process were made when the major feed was converted from nickel concentrate to cobalt rich mixed sulphides in the early 1990s. Since the early 1990s, the production capacity of the refinery has expanded to match increases in both mixed sulphides and other feeds. In addition to increasing the production capacity of the refinery, other changes have been required in order to improve the operability and reliability of the refinery as well as to deal with increasingly stringent safety and environmental requirements. This paper describes recent changes at the refinery including changes to the flow sheet, improvements in unit operations, incorporation of new feeds, management of byproducts, and control of impurities.INTRODUCTION The Cobalt Refinery Company (Corefco) plant in Fort Saskatchewan processes nickel-cobalt mixed sulphide intermediate produced at the lateritic nickel mine and high-pressure acid leach (HPAL) facility in Moa Bay, Cuba. Both operations are jointly owned and operated by Sherritt International and General Niquel of Cuba. The mixed sulphide, along with other feed materials, is processed at the Fort Saskatchewan refinery using a pressure ammonia leach-hydrogen reduction process to produce nickel and cobalt metal. This refinery was originally constructed in 1954 to treat nickel concentrate from Sherritt’s Lynn Lake mine in Manitoba. (Benson and Colvin, 1964; Boldt and Queneau, 1967; Forward, 1953; Forward and Mackiw, 1955; Kerfoot, 1989) From the mid-1970s until the early-1990s, the facility operated as an independent refinery, treating nickel-bearing feeds from around the world. The flowsheet was changed in 1992 to address the increased cobalt content of the feed. (Cordingley and Krentz, 2005; Kerfoot and Cordingley, 1997) The flowsheet was adapted further in 2009 to improve cobalt speciation in the leach process, which allows better cobalt-nickel separation. The 2009 iteration is shown in Figure 1. Three ammonia leach stages were used to ensure high recoveries of nickel and cobalt. Underflow solids from the final leach stage contained mainly iron oxides. One of the features of the leach process is the innovative recycling of ammonia. Ammonia vented from the leach process in tail gas and from atmospheric tanks is recovered and recycled into the refinery using water based scrubbers and a high pressure distillation process. Indeed, roughly 250 t NH3/d is recovered as distillate and recycled back into the process. Also, air enriched with ammonia which is vented from the later first stage autoclaves is recycled to the lead first stage autoclaves to maximize oxygen and ammonia utilization."

Jan 1, 2017

By J. S. C. Joubert

The Koidu Kimberlite Project is situated in the Kono District of Sierra Leone, approximately 330 km east of the capital city, Freetown. The mining lease area is 4 km2 and comprises 2 kimberlite pipes, 4 dyke zones and a number of blows off the dykes. Koidu Holdings established on the property and began dewatering and the removal of silt from the existing 30 m excavation of the No.1 Pipe in 2003. While the original planning for the pipes included conventional open pit operations, mitigating factors such as the proximity of the town, the presence of houses close to the perimeter of the pipe, the size of the pipe and the planned open pit depth with relevant stripping ratios, as well as uncertainties on the grades in respect of an underground operation, lent itself to the vertical pit concept. The vertical pit was established using an A-frame headgear for the hoisting arrangement, with sidewall support comprising a combination of 20 m and 40 m long cable anchors, rock bolts, wire mesh and pneumatically applied concrete. The pit reached steady state production in January 2007 and produced some 26,000 tonnes of head feed per month until August 2007 when mining reached a depth of 74 m below the pit collar (approximately 126 m below surface). Mining was suspended following a sidewall failure that disrupted operations. Now that the grades in No.1 Pipe have been validated, focus has been switched to an underground operation taking account of both No. 1 Pipe and No. 2 Pipe. While the mining costs for the vertical pit have been higher than for a conventional open pit, the concept did circumvent the social implications, the issue of grade consistency and diamond value at depth, as well as providing the time frame to carry out a full underground mining study.

Jan 1, 2008

By Alfredo Menendez, Alberto Sarmentero

A B S T R A C T The Los Pijiguaos bauxite is one of the largest accumulations of trihydrate alumina ore recently discovered; it is a plateau type, with no overburden, relatively soft tertiary quartz-bearing bauxite developed on a pre-Cambrian Rapakivi Granite batholith. The deposits are found in the northwestern rim of the Guiana Shield, State of Bolivar, Venezuela, and were discovered in 1976 after a grass-roots exploration campaign. Target areas were mainly selected on the basis of geological and geo¬morpholigcal criteria, guided by correlation with known deposits elsewhere in the Guiana Shield. The vertical. lateritic profile consists of an upper concretionary zone, followed by a mottled zone, a palid zone and finally the weathered rock merging into fresh granite. The upper concretionary zone displays a cellular, pisolitic or spongy texture and contains the following minerals: gibbsite (60-90%),quartz (5-10%), hematite (5-10%), goethite (under 5%), boehmite (traces), kaolinite (traces). The gibbsite content decreases sharply downward from the lower limit of the concretionary zone and the kaolinite and quartz content increases in the underlying mottled zone. The mottled and palid zones display a pseudo rapakivi texture and quartz, kaolinite and mica are the. essential minerals.

Jan 1, 1984

Safety bulletins and stickers issued for the paste backfill plant at Cannington read as follows: æCannington Paste Fill Plant, First of ItÆs Kind in AustraliaÆ. We could even dare to state that the Cannington plant is different than any other paste backfill plant in the world because of the overall design, plant equipment and underground delivery. However, one thing to be certain of is, the paste backfill plant works as designed and a pump is not required to deliver paste underground given the general plant arrangement at Cannington. The past two years have been a process of evolution to design and construct the plant and make it work. This paper will describe the paste process using full mill tails along with placement of cemented paste underground. Discussions will include rationale of fixed plant selection along with various control requirements. BHP World Minerals recently commissioned its paste backfill plant in December 1997. Cannington is placing full mill tails underground via two surface boreholes that deliver either to primary or secondary stopes.

Jan 1, 1998

By AIME AIME

AWRDED jointly by the four AW Founder Engineering Societies the John Fritz Medal is generally regarded as the most signal honor that American engineers can confer on a fellow engineer. The roll of 34 recipients contains the names of Lord Kelvin, George Westinghouse, Alexander Graham Bell, Thomas. A. Edison, George W. Goethals, Guglielmo Marconi, and Michael I. Pupin; and among members of the A.I.M.E. now living, Sir Robert A. Hadfield, Herbert Hoover, and Daniel C. Jackling. On the evening of March 1 7 the name of Paul Dyer Merica was formally added to this list of illustrious engineers when the medal was presented to him at a dinner at the Metropolitan Club in New York. The citation read. For important contributions to the development of alloys for industrial uses. Arrangements for the dinner were made by the following committee representing the four Founder Societies: R. C. Allen, George S. Davison, A. A. Potter, and J. B. Whitehead.

Jan 1, 1938

By Cintia Braga

O processo de retificação é empregado na fabricação de componentes que requerem excelente qualidade dimensional com elevado acabamento superficial. O desempenho deste processo depende muito das condições de lubri-refrigeração produzidas pelos fluidos de corte, que são utilizados para amenizar os problemas que afetam a integridade superficial das peças, como queima e danos microestruturais, e também proporcionar melhor desempenho do processo e aumento da vida útil do rebolo. Entretanto, os fluidos de corte são uma das fontes mais problemáticas na manufatura, pois são produtos nocivos ao meio ambiente e a saúde humana, e aparecem como elemento determinante para a otimização do processo de fabricação. Desta maneira, este projeto visa analisar o comportamento do fluido de corte integral comercial em comparação com formulações biodegradáveis (óleos de soja e milho) no processo de retificação cilíndrica externa de mergulho no aço ABNT 4340 temperado e revenido com dureza média de 52 HRc. A avaliação do desempenho dos fluidos consistiu na análise da integridade superficial (rugosidade, microestrutura e microdureza) e no desgaste do rebolo. Os resultados comprovaram a eficiência dos óleos vegetais e viabilidade do uso no processo de retificação, proporcionando melhoria na eficiência do processo e contribuindo para uma manufatura ecologicamente correta.

Aug 7, 2018

By Juliana Porto Guimarães

A crescente demanda por aços galvanizados com alta lubricidade tem impulsionado o desenvolvimento de pós-tratamentos que, aplicados sobre a superfície dos revestimentos, reduzem o atrito entre o ferramental e a chapa durante o processo de estampagem de peças críticas na indústria automotiva. Diante disso, a Usiminas desenvolveu, em parceria com a Quaker, a aplicação do pós-tratamento tipo microfosfato denominado Primecoat Z Auto, com a função de melhorar a estampabilidade de aços galvanizados a quente do tipo GI (Zn puro). Nesse estudo foi avaliada a Razão Limite de Estampagem (RLE) de um aço GI destinado a produção de peças críticas, após aplicação desse pós-tratamento em escala de laboratório. Adicionalmente, foram caracterizadas a morfologia e a constituição química do microfosfato, e o desempenho do aço quanto à fosfatização, à pintura automotiva e à resistência a corrosão. Concluiu-se que o filme de pós-tratamento é amorfo, constituído por Zn, P, Al e Mg, promovendo um excelente ganho de lubricidade ao aço GI, sem interferir nos processos subsequentes de fosfatização e de pintura nas montadoras. Além disso, o material apresentou excelente desempenho quanto à resistência à corrosão.

Jul 30, 2018

By Leandro Brunholi Ramos

O aço API 5 CT P110 é amplamente utilizado no setor de petróleo e gás no Brasil devido sua elevada resistência mecânica, contudo ele não possui uma boa resistência a corrosão. Com a descoberta do pré-sal, novos desafios surgem neste setor, tornando necessário o desenvolvimento de novas tecnologias resistentes aos ambientes agressivos que os materiais serão expostos. A aspersão térmica por HVOF se destaca pela obtenção de revestimentos contra corrosão e resistentes ao desgaste com baixa porosidade e com um relativo baixo custo em comparação a outros processos. Dentre os materiais que podem ser aplicados como revestimentos por aspersão térmica, o níquel se destaca pela ótima resistência à corrosão por formar um óxido protetor na superfície. Sendo assim, o presente trabalho tem por objetivo obter e caracterizar revestimentos de níquel obtidos por aspersão térmica HVOF, no aço API 5CT P110. Os revestimentos foram caracterizados morfologicamente por microscopia eletrônica de varredura (MEV). Foram obtidas curvas de polarização para avaliar o comportamento frente à corrosão e foram realizados ensaios para determinação do coeficiente de atrito. A camada aspergida de níquel apresentou resultados satisfatórios quanto às análises estudadas.

Aug 8, 2018

By M. McPherson, G. Danko

Methods of measuring in situ rock thermo-physical properties are rapidly evolving. Among those existing in the literature, a particular measurement procedure was selected for further development. The measurement is based on creating a spherical temperature field in a drill hole using a point source heater of constant heat flux. The bivariate temperature distribution 0 (r, t) is measured at several points along the length of the drillhole, radius r from the heater and at particular time intervals (t). A number of different evaluation methods were tested for calculating the unknown thermal conductivity (k) and diffusivity [] from the measured temperature and the known heat flux. The results showed that evaluation using the finite difference scheme and small temperature differences measured at points close together, cannot give a reasonable result. In order to solve the problem a new general analytical evaluation method is developed. Using an appropriate technique, it is possible to simultaneously obtain values for k and [], incorporating a semi least square technique to reduce the uncertainty in the evaluation. The new device and evaluation method makes it possible to obtain from a single drill hole highly precise k and [] values within an 8 hour period. The method has been used in several underground mines in the U.S. with good results.

Jan 1, 1987

By Anderson Azevedo Agra

A geração de resíduos siderúrgicos é um problema que abrange dois cenários: o ambiental, no que diz respeito ao descarte de resíduos no meio ambiente e também tange o econômico, pois trata-se de material não reaproveitado que deve ser destinado a aterros industriais, gerando custos. Tendo isto em vista, a reciclagem desses possíveis coprodutos para a reutilização como matéria-prima do processo torna-se uma alternativa pertinente. Uma das formas de recuperação do pó de aciaria elétrica (PAE), resíduo abordado neste trabalho, é através da pelotização. Para o reaproveitamento de metais de interesse do pó foi utilizado um agente redutor, o coque de petróleo. No entanto, para formação das pelotas um aglomerante se faz necessário. Este, em associação com as partículas do óxido, tem como objetivo conferir resistência mecânica adequada às solicitações que o processo de fabricação do aço exige. Neste trabalho, são feitas considerações acerca do uso de seis composições diferentes de aglomerantes com o objetivo de avaliar o desempenho destes, através de ensaios de resistência a compressão, testes de queda e tamboramento. Como resultado, pode-se verificar o melhor desempenho da combinação da cal com cinza de casca de arroz.

Aug 16, 2017

By Aline Silva Magalhães

Os aços com médio teor manganês são uma classe da terceira geração de aços avançados de alta resistência (AHSS), combinam propriedades mecânicas como ductilidade e resistência mecânica e são assistidos pelo efeito TRIP, características determinantes para sua aplicação na indústria automobilística. Convencionalmente, tais ligas são produzidas por meio de laminação a quente e a frio, seguidas de recozimento intercrítico. No entanto, o trabalho a morno têm ganhado interesse com o intuito de reduzir custos e tempo operacionais. O objetivo deste trabalho foi comparar a influência da laminação a quente e a morno por meio de análises de microscopia óptica, eletrônica de varredura, difração de raios x, microdureza Vickers e técnicas de EBSD em um aço 8Mn- 0,08C. Observou-se uma microestrutura mais refinada e deformada no material laminado a morno com um maior percentual de austenita retida, o que derivou uma menor dureza. Na amostra laminada a quente, o valor médio de dureza evidenciou uma microestrutura martensítica de baixo teor de carbono. Em relação à textura verificou-se uma maior intensidade de componentes da fibra a na amostra laminada a morno devido a um maior grau de encruamento neste processamento termomecânico.

Aug 17, 2017

By Klaus-Peter Kinzel

Staves Coolers de cobre proporcionaram uma excelente proteção da carcaça do alto-forno em áreas de alta temperatura. Isso resultou para que os operadores de alto-forno alcançassem alto desempenho em termos de produtividade e taxa de combustível, além de campanhas de mais de 15 anos. No entanto, nos últimos anos, alguns altos-fornos experimentaram um desgaste prematuro nos staves de cobre. Algumas dessas empresas se alinharam com Paul Wurth para investigar a causa fundamental desse fenômeno com base em todos os fatores de influência e, em seguida, propor ações corretivas. Estes resultados são discutidos e apresentados a seguir no trabalho técnico.

Oct 30, 2017

By Tiago Ribeiro Costa

A otimização da matriz energética na produção de metais tem sido um dos tópicos predominantes mundialmente. Um dos principais consumidores ineficientes de energia, em alguns casos impactando inclusive no consumo de fornos elétricos são os sistemas de aquecimento de panelas. Buscando novas alternativas de redução de custos de energia, e redução de emissões, a White Martins encontrou uma alternativa técnica aos convencionais Pré-Aquecedores de panelas ar-gás. É o Sistema de Aquecimento de Panelas Oxicombustão com queimador Optifire, que utiliza oxigênio puro como comburente ou ar enriquecido. Comparado ao sistema ar-gás convencional, é possível promover uma economia de combustível de até 50% e redução de emissões de carbono e NOx. A tecnologia do equipamento consiste em realizar a queima estequiométrica balanceada, através da medição precisa dos gases, utilizando queimadores avançados com maior eficiência e melhorando a distribuição de calor, de forma a não gerar diferenças de temperatura entre seções. Com a tecnologia Optifire é possível inclusive o remanejamento de combustível mais nobre, como gás de coqueria em processos como aquecimento de regeneradores de altos-fornos. Este trabalho descreverá o estudo da oportunidade e dimensionamento para aquecedores de panela.

Oct 30, 2017

By Lucas Kling e Silva

A deformação plástica de aços acompanha mudanças irreversíveis da microestrutura, que podem ser consideradas como o estágio inicial do processo de fratura. No entanto, detectar, monitorar e avaliar previamente, estados de dano e pequenos defeitos, de forma não destrutiva, ainda se mostra desafiador. Foi reportado na literatura o fenômeno do surgimento espontâneo de fracos campos magnéticos em aços estruturais e em oleodutos, que são originados devido a tensões mecânicas heterogêneas ou térmicas. Esta observação não é associada com transformações de fase induzidas por deformação e parece ser uma ferramenta promissora para a caracterização prévia de danos em aços ferromagnéticos. Para proporcionar uma melhor compreensão das bases físicas deste processo, foram observadas as microestruturas magnéticas de tais materiais e as mudanças ocorridas nos domínios magnéticos dos mesmos após sofrerem deformação plástica. Para isto foi utilizado um meio de solução coloidal com partículas superparamagnéticas na escala nanométrica (ferrofluido) que proporcionou, através da técnica Bitter, observar não apenas uma mudança de tamanho dos domínios magnéticos do material, mas também modificações em sua morfologia. Foram estudados neste trabalho aços ferríticos com as respectivas concentrações de carbono em sua composição: 0.08%; 0.22% e 0.45%.

Oct 30, 2017