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By Stephen A. Hare, O&apos

The melting, casting, and welding of the Raney nickel alloy (42 pct Ni-58 pct A1), a methanation catalyst useful in coal gasification, were investigated. Melting was done in graphite crucibles by heating aluminum and adding nickel using a cryolite slag cover. Casting conditions were found to be optimum when the melt temperature ranged from 1,125° to 1,200° C and the mold temperature ranged from ambient to 250° C. Suitable mold materials were found to be quartz, heat-resistant glassware, olivine, and zircon. Welding of the alloy can be accomplished using tungsten inert gas process. Tensile strength of the alloy, in the as-cast condition, was found to be 2,000 1b/sq in with an impact strength of less than 1 ft-1b. The coefficient of thermal expansion was determined to be 18.4 x 10-6/° C after heat treatment.

Jan 1, 1977

By Oliver Bowles

[In an endeavor to promote greater efficiency in the lime industry, the United States Bureau of Mines is preparing a series of preliminary reports dealing with particular problems of the industry. Through the circulation of these reports, it is hoped that sufficient interest may develop among lime-plant operators to prompt them to discuss with the bureau their our experiences with these problems. By such an interchange of ideas, it is believed that conclusion may be reached which will be of practical benefit to try entire industry. The first report, "Stripping problems it Limestone quarries of the Shenondoah Valley", Serial No. 2401, was issued during October, 1922. This report t is the second of the series. It is hoped that may operators will contribute additions to the information now at hand.]

Jan 1, 1922

By Jürgen F. Brune, William H. Schiffbauer

Communication problems are not new. Research in this area goes back as far as 7922 when the US Bureau of Mines performed experiments to detect radio signals from inside their experimental mine in Bruceton, Pennsylvania. Many improvements to mine communications have been made over the years but for any number of reasons the underground coal mining industry has been behind in implementing advances. Present communications systems far underground mines can be hard-wired or wireless. Both types of systems can fail when faced with fires, roof falls, explosions, and power or battery failure. Currently installed wireless communications systems usually employ a special antenna cable called a "leaky feeder" Fiber optic cables are also used in some applications to form a "backbone" for wireless transceivers. Through-the-earth (TTE) and wireless radio systems are less common. Except for TTE systems, most wireless systems require some wire-bound components, which are susceptible to failure during disasters as cable breakage interrupts communications.

By J. Grumer

Nine dust and gaseous inhibitors of propagating coal dust-air flames (lean, stoichiometric, and rich) were evaluated in a newly developed 15-cm-id, 3.6-meter-long instrumented flame duct, under conditions such that wall quenching was virtually absent and the dust concentration was temporally and spacially uniform to within about t5 percent. Listed roughly in order of increasing efficiency, the inhibitors evaluated were rock dust (calcium carbonate), powdered oyster shells (calcium carbonate), Halon 1301 (trifluorobromomethane), Halon 1211 (difluorochlorobromomethane), sodium chloride, Super-K (potassium chloride), regular-grade fire extinguishant powder (sodium bicarbonate), Purple-K (potassium bicarbonate), and Monnex (potassium bicarbonate combined with urea). Experiments were extended to clouds containing 1 and 2 volume-percent of methane. The inhibition of lean, stoichiometric, and rich methane-air flames without coal dust was also examined in a few instances; results agreed with those obtained for coal dust-air flames.

Jan 1, 1971

By I. A. Jacobson

In a closely controlled laboratory retorting system for oil shale, a relationship was developed by the Bureau of Mines between the temperature in the retort and the weight ratio of ethylene to ethane in the gases produced. Reciprocal temperature was shown to be directly proportional to the log ([ethylene]/[ethane]). From this relationship a number, called retorting index, was developed. The retorting index has the dimension of temperature, but its magnitude depends on both temperature and residence time for the reactants in the heated zone in the oil-shale retort. The slopes of the lines relating reciprocal temperature and the logarithm of the ethylene-ethane ratios are nearly constant for each of the retorting processes for which data have been presented. The retorting index should be a valuable tool to control the operation of oil-shale retorts, either aboveground or in situ. If an optimum operating condition can be established, the maintenance of the optimum or the departure from it should be easily monitored by use of the index.

Jan 1, 1974

By R. C. Gabler

Laboratory tests on a combined nitrogen roast--two-stage leach--electro-winning approach show promise as a possible process for recovering copper, sulfur, iron oxide, and valuable minor metals (gold, silver, and molybdenum) with a minimum impact on the environment. During the nitrogen roast at 800° C, 15 to 20 percent of the sulfur together with a significant fraction of the volatile elements, such as arsenic, bismuth, lead, and zinc, are removed from the chalcopyrite concentrate. The resulting calcine, consisting of 8-chalcopyrite, troilite, and a bornitelike structure, is leached with hydro-chloric acid to remove 70 to 85 percent of the iron. The digenite in the leach residue is dissolved in an oxygen-saturated, spent sulfate electrolyte. Using a graphite 'anode plus sulfur dioxide to reduce interference from ferric iron, copper of 99.99+ purity is electrowon at current efficiencies of 88 to 92 percent and a cell voltage of 0.4 to 0.5 volt. Copper recovery for the overall process is 98 to 99 percent. Sulfur is obtained in the elemental form from the roasting and leaching steps. Iron can be recovered from the hydro-chloric acid leach solution. Gold, silver, and molybdenum are concentrated in the silica residue from the spent electrolyte leach.

Jan 1, 1975

By S. H. Ash

"INTRODUCTION Mine fires have occurred since underground mining of minerals began, and they are still occurring. The technical literature is replete with papers relating to mine fires.Means and methods for controlling and extinguishing mine fires and preventing explosions and other accidents require the collection and analyses of samples of the atmospheres surrounding the fire. Such atmos¬pheres are complex mixtures of gases (1, 3, 4, 15, 21, 23).3/SUMMARYExperiences at mine fires (1, 3, 4, 15, 21, 23) have proved conclusively that mine-air analyses furnish the only means of judging what is going on in a mine fire area. Mine-air analyses give evidence of conditions that require immediate protection, govern the order and control the manner in which a fire is fought, show the necessity of bulkheads and establish the places to construct them, indicate whether or not a fire is being controlled or is being extinguished, and govern procedure in sealing and unsealing mine fires.It is commonly believed that danger to life and property from mine-fire atmospheres is greatest in coal mines; this is true only to the degree that the explosion hazard is greater in coal mines than in noncoal mines because of the presence of combustible gases. The problem of gas poisoning is greater in noncoal mines because of the more frequent occurrence of poisonous and innocuous gases, oftentimes the lack of controlled ventilation, and usually greater difficulties in sealing mine-fire areas. Sulfide minerals present a serious hazard in many metal-mine fires when sulfur dioxide is formed. The country rock or ore body itself may contain or be limestone, which may be calcined. Emanations of carbon dioxide are found."

Dec 1, 1950

By Fun-Den Wang

A two-dimensional plane strain analysis by the stiffness matrix method was used to analyze two basic pit slope configurations. The magnitudes and the directions of stresses are given for a V-shape and for a flat-bottom pit with the slope angle varying from 30° to 90° at 10° intervals, Stress effects due to irregular pit configuration or to in-situ forces are discussed. Equations of similitude for gravity loading are given. Expressions are also given for the stresses at the toe as a function of slope angle. Procedures are given for finding the stresses in any geometrically similar pit slope of different dimensions and material properties from the stresses and equations presented in this report. Numerical results show that the V-shape pit slopes have lower stresses than the flat-bottom pit slopes; hence, they are inferred to be more stable.

Jan 1, 1970

By David A. Monaghan, Kenneth R. Maser, Adi R. Gurdar, D. Randolph Berry

9. Remote Sealing System Sensitivity 9. 1 Introduction In the previous sections a description of the overall system has been presented along with detailed descriptions of the equipment and techniques employed with the preliminary probing system, the seal em¬placement system and the seal checking system. In addition, the use of these subsystems in a specific mine application has been described in considerable detail. A broad range of parameters of interest was specified in the contract, as summarized in Section 1. 3. Most of these are a function of the general location; i. e. , the location of the mine, and the specific location; i. e. , the location of the boreholes. These parameters of interest include passage size, shape, depth, slope and water con¬ditions. The length, diameter and location of the boreholes within the mine passage and on the surface are critical parameters as well. A few additional parameters may affect one or more of the remote sealing subsystems. These include temperature, topography, rock and soil conditions, and underground water. While variation in these parameters will not render the system inoperative, consideration of them in the planning stages will simplify and expedite the field operation. In the following sections the effect of the various parameters on the remote sealing operation will be discussed. For clarity, the several tasks, borehole drilling and casing, preliminary probing, fly ash delivery, foam topping and seal checking, will each be considered separately.

Jan 1, 1973

By Thomas P. Mucho, William D. Monaghan, John Wood, Michael A. Trevits

We have tested the ability of ground penetrating radar (GPR) to resolve adjacent mine workings. The work was conducted at two National Institute for Occupational Safety and Health locations – an underground coal mine and an underground limestone mine. The objective of our work was to determine if GPR signals could be received from distant mine workings. The GPR system was calibrated on underground mine pillars of known dimensions using a variety of antennas. The system was then tested at several underground locations in an effort to detect an adjacent drift entry; and an adjacent abandoned coal mine. As a means of verification, an in-seam horizontal hole was drilled from the active coal mine to the abandoned mine to confirm the presence and location of the abandoned mine workings. Our results show that in the case of the limestone mine the maximum depth of penetration where the mine workings could be resolved was 85 ft; and in the case of the coal mine the abandoned mine workings could be resolved at a depth of 205 ft. We conclude that it may be possible to utilize GPR for initial underground mine studies followed by directional drilling to accurately delineate the extent and position of adjacent abandoned mine workings.

Detect hazards associated with abandoned mine openings through the use of integrated geophysical technology. Background Many abandoned mines in the U.S. present hazards to the public. The first step in abatement of these hazards usually requires locating the abandoned workings. Recent Colorado legislation resulted in a concerted effort aimed at mitigating the hazards associated with abandoned mine workings. The Colorado Department of Natural Resources-Mine Land Reclamation Division (CDNRMLRD) is responsible for locating and backfilling abandoned mine openings such as shafts, adits and collapsed features. Many shafts and adits can be located by inspection, other openings give little or no surface expression and must be located by drilling, or through the use of geophysical methods. A common method used for locating underground mine workings is to drill throughout the suspected area. However, it is prohibitively expensive to drill holes at the spacing needed to detect backlilled shafts and small voids associated with caving and/or chimneying. It may also be dangerous to move heavy equipment over shallow mined-out workings. Geophysical investigations that employ only a single method have had mixed success in detecting hazardous abandoned mine land cavities.

Jan 1, 1991

By Robert F. Chaiken

A novel approach to eliminating environmental and public safety hazards that are associated with fires in abandoned coal mines and waste banks involves the use of in situ combustion technology developed by the Federal Bureau of Mines to accelerate the burning of the wasted coals in place. This technology would be used under exhaust ventilation control conditions that would allow for total management of the hot gases produced. Combustion stoichiometries would be optimized to minimize unburnt combustibles and to maximize the heat content of the gas products, which will be exhausted at one or more fan locations. When necessary, scrubber systems would be employed to remove air pollutants, such as sulfur dioxide; heat utilization systems (process heat, steam, and electricity) would also be employed to offset operational costs. Ultimately, complete burnout would solve the fire and acid water formation problems of the abandoned coal mine or waste bank. Pertinent technical data for burnout control are derived and discussed in terms of the important material and operational parameters. In general, it is believed feasible to operate a burnout system in an existing abandoned mine or waste bank fire at thermal power levels in the range of 10 to 100 Mw, and at exhaust gas temperatures of 1,000° C (1,830° F).

Jan 1, 1980

By R. A. Keaens, L. C. IlsLey

For the purpose of this paper a junction box is defined as " a fused switch, inclosed in an explosion-proof compartment, provided with a ready means of connecting or disconnecting a trailing cable without exterior arcing." Junction boxes are intended for use 'at the end of trailing cables and are usually placed outby the last open break through in a coal mine. Where it is not safe to supply current through nips or a trolley, junction boxes suitably spaced along an entry permit tramming and movement of machines with safety, although not with any considerable speed. Junction boxes serve a threefold purpose: (1) They prevent dangerous arcing at the outby end of trailing cables; (2) they afford a safe, practical means of fusing or otherwise protecting the trailing cable; and (3) they provide an efficient means of transmitting power from the power circuit to the trailing cable. The first purpose is the most important from a safety standpoint. Dangerous arcing-that is, arcing capable of igniting gas-frequently takes place where trailing cab1c.s are attached to the power circuit. At either 250 or 500 volts only a very small arc is required to ignite mine gas. The usual method of connecting the trailing cable to the power circuit by cable nips or trolley taps does not make a good electrical connection; hence arcing may be expected at any time. Furthermore, junction boxes eliminate the personal hazard attendant upon the use of trolley taps by removing the possibility of accidental contact with trolley hooks or wire and the liability to injury due to manipulation of the device. In the general scheme of mine ventilation it is assumed that gas will not accumulate where junction boxes are placed, an assumption based on the normal operation of the ventilating system. In many

Jan 1, 1929

By Michael J. Magyar

This report contains a cost estimate of the Bureau of Mines process for dewatering Alaskan placer effluent streams with polyethylene oxide (PEO). In this process effluent slurry is withdrawn from the placer plant pond system after a primary settling stage. A dilute PEO solution is injected into the slurry line to flocculate the fine, suspended solids. The flocculated solids are dewatered on a stationary screen. Clarified water is returned to the placer operation or discharged, while the 35 percent solids waste is pumped back into the mine cut. Cost estimates are presented for dewatering plants processing 1,000 gallons per minute of effluent slurry at three representative turbidity levels. Both the placer and the dewatering plants operate on the same 1-shift-per-day, 6-day-per-week schedule for the 100-day Alaskan operating season. Estimated fixed capital costs for these plants processing placer with effluent turbidities of 1,000, 3,000, and 5,000 nephelometric turbidity units (NTU) are approximately $29,000, $31,000, and $34,000, respectively, on a fourth quarter 1986 basis. Operating costs are estimated to be $0.34, $0.37, and $0.40 per thousand gallons of effluent slurry.

Jan 1, 1987

By H. A. Tucker

This Bureau of Mines investigation was conducted to determine the appropriate quantities of rare-earth methals (REM) in the form of silicides to add to an alloy steel for the purpose of increasing toughness and ductility. The work was conducted in a vacuum induction furnace with the rare-earth additions required to deoxidize and desulfurize a simulated basic oxygen furnace (BOF) vacuum-degassed steel initially containing 0.013 to 0.016 percent sulfur. The product proved to be as good or better than the best basic electric furnace steel of the same composition made by the steel industry. Twenty-three experimental heats of 5 Ni-Cr-Mo-V steel were made, cast into 50-1b ingots, and hot-worked in a press and a rolling mill to ½ inch plates which were then heat-treated to 130/150 ksi4 yield strength. Impact and tension tests showed that the addition of 0.025 to 0.100 percent, or ½ to 2 lb per ton, respectively, of rare-earth metals when compounded with silicon were appropriate for increasing toughness and ductility. These quantities resulted in retained cerium contents between 0.014 to 0.025 percent, and increased the Charpy V-notch energy absorption and the percent reduction of area significantly as compared with base heats at the same sulfur content levels. All the test heats, including those with additions of REH of as much as 4 lb/ton, had greater Charpy V-notch energy absorption values than the base composition could have developed at the starting sulfur range of 0.013-0.016 wt pct.

Jan 1, 1968

By D. E. Wolfson

Destructive distillation (carbonization) was shown to be a feasible method of disposing of scrap tires. The Bureau of Mines conducted tests under a variety of conditions. Solid, liquid, and gaseous products were produced, recovered, and analyzed. The quantities of the various products were shown to be quite dependent on the test temperature. Variability in composition of the liquid and gaseous products with changes in test temperature was also significant.

Jan 1, 1969

By T. T. Campbell

This report describes the development of new electroplating baths from which tin-nickel alloy plate was deposited. Although tin-nickel plate can be deposited from an aqueous ammonium bifluoride bath, the corrosive nature of this bath has served as a deterrent to its use. The Bureau of Mines felt that more general acceptance of this new alloy plate would follow if neutral or alkaline baths could be developed. Promising results were obtained from electrolytes containing both tin and nickel chlorides dissolved in triethanolamine-hydrochloric acid or in ethylene glycol hydrochloric acid baths. Current efficiencies close to 100 percent were obtained with these baths. Research revealed that tin-nickel plate could be produced from organic solvents or from mixed aqueous-organic electrolytes. The composition of the alloy deposit - 65 percent tin and 35 percent nickel - was found to exhibit the same single-phase structure that is obtained from the commercially accepted fluoride-type bath.

Jan 1, 1959

By Joseph P. Flick, Kathleen M. Kowalski, Lynn L. Rethi, Roberta A. Calhoun

Many miners are involved in tasks at the mine site that are similar to those sub-tasks performed in general construction, maintenance and repair (CMR) type work activities. As a result, many of the injuries in the mining industry today can be traced to employees performing these CMR type work activities. Indeed, a recent analysis of a major aggregate company revealed that 65% of all injuries documented originated from performing such CMR activities. It is hypothesized that the number of injuries to miners performing construction, maintenance and repair (CMR) work activities on mine property may be reduced through improved training that focuses on better hazard recognition using the numerous visual and other cues that are available for evaluating workplace health and safety hazards. To this end, researchers at NIOSH’s Pittsburgh Research Laboratory have merged two proven methods of training miners to recognize hazards, stereoscopic (3-D) slides and the concept of degraded images, into this training program. Stereoscopic (3-D) slides have been shown in earlier NIOSH and U.S. Bureau of Mines research to be an effective training aid for improving the ability of miners to recognize various geologic and mining-induced irregularities that can cause groundfalls.3 They realistically portray the natural mine environment, and thus are an excellent training aid for teaching miners to recognize such visual cues. The degraded image concept, originally developed by the military and used for target detection training, describes scenes where the target is partially hidden by cloud cover, dust, rain, natural barriers, buildings, or other obstructions that can camouflage or confuse the target. Research had shown that flight observers who were trained with less than ideal (or degraded) pictures were more successful in subsequent identification of targets than those trained using ideal (or highlighted) pictures of targets. In order to investigate this concept for training miners to recognize hazards, NIOSH researchers developed a prototype hazard recognition training program using such mining scenes. A control program based on traditional highlighted mining scenes was also developed. Both programs were applied to subjects in a field experiment. Results indicated that miners trained with the degraded images did significantly better on a follow-up test of hazard recognition.4 This hazard recognition program teaches trainees to look for hazards in a more realistic manner than that of the control program. This specific training program for CMR activities involves using the degraded image concept and 3-D slides. The module is designed to educate workers on hazard identification techniques and safe work practices. It focuses on teaching miners techniques for recognizing visual (sight) cues, and then uses these cues to evaluate mining conditions. It should be stressed that other senses, such as sound can also play an important role in hazard detection.

Jan 1, 1999

Improve the safety of salt mine workers by providing a means for quickly identifying areas within the mine that?s how an increased potential for gas and salt outbursts. Approach Outbursts occur in salt mines when a high-pressure pocket of gas is intercepted during the mining process, resulting in a sudden and sometimes catastrophic expulsion of gas and salt. In one case, the amount of gas released through such an event caused an explosion that resulted in five fatalities. The U.S. Bureau of Mines has designed and developed a gas outburst prediction system that can quickly determine the potential instability of areas within rock salt mines. The determination is based on noise measurements obtained from samples of the salt as they are dissolved in water. This system improves upon technology currently available because it provides information in only a few minutes instead of in several days. In addition, present prediction systems are not only time consuming, but expensive because they require laboratory conditions and highly trained personnel to operate them and determine results.

Jan 1, 1989

By David C. McHuron

The U. S. Bureau of Mines in their continuing research into sealants, selected MBAssociates to design, build, and test equipment and evaluate sealant as to its effectiveness is shale degradation. There were 20,050 sq.ft. of coal mine roof sprayed with a mine sealant and as a result, it has been estimated that the sealant coated roof has from 50% to 95% less roof falls than that roof which was not coated with sealant.

Jan 1, 1980