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By Anand Kumar Agrawal, Kinzel Klaus Peter, Lorenzo Micheletti, Cristiano Castagnola, Horst Kappes, Andre Oliveira, Björn Rösner, Philippe Bermes

Blast furnaces are widely employed today for iron production all around the world, with a total production of around 1.2 billion tons per year. Its operating principle, which relies on usage of coke to reduce the ore, to ensure the permeability in the reaction vessel, to maintain its flexibility of operation and acceptability for varying qualities of iron ores. The blast furnace route is widely considered as the most economic and efficient route of iron production, however it is based on fossil energy carriers. The blast furnace route has undergone significant developments in terms of energy efficiency in the last decades, which led to a substantial reduction in the use of fossil reduction materials. Being an energy intensive process, competitiveness and cost saving in the blast furnace plant was always strongly related to the saving of energy and hence reduction of CO2 emissions. In addition to this, EU emissions trading system (EU ETS) as a cornerstone of the EU's policy in response to climate change has set new “challenges” for iron production in Europe. Paul Wurth has always been deeply involved in the development of energy saving technologies for blast furnaces. In the following a review of energy saving achievements developed in the last decades will be presented and the potential of available CO2 saving technologies will be summarized. Additionally, an outlook about the potential of future technologies, concepts and their impact on the blast furnace and the steel plant’s energy balance will be discussed. Finally, the replacement of carbon by hydrogen as reduction agent in the steel plant will be reviewed, with special focus on a comparison of costs and incentives.

Oct 1, 2019

By Stefan Wahlund, Tom Adams, Mats Söder, Zhi Zhang

By applying high-end rolls with utmost performance and superior surface quality, hot strip mills can be further optimized. Operations in the mill have been also waiting for improved roll solutions that can minimize required roll changes which impact production efficiency. Limitations are usually due to the low performance and surface degradation of the rolls in the late finishing stands (F5 – F7). VICTURATM is the most recent developed grade for rolls utilized in the late finishing stand at Union Electric Åkers (UEÅ). These rolls have been tested and applied in mills all over the world. A significant improvement over the enhanced ICDP rolls has been observed. Hot strip mills are realizing improved operating efficiency and Total Cost of Ownership (TCO) through the transition of their entire roll inventories to these break-through products.

Oct 1, 2019

By Johanna Alegría-Ortega

Cr/CrN bilayer coating was deposited on AISI 440C by Cathodic Arc. The composition and structure of the Cr/CrN coating were investigated by scanning Electron Microscope, X-Ray Diffraction and X-ray Photoelectron Spectroscopy. The results show that crystal structure obtained was CrN phase with preferred [220] orientation. The hardness and adhesion of coating also were studied. The evaluation of erosion-corrosion (EC) on 440C bare and coated with Cr/CrN was performed by carrying out wear tests using a slurry jet with impingement angle 90° at 4 and 8 m/s. Corrosion, erosion and synergism wear rate were evaluated following the procedure described in ASTM G-119-09. This study presents that the synergism wear rate exceeds 40% of the total mass loss for coating and 60% of mass loss for the 440C, being the most aggressive wear component. The increase in impact velocity generated a rise in mass loss for both 440C bare and coated. The Cr/CrN coating offers better corrosion and erosion–corrosion resistance under all the tested conditions.

Aug 8, 2018

By Enif Gutiérrez Guerrero

Inclusion deposition is still a standing problem in the continuous casting of steel since the deposition of alumina inclusions inside the SEN affects the productivity and the product quality. The present work studies the factors involved in the inclusion deposition at the nozzle and the effects of inertial, gravitational, buoyant, pressure gradient, and Saffman forces on the inclusion trajectories. The results show that the inclusions reaching the nozzle, only 30% get deposited along its walls mainly at the Upper Tundish Nozzle (UTN). This area of higher deposition is identified close to a low static pressure and a high turbulent kinetic energy dissipation zones where the effects of the gravitational and buoyant forces do not promote a significant inclusion radial movement since these are aligned with the direction of the flow stream lines. In contrast, in this zone, the Saffman force shows an important effect on the deposited inclusions, slowing down the inclusions in the vertical axis and increasing their radial movement.

Aug 17, 2017

By Rudolf Hubmer

In October 2013 JSW Steel decided to place an order to Primetals Technologies Austria (former Siemens VAI Metals Technologies) for the installation of a comprehensive Level 2 process optimization system for more than 20 existing production facilities of various suppliers. For SMS-I new L2 systems are provided for two hot metal pretreatment stations, three hot metal desulphurization stations, three ladle furnaces, two 1-strand slab casters, a ladle tracking system as well as a shop supervisory system. Additionally the existing L2 system for one 1-strand slab caster is being upgraded in the course of the project. In SMS-II new L2 systems for the 7 hot metal desulphurization stations, 4 ladle furnaces, 1 new RH vacuum degasser, ladle tracking system and a shop supervisory system are supplied. Despite of the challenging time schedule the commissioning of the single facilities started within less than 12 month after contract effectiveness. The installed Level 2 process optimization systems together with the achieved results are described in this paper.

Aug 16, 2017

By Madson Pereira Martins

A utilização de resíduos oriundos de processos industriais tem se tornado uma prática muito recorrente em todo mundo devido à questão ambiental. A legislação brasileira estipulou parâmetros rígidos de destino destes materiais e a indústria viu na construção civil uma possibilidade de utilização. Este trabalho tem como objetivo a caracterização do pó de pedra de gnaisse para utilização em concretos. Serão realizados ensaios de granulometria, determinação de massa especifica e material pulverulento. Os resultados mostraram a viabilidade da incorporação deste resíduo para a produção de concretos.

Aug 16, 2017

By Daniel Antonio Kapper Fabricio

Laboratórios de ensaios têm buscado implementar Sistemas de Gestão da Qualidade baseados na norma ABNT NBR ISO/IEC 17025 e procurado a acreditação de seus ensaios. A norma ASTM E517 estabelece um método de ensaio para a determinação do índice de anisotropia plástica de metais laminados, um importante parâmetro em processos de conformação mecânica por estampagem. Atualmente nenhum laboratório é acreditado pelo Inmetro na realização desse ensaio. Assim, o Laboratório de Metalurgia Física (LAMEF) da UFRGS optou por aumentar seu escopo de acreditação para abranger esse ensaio. O objetivo do trabalho é apresentar as adequações gerenciais e técnicas ao Sistema da Qualidade existente para a extensão de escopo, assim como as não conformidades encontradas e os pontos fortes para obtenção da acreditação junto ao Inmetro.

Aug 7, 2018

By Jorge Madias

Neste trabalho se leva a cabo uma revisão da literatura sobre defeitos em beam blanks. O foco é no mecanismo de formação e as soluções propostas para diminuir sua ocorrência. Os defeitos superficiais incluidos são as trincas longitudinais e transversais, bleeding, pinholes e escória. Os defeitos internos levados em conta são os blowholes, as trincas centrais e as trincas nas pontas das abas. A revisão incluie as técnicas utilizadas para pesquisar os defeitos: caracterização metalográfica, CFD, modelagem termodinâmica e termomecânica, etc. As medidas adotadas estãorelacionadas a mudanças no sistema de lingotamento (por exemplo o design da vâlvula submersa), design do molde, mudanças e regulação do resfriamento secundário, suporte dos veios.

Oct 30, 2017

By Bianca Proença

Fotocatalisadores de nióbio foram obtidos por anodização a 15 V, utilizando uma solução de K2HPO4 10% p/p em glicerol anidro como eletrólito por 15 minutos. As amostras foram caracterizadas por difração de raios-X para avaliação da estrutura cristalina obtida. A fotodegradação do glicerol (utilizado como agente de sacrifício) foi avaliada pela técnica de cromatografia líquida de alta eficiência.

Aug 16, 2017

By Gabriella Cruz dos Santos Roza

Os aços 1Cr-Mo-V forjados são largamente utilizados em rotores de turbinas a vapor, e o seu desempenho em condições de fluência vem sendo melhorado por tecnologias de fabricação. Sendo assim, os fatores metalúrgicos que afetam o comportamento em fluência dessa classe de material vem sendo estudados. O objetivo deste trabalho foi a avaliar as diferenças na microestrutura e nas propriedades mecânicas, a temperatura ambiente, entre amostras de aço 1Cr-Mo-V fundidas em forno elétrico aberto e amostras que posteriormente refundidas no forno a arco elétrico a vácuo (VAR). As amostras foram forjadas a quente e tratadas termicamente em mesmas condições. Para a avaliação das diferenças, foram comparadas as microestruturas nas duas condições e feitas análises de inclusões através de microscopia ótica e microscopia eletrônica de varredura. Foram realizados ensaios de dureza e de tração a temperatura ambiente. Os resultados mostraram que a refusão foi eficiente na redução do teor de alguns elementos deletérios e na redução do tamanho e do número de inclusões, sulfetos de manganês e silicatos de manganês, além de contribuir para uma distribuição mais homogênea tanto das inclusões como da microestrutura bainítica apresentada. As medidas de propriedades mecânicas a temperatura ambiente não mostraram alterações significativas na resistência. Porém, houve aumento na ductilidade, manifestado por uma maior redução de área.

Aug 16, 2017

By Breno Totti Maia

Due to operational conditions and locations, BOF suffers variations in important parameters whose effects on the liquid bath are usually neglected. The present paper investigated two aspects: inner BOF pressure and oxygen temperature in the stagnant reservoir. The results have shown that oxygen temperature changes properties like density and velocity but has small influence on jet penetration. The BOF inner pressure has significant influence on jet penetration and creates a new challenge regarding nozzles dimensions considering overexpanding and underexpading jets.

Oct 30, 2017

By Dilermando Nagle Travessa

High strength-light weight materials are very attractive for the transportation sector, particularly to the aerospace industry. High strength-age hardenable aluminium alloys are widely used in airframes due to their unique combination of strength, density, toughness, corrosion resistance, cost and easy processing. However, the hardening capacity of such alloys is somehow saturated due to thermodynamic issues related to the conventional processing. The production of aluminum-matrix composites is a promising strategy to overcome this limitation, resulting in strength levels that cannot be reached by actual commercial aluminum alloys. In the present work, multiwall carbon nanotubes were used to reinforce the AA6061 aluminium alloy. 1 and 2% weight percent of MWCNT were mixed to the alloy powder by high-energy ball-milling process. The blended powder was consolidated by hot extrusion. The obtained composite bars were submitted to heat treatment for the T6 condition in order to combine both CNT dispersion and precipitation hardening effects. Optical and scanning electron microscopy, as well as hardeness testing, was used to characterize the bars. Typical wrought microstructure, free of defects, was observed on the extruded bars. Hardness of the composites was observed to increase by 20, 28 and 68% for 1% MWCNT 6 h milling, 2% MWCNT 6 h milling and 2% MWCNT 10 h milling, respectively, in the as-extruded condition. The better performance for the composites blended at higher milling time was attributed to a better nanotubes dispersion. Subsequent heat treatment to the T6 condition did not result in additional hardening.

Aug 8, 2018

By Tiago Silva Costa

Os tratamentos térmicos são um conjunto de operações que têm por objetivo modificar as propriedades dos aços e de outros materiais através de um conjunto de operações que incluem o aquecimento e o resfriamento em condições controladas. Os aços SAE J403 1045, SAE J403 1075 e DIN 100CrV2 são aplicados em diferentes setores industriais graças às diferentes propriedades que podem ser alcançadas através de tratamentos térmicos. Este trabalho visou caracterizar e descrever as fases formadas nos aços SAE J403 1045, SAE J403 1075 e DIN 100CrV2 após tratamentos térmicos de têmpera, normalização e recozimento pleno.

Aug 16, 2017

By Amilton Ferreira de Oliveira

Este trabalho se propõe a mostrar os resultados obtidos pela SunCoke Energy Brasil após as mudanças do perfil da mistura de carvões, na qual foram acrescidas criteriosamente as participações dos carvões denominados “soft” e carvões “steam coal”, seguido da redução também criteriosa dos carvões médio voláteis. A consolidação dos dados de qualidade do coque e do custo das misturas comprova que as modificações no perfil das misturas foram bem sucedidas, pois a qualidade do coque se manteve conforme a expectativa dos clientes (Altos-Fornos) e o custo das misturas apresentou uma significativa redução. Todos os testes e experimentos adotados foram embasados na utilização na metodologia denominada “Método e aparelho para avaliar as propriedades de coqueificação do carvão”, também conhecida como Box Test, e ainda no profundo estudo das características dos carvões utilizados e os impactos destes na qualidade do coque.

Aug 16, 2017

By Felipe Beluche Lima, Caio Augusto Silva Santos

Brazil is the largest producer of crude steel in the Americas by BOF process and many challenges come along with the increasing market demand. In the BOF, a tubular wall hood structure has been showing premature failures related to the overlay welded tube technology placed in the hood wall. The main root causes were: thermal fatigue at 1800°C, hot spot formation, high heat-affected zone (HAZ) leading to susceptibility of stress cracking, carburizing corrosion and superficial wearing. Based on that, co-extruded tube technology (named composite tube by Sandvik) was the alternative chosen to enhance hood performance without compromising BOF process. In order to rises safety and productivity, composite tube has 100% metallurgical bond assuring stable expansion, high heat exchange efficiency, better corrosion resistance and less rough surface finishing. It was highly suggested to many others mills due to similar and already existing reported cases.

Oct 1, 2019

By José Divo Bressan

Present work examines material surface damage by cavitation erosion of metals or the wear phenomenon from water bubbles collapse near the metallic surface. Material surface damage by cavitation erosion is due to wear mechanisms of liquid micro-jets impingement and shock waves. Experimental cavitation in tap water was investigated, using the proposed new design of compact rotating disk equipment. In this device, a rotating disk with cavitation inducers and specimens fixed on it ran in tap water to provide cavitating flow at constant high speed of 47.9 m/s similar to service conditions in pumps and propellers. Two types of cavitation inducers in the rotating disk were investigated: through-holes and pins. Carburized cast iron, aluminum, brass and bronze specimens were tested in this device. The cavitation damage mechanisms were observed by scanning electron microscope. Surface damage in the specimens was measured by mass loss and plotted in graphs of mass loss versus running time. After 25 hours testing, the specimens surface showed pitting formation and mass loss. All specimens presented surface damage: pit diameter size was about 100 or 150 to 300 micron. In aluminum specimen, damages by burned pit formation and plastic deformation could be seen, however, the mass loss was lower than the expected, possibly due to alumina film formation. Present equipment had quite good test reproducibility when compared with results from literature.

Jul 31, 2018

By Rodrigo Perito Cardoso

Low-temperature nitriding of stainless steels is applied to obtain wear resistant surfaces without losing its corrosion resistance. The treatment consists in introducing nitrogen into the steel surface avoiding chromium nitride precipitation. The corrosion resistance of martensitic stainless steels is expected to be improved if the treatment parameters are correctly selected. It can be related to ?Fe2-3N and a'N phase formation on the treated surface. In the present work the influence of the pretreatment and treatment temperature on corrosion resistance of plasma nitrided AISI 420 steel samples is studied. Annealed, as-quenched and 400ºC-tempered samples were nitrided at 300, 350, 400, 450 and 500°C, for 6 h at 600 V. The pressure was 3 Torr and the gas mixture was composed of 70%N2, 20%H2 and 10%Ar, at a gas flow rate of 3.34×106 Nm3s-1. Plasma was generated using a square-wave pulsed DC power supply and the sample temperature was controlled by the duty cycle. The modified layers were characterized by optical microscopy, X-ray diffraction and microhardness measurement. The corrosion resistance was studied by electrochemical characterization, by means of Open circuit potential and Anodic polarization curves. The maximum surface hardness was achieved at 400°C. This temperature seems to be near the limit temperature for low-temperature treatment aiming to improve or at least to keep unaltered the corrosion resistance in relation to that verified for non-treated steel samples. Results confirm that the pretreatment and treatment temperature significantly affects the corrosion resistance of the treated surface.

Aug 8, 2018

By Fernando Velazquez Guzman

Titanium is an alloying element used to refine grain size in steel and improve its physical and mechanical properties. In some stainless steels it is used to increase the resistance to corrosion by the precipitation of titanium carbides or carbonitrides. Its alloying performance is highly variable and depends largely on the stage of the secondary metallurgy process when it is added. Furthermore, the addition method (wire injection or direct addition) has a remarkable influence in secondary refining. This paper describes the tests performed in vacuum degasser (VD), with a highly compacted and encapsulated Ferrotitanium wire (FeTi HC). The yield of titanium in steel increased from 52% to 89%. Moreover, the consumption of the highly compacted Ferrotitanium was optimized.

Oct 30, 2017

By Washington Martins da Silva Júnior

In stamping process, sliding between metal sheet and forming tool leads to wear of tool surface. Maintenance of stamping tools involves polishing the tool edge, or, in case of severe damage, replacement of the tool. Hard coatings have been applied on the stamping tool surfaces in order to reduce the maintenance cost causing a great economic impact in metal work industry. In this work, CrAlSiN coatings were applied by PVD onto SRV2W tool steel. The coating toughness was avaliated by the critical load in scratch tests. The following coating parameters were analyzed: 1- substrate surface finishing process; 2- coating architecture (multilayer or gradient); 3- chemical composition of the coating. AlSi concentration varied from the substrate/coating interface to the surface. Coatings were 3 µm thick. Scratch tests were carried out using a Vickers indenter. The applied normal load was varied from 0 to 13 N for a scratch length of 5 mm. In order to study the effect in the toughness, the substrate roughness was controlled by the finishing process before PVD coating. Samples subjected to polishing presented highest critical loads. Gradient coatings presented higher critical loads than those with a multilayer architecture. Coatings with higher concentration of AlSi near the surface supported higher loads before failure.

Jul 31, 2018

By Eduardo Piassi Nicoli

Este trabalho tem a finalidade de apresentar projeto para melhoria de qualidade e redução do consumo de água em torres de resfriamento sem a utilização de produtos químicos e ainda eliminando problemas de incrustações e acúmulo de metais pesados, corrosão e formação biológica, através de solução inovadora (novo modelo mental).

Oct 30, 2017