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By Harold W. Lipper

Helium production and shipment reached new peaks in 1.361. The Bureau of Mines produced 727 million cubic feet, 13 percent more than the 1960 record, and shipped 552 million cubic feet, 16 percent more than the 1960 record. Production exceeded demand for the third successive year, enabling the Bureau of Mines to add 174 million cubic feet to the volume stored underground for future use. At the end of 1961, the total volume of helium in underground storage in the Clifside gasfield was 44-7 million cubic feet. Contracts to implement a long-range helium conservation program were completed with four companies, obligating all the contracting authority of $47.5 million a year made available by the Congress. The four companies will finance, build, and operate helium extraction plants to recover from natural gas an annual average of 3.1 billion cubic feet of helium that would ordinarily be wasted when the helium-bearing natural gas is used for fuel.

Jan 1, 1962

By A. Dale Marcy, Pamela L. Drake

Workers who perform routine welding tasks are potentially exposed to fume that may contain manganese. Manganese may cause respiratory problems and is implicated in causing the occurrence of Parkinson-like symptoms. In this study, a field colorimetric method for extracting and measuring manganese in welding fume was developed. The method uses ultrasonic extraction with an acidic hydrogen peroxide solution to extract welding fume collected on polyvinyl chloride filters. Commercially available pre-packaged reagents are used to produce a colored solution, created by a reaction of manganese(II) with 1-(2-pyridylazo)-2-naphthol. Absorbance measurements are then made using a portable spectrophotometer. The method detection limit and limit of quantification (LOQ) were 5.2 mg filter-1 and 17 mg filter-1, respectively, with a dynamic range up to 400 mg filter-1. When the results are above the LOQ for the colorimetric method, the manganese masses are equivalent to those measured by the International Organization for Standardization Method 15202-2, which employs a strong acid digestion and analysis using inductively coupled plasma-optical emission spectrometry.

By I. AITKENS

The group of gems included under the general name "feldspar" occupies only a minor place in jewelry. Feldspars, with the possible exception of quartz, are the most important of rock-forming minerals, but most occurrences are of quite ordinary varieties, without striking color and unattractive. Few specimens are suitable for use as gem stones, but occasional crystals that exhibit unusual brilliance or play of color are cut into various shapes for personal adornment or for architectural decoration. The best known of the feldspar gems, and probably the most important in point of production, is the moonstone. Amazon stones, labradorite, sunstone, and a number of less common varieties have been produced in various parts of the world.

Nov 1, 1931

The faculty, graduate students, and post-doctoral researchers are an integral part of the Generic Mineral Technology Center for Respirable Dust. More than fifty (50) scientists, engineers, and medical personnel are engaged in respirable dust research at five universities, The Pennsylvania State University, West Virginia University, Massachusetts Institute of Technology, University of Minnesota, and Michigan Technological University. The expertise, effort and contribution of these individuals has proven to be invaluable in the attack on respirable disease. Nationally and internationally recognized researchers in the areas of particle characterization, interaction of dust and lungs, dilution and dispersion, rock mechanics and continuing education lend their laboratory facilities, equipment and human resources to benefit the mining industry. The expertise and resources of the National Institute for Occupational Safety and Health--Division of Respirable Disease Studies is available through their relationship with West Virginia University.

Aug 31, 1989

By B. Dimitriades

Experimental work has been done to refine and to confirm an analytical procedure by which gas-liquid chromatographic (GLC) spectra are interpreted from retention time data alone. The rationale of this spectra interpretation technique involves whether or not a given peak invariably represents the same component or component mixture; if not, what factors influence changes in peak identifications. To answer these questions, peak-identification procedures, based mainly on the use of subtractive columns, were developed and applied to interpret GLC spectra of several exhaust (and fuel) samples.

Jan 1, 1972

By T. Brady, R. Langston, J. C. Johnson, H. Kirsten

An experiment is described in which instrumented rock bolts were used to measure strain in the rock mass during drift development at the Stillwater Mine, Nye, Montana, USA. Two strain-gauged rock bolts were grouted into the middle of the rib next to the face. The drift was excavated in three advances, each one-half drift wide. Strains were recorded hourly by a data logger. Results show that the average change in axial bolt strain for the first and second advance was about the same and that there was almost no change in strain after the third advance. Bending strain was observed 19 cm from the head of the bolt.

By W. S. Sanner

Grinding experiments were conducted to determine the finest anthracite particles that could be produced in a ball mill. Continuous and batch tests were run in a dry-grinding ball mill. Batch grinding produced the finest coal particles. They averaged 2.2 microns in diameter and were 99.0 percent smaller than 37 microns. Continuous grinding yielded a product 6.1 microns in diameter, with 96 percent smaller than 37 microns.

Jan 1, 1968

By Frank J.

The increased demand for aluminum for military purposes during World War II necessitated the development of domestic deposits of alumina-bearing ores. Kaolin, siliceous bauxites, anorthosite, and diaspore-containing clays have been investigated and studied in the laboratory and pilot plant. The Bureau of Mines is preparing a series of reports covering investigations of these ores. The tests contained in this report are restricted to sintering and leaching tests on kaolin from South Carolina, where extensive deposits were proved to exist. The leach liquors were found to have substantially the same composition as those produced from the diaspore-containing clays, and therefore it would be expected that no difficulty would be experienced in producing calcined alumina of relatively coarse particle size and with other properties conforming to the specifications for metallurgical-grade alumina.

May 1, 1947

By Ruth A. Holmes

A Bureau of Mines method for recovering nickel, cobalt, and copper from low-grade domestic laterites is described, which includes the unit operations of solvent extraction and electrowinning. Previous Bureau work indicated that addition of Na2S04 (sodium sulfate) to the nickel electrolyte improved current efficiency in nickel electrowinning. The present study determines the compatibility of Na2S04 with nickel strip-ping in the solvent extraction operation of the Bureau method. The effect of adding 100 g/l Na2S04 on nickel stripping, phase disengagement, and pH was determined in comparative laboratory-scale tests. In continuous-circuit testing, Na2S04 reduced stripping efficiency to the extent that five, instead of four, strip stages were required for complete stripping of nickel from the loaded solvent. In tests made in a phase-disengagement cell that had a variable settler area, the addition of Na2S04 did not significantly affect phase separation characteristics. The pH of the nickel electrolyte in the temperature range of 20° to 65° C was also unaffected by the addition of Na2S04. An economic evaluation showed that the energy saved by adding Na2S04 to the electrolyte would more than offset the cost of adding another stripping stage.

Jan 1, 1983

Reduce the dust exposure to the operator of a longwall shearer with a novel foam spray system. Approach Discharge foam through the nozzles of a shearer drum so that foam and coal are better mixed. How It Works Bureau of Mines research showed that two very important principles for successful application of foam are: (1) moisture distribution and (2) degree of mixing. Foam can distribute a given quantity of moisture much more evenly over a large surface area. Successful Bureau tests of foam for dust control always involve a high degree of mixing between the foam and the material, Mixing, permits a greater distribution of foam throughout the mined product. The most suitable location of foam application would be at the point where the dust is generated, before the dust becomes airborne. Foam nozzles located in the cutter drum (pick face foaming or ejecting foam through scroll sprays) will suppress dust close to its source.

Jan 1, 1989

Develop a safe, nonpolluting power source for underground mining equipment. Approach The Bureau of Mines and EIM-CO Mining Machinery International entered into a cost-shared project to develop and demonstrate a novel power source for mining. An underground mining utility truck was equipped with an ultra-low-emission hydrogen-fueled engine and a safe, metal hydride fuel storage system. How It Works The nonpolluting hydrogen engine and a "solid-state" (metal hyride) hydrogen fuel storage system were combined to power a utility mining vehicle. An 85 horsepower diesel engine was convened to burn hydrogen. The engine was converted by equipping it with a spark ignition, lowering the compression ratio, turbocharging, and adding an ahercooler and a parallel fuel induction system. Parallel induction provides two intake paths, one for hydrogen and one for air. It avoids intake-manifold backfiring by keeping the hydrogen and air separate until they enter the cylinder.

Jan 1, 1986

By Frederick C. Trutt, Jeffery L. Kohler, Joseph Sottile

Twenty-five years ago, the former U.S. Bureau of Mines funded a research project aimed at developing the enabling technology for incipient failure prediction in electric power system components as a means of reducing the injuries and fatalities that sometimes occur when equipment malfunctions. Over the ensuing years, interest in this has waxed and waned, but recently interest has been growing for both civilian and military applications. This paper addresses the level of turn-to-turn insulation deterioration that can be resolved using an on-line monitoring technique. The detection of turn-to-turn defects is especially important because they are believed to represent the beginning stage of most motor winding failures.

By J. E. Matta

The Bureau of Mines has developed a tracer gas method for measuring leak-age through permanent mine stoppings. In this method, a temporary brattice is erected in the same entry as the leaking permanent stopping. Leakage was evaluated from concentration measurements of a tracer gas introduced into the space between the stopping and brattice. Stopping leakages ranging from 15 cfm to 265 cfm were simulated in an underground coal mine. Leakage values determined by the new method were within 10 pct of the known values.

Jan 1, 1978

This report was prepared by Jacob Tolsma and Arnold N. Johnson of the Uniroya 1 Research Center, Wayne, New Jersey. The valuable assistance and suggestions of the project officers, Mr. Ronald D. Hill, Dr. David R. Maneval and Mr. John J. Buscavage is gratefully acknowledged. The authors are grateful to the following Uniroyal personnel: Mr. Daniel Shichman, manager of Engineering Research, and Dr. Emmanuel G. Kontos, manager of the Polymer Physics Research for their direction, encouragement and suggestions regarding the experimental work, and Mr. Mark Olson for the design of the hollow auger soil sampler. We also wish to gratefully acknowledge the efforts and contributions of ideas proposed by our consultants, Dr. Frank T. Caruccio, assistant professor of geology at State University College, New Paltz, New York, and Dr. Pa Ho Hsu, associate professor of soil chemistry, Rutgers University , New Brunswick, New Jersey.

Jan 1, 1972

By M. M. Tilman

A series of alloys was laboratory prepared by adding up to 4 weight-percent cobalt to the basic composition of type AM 350 (AISI 633) stainless steel. Aging curves were established for each alloy at 750° F, 850° F, and 950° F for lengths of time up to 100 hours. A series of annealed steels containing as much as 1 weight-percent cobalt was cold-rolled 50 percent and aged for 3 hours at 850° F. No improvement in hardness due to cobalt was observed in the steels transformed by heat treatment. Slight improvements in hardness were observed in the steels transformed by cold working.

Jan 1, 1968

Aid mine workers in detecting hazardous roof conditions in underground mines by developing a method of roof sounding which supplements or replaces the traditional roof sounding technique where the miner relies on experience to determine whether or not the rock is sound. Approach The Bureau of Mines developed an electronic roof sounding de-vice that acoustically determines the integrity of mine roof rock by "listening" to the variation in frequency vibrations within the rock. How It Works n previous research, the Bureau of Mines found that loose rock in a mine, when impacted, vibrates at a much lower frequency and for a lower time period than does a solid slab. By quantifying the enhancement of low frequency vibrations in loose rock over solid rock, a repeatable, objective measure of the rock's soundness can be obtained. This approach was used in developing the rock stability tester.

Jan 1, 1986

By Thomas O. Llewellyn

Laboratory semicontinuous and continuous heavy liquid cyclone separation pilot plant tests were made to determine the feasibility of producing a high-grade kyanite concentrate from a kyanite-quartz rock sample from Graves Mountain, Ga. Use of a three-stage heavy liquid cyclone circuit demonstrated that a 96.4-to 99.0-percent kyanite concentrate could be obtained with recoveries of 95.5 to 96.7 percent. The test work showed that by steam stripping with 6.9 tons of steam per ton of ore and two stages of detergent scrubbing the residual TBE content of kyanite cyclone products was 0.22 pound per ton of ore.

Jan 1, 1971

By J. H. Russell

As part of its efforts to maximize resource recovery, the Bureau of Mines conducted studies to recover valuable byproducts from Western phosphate beneficiation tailings. Potential byproducts include phosphorus, vanadium, and uranium. The objective was to determine roasting and leaching conditions for maximum dissolution of vanadium from tailings containing approximately 13 pct P205 and 0.23 pct V. Sulfuric acid leaching tests were conducted with the tailings either as a dilute suspension dried, or in a roasted condition with or without NaCl added during roasting. More than 90 pct of the vanadium was dissolved by roasting at 850° C for 120 min with 8-pct NaCl and leaching at 75°C for 120 min with an excess of 2N H2S04, By roasting without NaCl and avoiding the difficulties of the chloride impurity, nearly 80-pct vanadium dissolution was achieved with an 800° C roast for 180 min. Quadratic regression equations were derived to relate vanadium dissolution to roasting and leaching conditions.

Jan 1, 1982

By A. J. Miscoe, W. M. McKewan

A unique machine for inducing bending fatigue in wire ropes was built at the U.S. Bureau of Mimes' Pittsburgh Research Center. This machine can produce nine levels of degradation through repetitive cycling of long samples of wire ropes of the types used in the mining industry. This report provides an analysis of the results of the first wire rope to be fatigued on this machine. These results have indicated that as a wire rope accumulates bending cycles, its strength first decreases because of wear and then in- creases due to cold working of the wires. As the amount of cold working increases, more and more of the embrittled wires break and the strength of the rope decreases rapidly. In this test, application of several of the regulatory retirement criteria to various sections of the rope suggests that there may be some inconsistency among them.

Jan 1, 1993

By R. V. Ramani, V. T. Burgos, J. A. McClay

This report was prepared by The Pennsylvania State University under USBM Contract No. G0111808. The contract was initiated under the Coal Mine Health and Safety Program. It was administered under the technical direction of DMSE, with Mr. G. R. Schottler acting as the technical project officer. Mr. J. A. Herlckes was the contract administrator for the Bureau of Mines. This report is a summary of the work recently completed as part of this contract during the period June, 1971 to September, 1974. Thls report was submitted by the authors on February 13, 1975.

Jan 1, 1975