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By J. P. Walsted

The lack of an iron-smelting industry in the Pacific Northwest places the ferrous metals industries under an economic handicap. No iron-smelting enterprises, now dormant, had been operated successfully. Iron made at both of hoes installations proved to be satisfactory for normal pig-iron uses. Electric power and reductants acre available in the area. Power from the dames now completed and. those being constructed insures present and future needs for basic industries. Subbituminous coal, close to the main supply of iron ore, insures ample reluctant for all smelting requirements.

Jan 1, 1954

By J. J. Drost

This Bureau of Mines investigation studied the effect of thermal treatments upon concentratability of a western Mesabi Range nonmagnetic taconite ore and is a sequel to Bureau of Mines RI 7567. Magnetic tube tests were used to develop the data needed to calculate separation efficiency, the primary measure of concentratability. A horizontal tube furnace was employed to heat treat and reduce the hematitic ore samples. The two variables studied were roasting temperature and cooling method. The manner of cooling, either by slow cooling or quenching in water, produced no significant difference in concentratability. Roasting temperatures employed ranged from 500° to 1,000° C, and a temperature of 650° C effected the best concentratability. The temperature of 650° C correlated with the most effective roasting temperature for grindability.

Jan 1, 1973

By L. C. George

Addition of an acid waste to an alkaline cyanide waste was investigated for five different combinations of electroplating wastes. At the optimum final pH values of the mixtures, metals and cyanides were almost quantita¬tively precipitated. No evolution of hydrogen cyanide was detected by a few additional processing steps, significant amounts of variable metals were recovered for recycling the waste-plus-Waste step is attractive because no reagents are required, metals arc concentrated, and a relatively harmless effluent that meets most water quality Standards for cyanide content is produced.

Jan 1, 1970

By B. J. Scheiner

Extraction of molybdenum from molybdenite ore by an electrolytic oxidation procedure was investigated by the Bureau o f Mines. Various parameters affecting molybdenum extraction, such as salt concentration, temperature, treatment rate, current density, and particle size, were studied. Molybdenum extraction of 95.2 percent was achieved on a laboratory scale from an ore containing 0.35 percent molybdenite. Corresponding power consumption was 24 kwhr per pound of molybdenum extracted with a base consumption of 4.5 pounds of sodium carbonate. Laboratory and pilot plant experiments are in progress on low-grade molybdenum concentrates containing rhenium and copper. Preliminary results indicate that molybdenum extractions in the 90- to 99-percent range and rhenium extractions of 93 to 99 percent can he obtained without appreciable oxidation of associated copper minerals.

Jan 1, 1972

By Jon C. Volkwein

Advances in mining technology have enabled deeper seams of coal to be mined from the surface. Highwall mining is frequently used to mine areas at the perimeters of a surface mine when removal of the overburden becomes uneconomical or threatens environmentally sensitive surface features. At the same time, advances in materials and technology have enabled highwall mining of coal that create blind headings over 300 meters in length. Deeper surface mining and deeper highwall penetration depths have lead to more frequent encounters with methane gas. While this coal is remotely mined from the surface, underground ignitions of methane have propagated to the surface and injured miners. Methods described in this paper show how this hazard can be correctly monitored and controlled for auger type highwall mining machines. Research indicates that small quantities of gas liberated during mining migrate to the face, creating higher gas concentrations than would otherwise be expected. Using the same principles that cause the gas to migrate to the face, researchers have shown that inert gas introduced at the collar of the hole can inert the entire hole, thus ensuring safe conditions for mining.

By Robert T. Beckman

The results of a preliminary investigation of compressive strength versus length-diameter (L/D) ratios of potash specimens and the statistical treatment of the data are summarized in this report. The purpose of the study was to evaluate a laboratory method for obtaining estimates of the strength of potash pillars during robbing operations. The specific objectives of this preliminary investigation were to test the method and the reliability (confidence limits) of the data, and to determine the number of additional specimens necessary for given confidence limits. The specimens were taken from three sites at two mines in New Mexico. The statistical analyses included the determination of the confidence limits for the data and the number of additional specimens necessary to obtain confidence limits of ±500 and 100 psi. The testing method was found acceptable, and estimates of the comprehensive strength, within 1500 psi, could be obtained by testing about 110 additional specimens from the three sites. The compressive strength of the specimens tested fits an empirical equation of the type

Dec 1, 1963

[THIS bibliography lists publications issued by the Bureau of Mines concerned with investigations on petroleum and natural gas. The items included are chosen for their continuing interest and value. It was recognized early that a list of petroleum and natural gas publications was needed for the Bureau's work, and unofficial publication of a ?straight forward listing? was begun. It was at first a chronological list; however, suggestions submitted by its users prompted a formed change to show publications under broad, general topics. Author and subject indexes were developed, becoming more detailed with each new edition. This present list supersedes the ones compiled in 1949, 1952, and 1957, and several supplements, which were aside available to the public by the Library Of the Bureau?s Bartlesville Petroleum Research Center. The unofficial field publication came to be widely known and in considerable demand by those who are primarily interested in the Bureau's publications on petroleum and natural gas so that it became, desirable to have it published as an Information Circular. It is hoped that this official publication will result in a wider and more effective use of the Bureau's research results which are reported in its publications.]

Jan 1, 1964

By John C. Franklin

A radon survey was made at five different locations in the Twilight mine near Uravan, Colo., to determine chances in radon concentrations in an inactive mine. Data were taken with a continuous monitor set for 1-minute count periods and readings were taken 24 hours a day for 9 days. The 12 readings per station each hour accurately showed how t w radon concentration varied during the day. From the data collected from the intake portal to station 4, the average radon emanation rate was estimated at 18 picocuries per second per square foot (pCi/sec/ft3). A daily cycle in radon concentration was detected that apparently was related to barometric pressure change.

Jan 1, 1976

By R. E. Lindstrom

Electrooxidation techniques were investigated on a bench scale by the Bureau of Mines to determine the applicability of the process for extracting molybdenum and rhenium from low-grade molybdenite concentrates. Parameters affecting the extraction, such as pulp density, power consumption, reagent requirements for pH control, and electrolytic cell configuration, were studied. Molybdenum and rhenium extractions of 98 to 99 percent were achieved from several concentrates containing 4.76 to 28.6 percent molybdenum and 180 ppm to 1,000 ppm rhenium. Optimum results were obtained by maintaining pH values between 5.5 and 7.0 during electrolysis and allowing the final pH to rise to about 8.2. Reagent consumption was 4 to 6 pounds of sodium carbonate per pound of molybdenum extracted. The power consumption declined from a range of 12 to 25 kilowatt hours per pound of molybdenum extracted with immersion electrodes to 9.7 kilowatt hours with a bipolar flow-through cell; however, molybdenum extraction was independent of cell configuration.

Jan 1, 1973

By Carl Belser

In 1925 the Park Utah Consolidated Mines Co., after several years of experimental work, installed a system for signalling from cages which has been operating efficiently and with low upkeep costs for the post 19 years. The system was adopted for a large western metal mine but was later abandoned be arse of the constantly shifting shaft alinement. Recently the system has been studied and probably will be put into service at two other large mines. One of the principal reasons wry the system has not boon adopted more widely has been the lack of adequate details both as to the desirability of having such a system and as to its construction and operation. Previous signaling, systems contained undesirable features, such as charged bare wires extending the full length of the shaft. Under the direction of O. N. Friendly, then general superintendent of the Judge Mining & Smelting Co., the present system, entailing the use of a samll current at low voltage, was gradually developed. Many of the refinements in the system wore contributed by Leonard Wilson, consulting electrical engineer, Salt Lake City, Utah.

Jan 1, 1945

By H. R. Shell, John L. Miller, M. V. Denny

In the mica research program conducted by the Bureau of Mines at Norris , Tenn . , many micas other than silicon fluorphlogopite have been synthesized . It has been well established since the initiation of the program that synthetic micas are important materials useful for their superior or unique properties as well as substitutes for natural micas . The possibility of controlling the physical properties of synthetic mica by isomorphic substitution of other ions in the fluorphlogopite lattice further emphasizes the importance of these materials . Accurate measurement and reporting of their properties constitute an essential part of the research program . The study of germanium fluorphlogopite is in keeping with the requirements of a comprehensive study on isomorphic substitution , specifically to identify precisely the material -- chemically , structurally , and optically . The X- ray measurements , including indexed powder and single crystal data , with a description of the methods used to obtain these data , are provided . 5 Earlier work on germanium mica by R. A. Hatch et al . (5) gave an estimate of the cell parameters from X - ray powder data , but no attempt was made to index the diffraction pattern or to determine the space group symmetry . Later work by E. A. Schatz and J. C. Withers (9) listed X- ray and optical measurements , but no attempt was made to index the mica or determine its symmetry . Roth (7) found that germanium dioxide having the a - quartz structure , when heated with equimolar percentages of MgO , CaO , Sr0 , or Ba0 at 1,235 ° C , formed ABO3 -type compounds , e.g. MgGe03 isostructural with enstatite (MgSiO3 ) . Geo₂ also has a rutile - type polymorph with Ge ++ ions in octahedral coordination . Germanium was substituted for silicon in the serpentine structure by Roy and Roy (8 ) using hydrothermal techniques . These authors wrote as follows : "The substitution of Ge + for Si + yielded a magnesia - germania serpentine , formed easily in euhedral hexagonal plates which in some instances were visible in the light microscope . Electron micrographs and the sharp X - ray diffraction patterns confirm a plate - like rather than tubular habit . " It has been shown in this investigation that substitution of germanium for silicon in the mica structure is readily accomplished without radically changing the characteristics of the mica . Substitutions in the mica structure take place in three locations : Tetrahedral , octahedral , and interlayer positions . The tetrahedral positions are normally occupied by Sit or by a combination of Sit with Al +3 the most common combination being 2A1 +3 and 6Si +4 · , The octahedral position , which has six - fold coordination in phlogopite , contains a larger cation such as magnesium . In muscovite it contains only 2A1 ions ; therefore , this mica is considered a dioctahedral mica , whereas phlogopite is considered trioctahedral . +3 The interlayer position has twelve - fold coordination with six oxygen ions from each of two adjacent tetrahedral silica layers . This is the cleavage plane of the mica and commonly contains the largest cation in the mica structure (e.g. potassium) .

Jan 1, 1964

Reduce costs of recontouring surface mined land by improving bulldozer blades. Approach A specialized 48-foot-wide bulldozer blade set at an angle, a 13-foot bulldozer blade with swept-forward end sections, and a 24-foot grading bar are used in conjunction with conventional bulldozers to reduce the cost of recontouring surface mined land. How They Work The angle blade is used to do the initial and intermediate leveling of long spoil banks. It is mounted at an angle on two 410-horsepower crawler tractors in a side-by-side offset configuration, but requires only one operator since both tractors are controlled by a single set of controls. The angle blade usually begins its cycle at one end of the spoil bank where the operator fills the blade and moves forward, continuously cutting and casting the material to the repose slope. At the opposite end of the spall bank, the angle blade turns around and begins cut-ting and casting material to the opposite repose slope. This action continues until adjacent banks meet or the lateral distance from the center line of the spoil bank to the repose slope exceeds approximately 40 to 50 feet. At this distance, the sidecasting angle blade is no longer effective, and conventional bulldozers are used to do the final land shaping.

Jan 1, 1981

Etching solutions containing hexavalent chromium ions (e.g., chromic acid) are used in brass finishing, printed circuit board etching, preparation of plastic for plating, anodizing, and various other industrial surface treatment operations. As the solutions are used, hexavalent chromium ions are reduced to their trivalent state, contaminants accumulate in the solution, and the effective acid concentration is reduced. When the etching rate becomes unsatisfactory for the particular operation, the solutions are discarded. This is a problem because the discarded solutions are pollutants, and because replacing the etching solution is expensive. The Bureau of Mines has developed a process for regenerating these spent solutions and returning them to the surface treatment operation without interrupting the etching process. An electrolysis cell containing anode and cathode compartments that are separated by permeable membranes, is used for regenerating the spent solutions. The spent chromic acid solution is fed to the anode compartment and sui (uric acid is circulated in the cathode compartment. Application of a steady electrical potential of a few volts dc across the electrodes causes the copper ions and other contaminants in the spent solution to migrate through the membrane to the cathode compartment where copper is plated onto the cathode. Zinc and the other contaminants remain in the sulfuric acid. At the same time, the complex, trivalent chromium ions in the spent solution are attracted to the anode where they are oxidized to their original hexavalent state. The regenerated solution in the anode compartment is then recycled back to the plant?s etching operation for reuse.

Jan 1, 1980

As part of the Bureau of Mines subactivity in secondary resource recovery and to expand the Nation's mineral base, the Tuscaloosa Research Center made characterization and preliminary beneficiation studies of the waste residues from various coal-conversion processes: from pilot plant tests of the Synthane process for coal gasification, the Synthoil process for coal liquefaction, and the solvent-refined coal (SRC) process for sulfur removal from coal. Those coal conversion processes selected for this study were based on the availability of pilot plant samples. Physical, chemical, and mineralogical examinations of the wastes made to determine the mineral content prior to physical beneficiation tests indicated that in addition to significant quantities of carbon, some trace elements offer potential for concentration.

Jan 1, 1980

By A. J. Kraemer

[A great deal of interest has been manifested in the question of sulphur in fuels for automobile engines. Many different opinions have been expressed with respect to the effect of sulphur in gasoline on engine wear and engine performance. A wide difference of opinion exists as to the permissible limit of sulphur content for satisfactory operation.]

Jan 1, 1927

By Thomas M. Barczak

The success of longwall mining can largely be traced to the development of powered roof support systems. The most significant improvement in powered support design has been the shield support, which improved kinematic stability and promoted the application of longwall mining in difficult-to- control caving conditions where chock and frame supports were inadequate. The most obvious trend in shield design has been an increase in shield size and capacity. This U.S. Bureau of Mines report examines shield design and operation practices and their consequences for the utilization of high-capacity shield support systems. An optimization goal is to minimize support loading by selecting an active shield setting force that is compatible with strata behavior and shield loading characteristics. Shield stiffness is an important design parameter that is often overlooked. A consequence of increasing shield capacity by incorporating larger diameter leg cylinders is a proportional increase in shield stiffness. Setting forces have also increased in direct proportion to the increase in shield capacity. The increased stiffness and higher setting force cause the available capacity to be consumed more quickly, severely limiting the ability of high-capacity supports to last longer and provide reserve capacity for difficult mining conditions.

Jan 1, 1992

By W. A. Selvig

"INTRODUCTION In 1942, Lowry and Junge 3/ reported the results of a statistical study of errors for the proximate and ultimate analysis of coal and coke when made according to the standard Methods of Laboratory Sampling and Analysis of Coal and Coke (D271-42) 4/ of the American Society for Testing Materials. Some of the laboratories that cooperated in the investigation reported difficulty with determination of the volatile matter of anthracite and low-temperature coke. The small number of analyses reported for these particular fuels was considered inadequate to justify definite conclusions regarding the precision of this determination.The investigation described in this report was made at the request of Committee D-5 on Coal and Coke, A.S.T.M. (A. C. Fieldner, chairman), to secure additional information regarding the errors of the volatile matter determination for anthracite, low-temperature coke, and subbituminous coal; the last fuel also gives trouble in this determination, The committee has recognized that the allowable differences between duplicate determinations of volatile matter for these fuels as given in the standard methods are perhaps too stringent and may require revision."

Dec 1, 1943

This bibliography lists publications issued by the Bureau of Mines concerned with investigations on petroleum and natural gas. The items included are chosen for their continuing interest and value. It was recognized early that a list of petroleum and natural gas publications was needed for the Bureau's work, and unofficial publication of a ?straight forward? listing was begun. It was at first a chronological list; however, suggestions submitted by its users prompted a format change to show publications under broad, general topics. Author and subject indexes were developed, becoming more detailed with each new edition. This present list supersedes the ones compiled in 1949, 1952, and 1957, and several supplements, which were aside available to the public by the Library Of the Bureau?s Bartlesville Petroleum Research Center. The unofficial field publication came to be widely known nail in considerable demand by those who are primarily interested in the Bureau's publications on petroleum and natural gas so that it became, desirable to have it published as an Information Circular. It is hoped drat, this official publications will result in a wider and more effective use of the Bureau's research results which are reported in its publications.

Jan 1, 1964

By Launa Mallett, Charles Vaught, Michael Brnich, ROBERT PETERS

Interviews of 48 miners who escaped underground coal mine fires revealed that none of them had ever, before that incident, worn their self-contained self-rescuer (SCSR) either in training or in a real emergency. Consequently, they were ill-prepared to use this emergency breathing apparatus. One persistent problem stemmed from the fact that miners had no notion of breathing resistance, nor of the fact that it would get more difficult to breathe the longer they wore their device. As a result, many of those who were interviewed had simply removed their mouthpieces and breathed ambient air. This is obviously behavior that should be trained out of the workforce. Unfortunately, because of high costs and difficult logistics, miner training is unlikely to ever include donning and wearing an apparatus on a regular basis. In order to give workers a better idea of what to expect from their devices, therefore, the National Institute for Occupational Safety and Health researchers developed a tabletop (paper and pencil) simulation based upon actual predicaments evacuees had reported encountering. The simulation is designed to emphasize important points related to donning and wearing a self-contained self-rescuer in a mine fire escape, and, by doing so, to bring miners' expectations more in line with what their actual experiences would be. The simulation was field tested in six training classes at three different mining operations. In all, 99 individuals were involved in completing the exercise and rating its properties. In their ratings 88% of the respondents indicated they thought the scenario could definitely happen in real life, and over 80% agreed they had learned something new. From the field test data it was concluded that the simulation had authenticity and potential value as a teaching tool. The simulation was therefore used in a pre-test/post-test control group experiment to determine whether it led to improvements in miners' scores on a true-false test of their SCSR's functional capabilities and proper usage. Eighty-three miners were included in this part of the study. As expected, miners who had participated in the training exercise scored significantly higher on their post-test than miners who had not.

The panic bars (and associated linkages and electrical circuitry) that are defined in this document are a machine operator-actuated control for the emergency deenergization of the tram motors on self-propelled, electric and diesel face equipment; including haulage equipment such as shuttle cars. There are nine basic types of panic bars (and several variations) that are recommended in this document, but all of the panic bars are characteristically of the "fire door" type that is frequently encountered on outside exit doors of many public and some commercial buildings. It is also the intent of the following panic bar designs that, when emergency brakes are added to the face equipment machinery for which they arc required, that they be designed and hooked up so that actuation of the panic bar will result in automatic application of the emergency brakes (immediately following the deenergization of the tram motors). The following panic bar design requirements are a restatement of the proposed requirements defined in the Federal Register, requirements cited in "Guidelines for the Design and Installation of Devices for Deenergization of Self-Propelled Electric Face Equipment/Automatic Emergency Brakes" by G. E . Lester and J. D. Greenhalgh of MESA, and Bendix recommendations that were formulated as a result of discussions with personnel at the various machine manufacturers and underground coal mines that we surveyed, discussions with G. L. Judy (our consultant), etc:

Jan 1, 1974