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By T. G. Carnahan

The Bureau of Mines conducted research to simulate in situ leaching of a porphyry copper sulfide ore. The purpose was to determine the effects on copper leaching of additions of NaCI to a conventional sulfate leach system and to analyze the oxidant requirements and the oxidation products that resulted from leaching of the sulfide minerals in the ore. Baseline sulfate and sulfate plus 2-pct-NaCl-leach-solution experiments employing 167-kg (367-lb) and 152-kg (333-lb) charges, respectively, were conducted. The minus 25.4-cm (10-inch) ore was leached at 90° C under flooded conditions with 2.8 MPa (400 psig) of oxygen bubbling through the system. Sixty-seven pct of the copper was extracted in 1,236 days of leaching in the NaCI experiment, whereas 47 pct of the copper was extracted in 913 days of leaching in the baseline experiment. Diffusion into and out of the ore fragments controlled the rate of leaching, which precluded enhancement of the leach rate by the chloride ions. The calculated oxygen consumption was 3.17 kg/kg of copper extracted in the baseline experiment and 3.46 kg/kg of copper extracted in the experiment to determine the effect of chloride ions.

Jan 1, 1982

By W. F. Hughes

The thermodynamics of an electromagnetic field-fluid interaction system is discussed. A review of the thermodynamics of linear media (the permittivity and permeability taken as functions of density and temperature) is presented; then an extension is made to nonlinear media (the permittivity and permeability taken as functions of the fields). Expressions for thermodynamic properties and reversible work are derived and the first law of thermodynamics for magnetohydrodynamic flow is discussed.

Jan 1, 1968

Provide an instrument for continuous remote monitoring of carbon monoxide concentration in underground mines. Approach A carbon monoxide fixed? point continuous monitor consists of two modules. A line-powered control module is designed to power a remote transducer module; provide continuous readouts, visual and audible alarms, operational checks; and activate fans and equipment shutdown circuits if preset CO concentration levels are exceeded. How It Works The control module must be used in conjunction with a single transducer module. Developed under contract. the control module is a wall-mounted Instrument which contains a readout and alarm capability and power supply

Jan 1, 1981

By B. J. Scheiner

Silver ores from the Candelaria District, Nevada, and Round Mountain District, Colorado, were investigated mineralogically and metallurgically. Silver minerals of four distinct groups were identified: (1) silver sulfide; (2) argentojarosite; (3) silver contained in the iron oxide; and (4) manganese carbonate-oxide minerals, Electrooxidation and acid-chloride leaching techniques were investigated as means of altering silver minerals, and their effects on subsequent silver extraction were determined. Application of the knowledge obtained from mineral leaching studies resulted in development of a sulfur dioxide-sodium chloride leaching sequence for extracting silver from these types of ores. Silver extractions of 80 to 85 percent were obtained by leaching the ores with a sulfurous acid-sodium chloride system. This was an increase of 9 to 61 percent silver extraction over that obtained by conventional cyanidation techniques.

Jan 1, 1973

By David Hoadley, Kenneth R. Maser, Ashok B. Boghani, James E. Billar, D. Randolph Berry, Mackenzie Burnett, Robert H. Trent

5. General Escapeway Requirements 5.1 Escape Routes Present escapeway regulations state "Every mine shall have two separate properly maintained escapeways to the surface which are so positioned that damage to one shall not lessen the effectiveness of the other, or a method of refuge shall be provided when only one opening to the surface is possible." "Escape routes shall be a. Inspected at regular intervals and maintained in safe, travellable condition, b. Marked with conspicuous and easily read direction signs that clearly indicate the ways of escape." "Application. "Regular" intervals means at intervals no greater than monthly where conditions are stable and oftener where conditions may change." "Designated escapeways inclined more than 30* from the horizontal shall be equipped with stairways, ladders, cleated walkways, or emergency hoisting facilities." As can be noted in present and proposed regulations there must be two separate properly maintained escapeways. In most operations, the escapeways will consist of one route that is the normal travelway used in day to day operations. The second route is usually a return airway through old work areas. Based on this generally accepted practice, we will designate the two types as primary and secondary.

Jan 1, 1976

Simplify the spraying of sealants onto coal mine roofs. Approach A nonclogging system in which dry-fed sealant is mixed with water down-stream of the spray nozzle, has been developed and tested. How It Works The two-channel nozzle of this spray discharges two separate flows, a mixture of air and dry sealant from a central cylinder, and an encircling spray of water from a concentrically mounted water ring (a ring-shaped manifold). Downstream of the nozzle, the water mixes with the air and sealant to form a wet sealant spray that adheres to mine surfaces with very little rebound. (See photograph.) Extensively modified commercial spray machines are used to feed the sealant to the spray nozzle smoothly, without raising dust. Plugging of the nozzle is practically eliminated by two self-cleaning design features of the nozzle. These are the air gap and the tapered bore of the cylinder, (See drawing.)

Jan 1, 1979

Continuously monitor air-borne radon daughters that are a hazard to underground miners. Approach A beta detector continuously counts beta activity collected on a filter paper to allow calculation of exposure in working level units. How It Works At each Site a constant flow pump draws mine air through a fiberglass filter located in front of a beta detector (pancake type Geiger Mueller tube), Radioactive particles (products of the radon 222 gas emanating from the mine walls) collect on the filter and decay, releasing alpha and beta particles as well as gamma rays. A portion of the beta particles penetrate the Geiger tube window and create electrical pulses in the tube. These pulses are then amplified and sent by a coaxial type or shielded electrical cable to a central monitor located some distance from a working level detector. At the central monitor incoming Signals are amplified and fed into two channels, (See the block

Jan 1, 1979

By P. G. Barnard

Losses of alloying metals in furnace flue dusts, grinding swarfs, and mill scale produced during the manufacture of stainless steel are substantial. About 25 million lb Cr, 8.7 million lb Ni, and 150,000 lb Mo and other critical metals can be made available annually for recycling by a process developed by the Bureau of Mines. Stainless steel wastes pelletized with a portland cement binder were reduced in a small electric-arc furnace by a two-stage process to produce a recyclable alloy containing Cr, Ni, Mn, and Fe. The initial reduction was with carbon; the second, with ferrosilicon. Results are compared with previously reported laboratory induction melting tests. A 2,000-lb demonstration test of the process in a commercial electric-arc furnace is also described. Data are also presented on three 1,500-lb tests made using various slag conditions in the electric-arc furnace. Recoveries up to 99 pct of the Fe, Cr, and Ni contents of stainless steel wastes were obtained in using the process.

Jan 1, 1977

Detemine the elastic properties and structural integrity of a rock mass in situ. Approach An acoustic device that transmits and receives high-frequency seismic waves between boreholes was designed, built, and field tested. How It Works The acoustic cross-borehole apparatus operates by sending a seismic wave from a transmitter in one borehole to a receiver in a second bore? hole which may be located as far as fifty feet away, depending on the wave transmission quality of the rock. By measuring the wave's travel time and the distance between boreholes, the acoustic velocity of the rock mass can be determined. Characteristics of the seismic wave arriving at the receiver (such as the wave velocity, amplitude, and frequency content) are related to the physical properties of the geologic media, as calcu-

Jan 1, 1982

By Robert R. Stein, Roy C. Bartholomae, William W. Aljoe

This Bureau of Mines report describes in detail the design and operation of a test apparatus for measuring the sound power levels of drills used by the mining industry. The two major components of the test apparatus are a computer-controlled automated drill test fixture (ADTF) and a large (45,000-ft3) reverberation chamber that houses the ADTF. Design specifications and performance capabilities of the ADTF and the reverberation room are given. Initial test results for three types of drills--a pneumatic percussion drill, a hydraulic percussion drill, and a pneumatic rotary drill--are given to illustrate the types of experiments that can be conducted with the test appartus.

By Robert C. Hickman

"INTRODUCTION The Big Four fault and the Sandy Creek fault, with several cross faults, traverse the Stalion-Curnel fluorspar prospect in a northeasterly direction. The Big Four mine, about three-quarters of a mile northeast of the prospect, is the only active mine in the immediate area.A resistivity survey was made of a portion of the prospect by the Division of Geophysical Exploration, Bureau of Mines, in May and June 1946. As a result of this survey, five holes were drilled by the Bureau of Mines during the period from October 8 to December 16, 1946. Two Longyear No. 12 Junior Straitline diamond drills were used for the work.ACKNOWLEDGMENTSIn its program of investigation of mineral deposits, the Bureau of Mines has as its primary objective more effective utilization of our mineral resources to the end that they make the greatest possible contribution to national security and economy. It is the policy of the Bureau to publish the facts developed by each project as soon as practicable after its conclusion. The Mining Division, Lowell B. Moon, chief, conducts preliminary examinations, does the actual investigative work, and prepares the final report. The Metallurgical Division, Oliver C. Ralston, chief, analyzes samples and makes beneficiation tests.The project was under the supervision of Mitchell H. Kline, chief, Raleigh Branch, Mining Division."

Mar 1, 1948

Provide an economic alternative to drill-blast excavation with the same ability to excavate openings of varied orientation, shape, and size. Approach Develop an efficient, adaptable, mechanical excavation machine that produces unconfined tensile failure in rock. How It Works A drill-split fragmentation machine that combines a drill and a unique splitter has been developed. The drill and splitter are mounted on a carriage that positions the splitter in a hole immediately after it is made by the drill. The splitter creates force loads that cause the rock to fragment, and the process is repeated for excavation. The unique splitter applies both radial and axial loads to the rock mass, which produces an excavation action comparable to pulling a plug. This excavation action distinguishes the radial-axial splitter from typical demolition splitters, which require a free surface parallel to the axis of the splitter toward which to break rock.

Jan 1, 1989

By W. M. Merritts, Charles Findlay, Stephen Krickovic

Methane emission rates were studied in a Pittsburgh coalbed mine in northern West Virginia. A fullface boring-type continuous miner, equipped with a methane monitor, was used in the development of a set of eight main headings, one side of which was near old workings; the other side abutted virgin coal. Two air splits ventilated the section. Air volumes and methane percentages were recorded, and time studies of the miner were made during five consecutive operating days, during which a complete cycle of mining the headings and one line of related breakthroughs was accomplished. Methane emission rates increased significantly as mining progressed from the side near old mine workings toward the virgin area, and generally increased with coal extract ion. Mining in the heading immediately adjacent to virgin coal was interrupted quite frequently, owing to excessive methane concentrations at the face, despite adequate air volumes and acceptable methane concentrations in the immediate return airway.

Aug 1, 1970

By Foster Fraas

A method is presented for the linear evaluation of adsorption data using the equations dC = Ae-rv dv and v = [jT] - q, where dC is the phase composition increment, v a calculated parameter, T the absolute temperature, and A, r, h, g, and q the constants. The value of v is calculated from the composition C for both the adsorption surface and the immersion phase. A plot of v for each phase on Cartesian coordinates results in straight line graphs. With temperature variation, a plot of v versus,[ ] also results in straight line graphs. The equations are applicable to electronic and salt equilibria.

Jan 1, 1962

By Thomas E. Marshall, Gerald L. Finfinger

The Bureau of Mines has developed a practical methodology for deter- mining occluded gas contents of domal rock salt samples. The method, which is portable and field worthy, provides results in 5 min or less and does not require a laboratory environment or specially trained personnel to obtain meaningful results. The results can be used to identify gas-enriched zones, and thus may aid mine operators in production planning or ventilation design. The test method is based on the relationship between gas content and the acoustic response of salt samples as they are dissolved in water. The relationship is defined by an equation, and the results are repeat- able. The equation was derived by testing a series of rock salt samples collected from domal salt mines in Louisiana.

Jan 1, 1987

By Ernest W. Loya

A method for preparing gravimetric primary standards of helium in the parts per trillion range has been developed by the Bureau of Mines. The standards are used to calibrate a specially modified mass spectrometer used in determining the abundance of helium-3 and helium-4 in geochemical samples and of helium-3 in isotopically purified helium-4. The desired gas standards are prepared in 5-kg metal cylinders filled to 1,800 psia. Relative errors of less than 1 pct have been attained in the parts per trillion range using a successive dilution technique.

Jan 1, 1982

By Thomas O. Llewellyn

Laboratory semicontinuous and continuous heavy liquid cyclone separation pilot plant tests were made to determine the feasibility of producing a high-grade kyanite concentrate from a kyanite-quartz rock sample from Graves Mountain, Ga. Use of a three-stage heavy liquid cyclone circuit demonstrated that a 96.4-to 99.0-percent kyanite concentrate could be obtained with recoveries of 95.5 to 96.7 percent. The test work showed that by steam stripping with 6.9 tons of steam per ton of ore and two stages of detergent scrubbing the residual TBE content of kyanite cyclone products was 0.22 pound per ton of ore.

Jan 1, 1971

Engineering controls for overburden drilling include dry dust collection systems, wet dust suppression systems, and enclosed cabs [Zimmer and Lueck 1986; Volkwein et al. 1979]. Proper maintenance of the dust suppression system is critically important for drills using dry dust suppression methods. Failure to rigorously maintain these systems will result in inadequate dust control. Acute silicosis has been reported in miners operating equipment that relies on dry dust suppression [NOSH 1992].

Jan 1, 1997

By A. W. Hall

A neutron meter was developed for monitoring the sulfur content of coal streams. Neutrons from 80 micrograms of californium-252 penetrate the coal, producing thermal neutrons that are captured by atoms of elements present in the coal. The excited atoms emit prompt gamma rays with energies characteristic of the capturing element. These gamma rays are detected with a 6-by 7-inch sodium iodide detector and processed by electronic equipment to produce a gamma ray energy spectrum of the elements. Tests of the meter at a commercial coal preparation plant showed that sulfur in moving coal can be determined to a precision of 0.05 percent sulfur within 2 minutes. Based on this report by the Bureau of Mines, reliability of the coal-handling system proved inadequate for long-term operation, however, and improvements are planned.

Jan 1, 1975

By W. F. Marshall

The Bureau of Mines conducted a series of experiments to determine the influence of exhaust rebreathing on emissions from various gasoline and diesel engines. Tests were conducted that simulated operation of engines in nonventilated spaces as well as in spaces with partially restricted ventilation. Results of these tests showed that exhaust rebreathing can have a marked effect on exhaust emissions and thus on the composition of the air in the working space. For the case of restricted ventilation, unacceptably high (greater than 50 ppm) levels of CO in the air of the working space resulted from exhaust rebreathing rates as low as 8 pct exhaust in the engine's intake. Operation in a nonventilated space resulted in highly critical CO levels (fatal in a few minutes) at times corresponding to 1 to 3 pounds of fuel consumed per 1,000 cu ft of space. Tests involving spaces of various sizes showed that volume of the air space [per se] is not important--the primary variable is fuel consumed per unit volume of air space.

Jan 1, 1973