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By Altair Vieira de Souza

O tântalo é um dos metais mais versáteis na engenharia, podendo ser utilizado desde tecnologias espaciais até a biomedicina. Isso incentiva o estudo de novas tecnologias de obtenção do metal a partir do óxido de tântalo (Ta2O5). Neste trabalho é apresentada uma nova rota de obtenção de tântalo metálico a partir da reação magnesiotérmica do óxido de tântalo, usando como ignição o plasma de hidrogênio. Propõe-se um método alternativo ao processo Hunter, que apesar de ser o mais utilizado, é lento, pouco eficaz na produção de grandes quantidades e gera rejeitos degradantes ao meio ambiente. Foram misturados pós de magnésio (Mg) e Ta2O5 em recipiente projetado para permitir o efeito de catodo oco, e então aquecidos a plasma até a temperatura de ignição. Os experimentos foram realizados variando a pressão de trabalho buscando a redução completa do Ta2O5. Os produtos resultantes desses processos foram analisados por equipamentos de difração de raios X. Os resultados mostram que é possível a obtenção de tântalo metálico (Ta) a partir da redução metalotérmica do óxido de tântalo (Ta2O5) usando como agente redutor o magnésio e o plasma de hidrogênio como agente de ignição. A redução completa do Ta2O5 é obtida com o uso de pressões de 4,5 e 5,0 Torr.

Oct 30, 2017

By Marília Silva Cavalcante, Filipe Brito Marinho de Barros, Suelen Silva Rocha, Jorge Luiz Valença Mariz

A seleção adequada da taxa de produção de um empreendimento mineiro tem influência direta na possibilidade de sucesso do projeto, assim como a definição do porte e quantidade de equipamentos empregados em sua operação influenciam a maximização do Valor Presente Líquido (VPL). Nesse processo, a análise de risco na variável de saída aliada à análise de sensibilidade fornece resultados mais consistentes, visto que considera os riscos e incertezas de um projeto ao longo de sua vida útil. Este estudo teve como objetivo analisar a operação em uma mina de agregados a partir da consideração de quatro diferentes conjuntos escavadeira-caminhões através do método do Valor Anual Uniforme Equivalente (VAUE), comparando-o com o método do VPL. Foram revistas as avaliações econômicas efetuadas em estudo anterior, no qual foi obtido o VPL e efetuadas as Análises de Risco e Sensibilidade em cada um dos cenários, e foi acrescida à análise a metodologia do VAUE, sendo esta também submetida à análise probabilística. Foi verificado o desempenho de cada escavadeira e seus correspondentes caminhões para diferentes taxas de produção em ambas as metodologias, permitindo concluir que, para um mesmo número de unidades de transporte e contanto que a taxa de produção requerida seja possível, quanto menor o porte do equipamento, mais econômico é o cenário. Por outro lado, quanto maior a taxa de produção do empreendimento, mais rentável este será.

Oct 3, 2019

By John Ross Middleton

Based upon 30 years+ experience in the Development, Implementation and Ongoing Support of Computer based Melt Shop Management Systems in about 40 plants in the UK, Europe and the USA, consideration of the overall facilities of a state of the art, comprehensive, Integrated Melt Shop System covering Melting and Secondary processes for all grades of steels and superalloys; the scope of functionality of these systems, covering Raw Materials and Consumables Procurement and Inventory Management, Laboratory Management, Melt Shop Scheduling, Furnace Charge and Additions Optimisation, Level 1.5 to Level 2.5 Materials Optimisation and Process Control Calculations, Process Data Recording, Management of Ladles, Furnace Bodies, Vessels and Moulds, Comprehensive Management Reporting and Integration with Corporate ERP Systems. The second section of the paper reviews the key ‘Success Factors’ to achieve rapid, successful implementation, comprehensive, fast response user support, continuing system improvement and maintaining ‘perfect fit’ of system to operations in an ever changing future technical, operations and business environment.

Jul 29, 2018

By Nigel Marx

In order to understand (and ultimately to predict) the friction reduction resulting from the use of polymer solutions, the rheological properties of model polymer solutions have been measured over a wide range of shear rates. Both temporary and permanent shear thinning have been observed. By using base fluids of different viscosities it has been shown that permanent shear thinning depends more closely on the shear stress experienced by the fluid than on the strain rate. Hydrodynamic measurements have been made on the polymer solutions using a compliant ball on flat lubricated contact that operates in isoviscous-elastic conditions. The measured friction values can only be predicted with reasonable accuracy if the measured shear thinning properties of the lubricant are taken into account in the hydrodynamic model.

Jul 31, 2018

By Leonardo Camilo dos Reis, Edmilson Fernandes Dadomi, Claudio Silva de Paulo

In the hot strip mill production, one of the factors that may affect the productivity is the occurrence of failure due to the geometry of the strip at the exit of the rolling mill, because the tip of the strip can turn-down or turn-up. This study had the objective of evaluating the behavior of the strip when leaving the working rolls, through numerical simulation, aiming to know the influences of the main variables that govern the formation of the turn-down. The methodology consisted in performing the computational simulation of the strip mill and to vary the operational and geometric parameters that could influence the process. The results showed that the rolling of hot strips of HSLA material with final thickness varying between of 3 to 6 mm and a reduction of 6.6% to 11.0% in the last stand of a hot strip mill, tends to bend towards the roll with larger diameter, higher friction coefficient , higher temperature and lower limit of material flow. It was observed that the variation in diameter is the main factor that contributes to the formation of the curvature of the front-end of strip. Based on these results, several measures were implemented in the industrial line, with a significant reduction in the occurrence of turn-down.

Oct 2, 2019

By Franz Reufer

At Rogesa in Dillingen, Germany, a joint venture company of AG der Dillinger Hüttenwerke and Saarstahl AG and at Salzgitter Flachstahl GmbH in Salzgitter the sinterplants are equipped with the Paul Wurth EFA™ process for the final sinterplant off-gas cleaning. In Dillingen two and in Salzgitter one EFA™ plant are in operation at the respective sinterplants to comply with the very stringent environmental rules prevailing in Germany according to the German Clean Air Act called “TA Luft”. The main target is to eliminate or reduce emissions like dust, sulfur components, dioxins/furans and others in the sinter process off-gas. Since 2006 and 2011 the two EFA™ plant are in operation at Rogesa while the EFA™ plant in Salzgitter was also commissioned in 2011. These installations significantly contribute to the improvement of the emission situation of the Dillingen and Salzgitter Works. The EFA™ technology is the state-of-the-art process for such kind of application in terms of additive and energy consumption, reliability and availability. The report gives an overview of the EFA™ process and the performance results of the Dillingen and Salzgitter plant.

Aug 1, 2018

By Zou Zhongpping

Under the new normal state, blast furnace outputneeds to be adapted to the market demand, however the limitation in blast furnace output has significant impact on blast furnace operation and is prone to cause inactive furnace hearth and higher fuel ratio. To address such problems, some practices to maintain stable and smooth operation of blast furnace in case of output limitation are proposed based on data analysis philosophy, which allows the blast flow and hence the top pressure to be determined based on the hot metal output, and adequate kinetic energy of blast supply can be assured by adjusting the tuyeres. Matching between the oxygen enrichment and the pulverized coal injection is also proposed based on theoretical flametemperature, and burden distribution cycle calculation method is proposed, whichoffersnew approach for analyzing the change in burden distribution pattern.

Oct 30, 2017

By Pedro Jorge Walburga Keglevich de Buzin

The steel production in mini mills generates several process residues, among them the electric arc furnace dust (EAFD). This residue has as main elements Fe, O, and Zn, being classified as hazardous by the presence of Pb and Cd. In recent years, a rise in the chlorine content of this residue was observed, motivated by the increased use of scrap with impurities bearing this element. In this work, a qualitative assessment of the presence of chlorine in the electric steelmaking process is made. Complementing it, theoretical considerations based on the computational thermodynamics tool FactSage show the effects of the chlorine on the mineral species in EAFD and on gaseous species in the gas phase (HCl and Cl2). For this study, PVC polymer was used as the chlorine carrier substance which contaminates the EAF charge; presence of other minor elements in the system such as K, Na and Pb were also considered.

Aug 7, 2018

By Stefan Stein, Jorge Davo, Adrian Villanueva, Abhay Kulkarni, Shane Hoff

Pellet sizing plays a key role in the productivity of the entire pelletization and subsequent induration processes, whereas uneven pellet sizing can increase the circulating load of the balling circuit inducing operational instability leading to production loses. The present work focuses in comparing the agglomeration kinetics, expressed as the number of pellets produced in a determined target size range, of different organic binder-bentonite binder systems. The batch experimental results show that the binder system has a great influence in the resulting pellet sizing, which could lead to advantages in terms of balling circuit efficiency and eventually operational de-bottlenecking.

Oct 1, 2019

By Matteo Tomba

Today’s steel market is characterised by high competitiveness and tight profit margins; therefore, the operational costs of rolling mills must be as low as possible, while ensuring a final product of the highest quality standards. PERT SRL is an engineering company with a long-term experience in the international steel market, specialised in the design and supply of highly innovative and bespoke solutions for siderurgical and environmental plants. Because of its strong commitment to deliver excellent products and services, and its ability to innovate and adapt to the fastchanging market requirements, PERT has studied a new generation of BI-SUPPORT rolling stands, designed to be used in rolling mill plants for the production of rebars, rounds and sections in special quality bars (SBQ) steel grade, wire rod, light and medium section, suitable also for special steel plants. This paper will provide a deep insight into the key technical and economic features that have revolutionised the rolling technology for long products, such as the absence of spindles and piping on board, the considerably reduced number of spare parts required, a ring gap regulation system, and the compact dimensions, which lead to significant savings in investments and production costs; at the same time, the BI-SUPPORT stands guarantee excellent standards to the final product, an increase in plant productivity and a general improvement in the plant management.

Aug 16, 2017

By Delio Amorim

Industry 4.0 concepts is the new biggest challenge on the industry nowadays and every company in every industry in every part of the globe is looking to implement this somehow on their factories and machines. To do that on the newest long rolling mills, that brings already onboard state-of-the-art technologies, is for sure a challenge of machinery builder industry, but how to become the long rolling mills built on 70’s, 80’s or 90’s part of this innovation process and connected to the new trends? This is the main mission here, to show some examples of applications that goes in this direction.

Oct 1, 2019

By Bi Zongyue, ZhangYongqing, NiuTao, Guo Aimin

Over the past twenty years, significant advances have been made in the field of microalloying steels and associated applications, among which one of the most successful application cases is development and application of heavy-gauge X80 coil with high temperature processing HTP practice used for China's Second West-East pipeline, the longest X80 pipe in the world. During this process, HTP design concept has been sucessfully applied to develop 18.4mm X80 coil with demanding low-temperature fracture toughness requirements. In the meanwhile, China's metallurgical workers have further optimized HTP design concept with the aid of powerful rolling mill and coiling equipment, and made it possible to develop 21.4mm X80 coil used for Russia-China East line. In the paper, we would simply review the development history of high-strength pipeline steels, and then give more priority to the fundamental points for sucessful development of 18.4mm X80 coil and SSAW pipe, which paved the way for subsequent development of 21.4mm X80 coil and SSAW pipe. Finally, we would present the test results of mass production and burst tests, and dispel the suspicion that SSAW pipes made of X80 coil are more qualified to resist ductile fracture.

Oct 1, 2019

By J. N. Stevens, M. Tulwin, P. J. Lawlor

All metals producers are on an unending search for a competitive advantage. They need to produce in the most cost effective way. Sometimes a new mill might be considered but in this paper we present examples of how this might not always be necessary. A detailed investigation by an equipment vendor who can consider the mill and or plant as a complete entity: mechanics, automation and process control can often find solutions that are both lower cost and can be implemented in shorter time frames.

Oct 1, 2019

By Patrick E. Connell

During the ABM Conference of 2015 the latest design and process features of the new 3-roll RSB® generation were presented together with a unique Size Control System SCS® for a real time closed loop control to produce an extraordinary quality SBQ – day in, day out. In the past two years, Kocks has focused on improving the repeatability of the rolling process and developed technology to enhance the performance of its equipment. These developments include Fast Remote Control (FRC), Stands Adjustable Under Load (AUL) implementation of closed loop Size Control System (SCS), and finally a state of the art laser Gauge (4D Eagle) that pulls all of these developments into a complete package of quality. Gauges used in the past generally operated with the “shadow” measuring system. The latest gauge developments are based on the “light section” method. This method is more suitable to provide real time measurement parameters of the rolled bar. Placed close to the last rolling stand, the “light section” gauge is capable of measuring around the complete diameter with a clear definition of the bar stage in relation to the axes of the rolls. It is also capable of making these measurements using a very high measurement frequency. Following requirements of the market, requiring the highest gauge measuring frequencies which display the bar in the most accurate way even at the highest rolling speeds, the “4D Eagle” gauge was developed. This paper describes all the process features and parameters of this impressive and unique newly developed gauge as well as the other described technical improvements.

Oct 30, 2017

By Samanta Neves da Silva

Depósitos estratiformes são característicos por apresentarem irregularidades nos contatos entre minério e estéril, motivo que requer especial atenção no planejamento de lavra. No depósito de Bauxita em estudo, a definição da geometria da camada de minério é realizada por interpretação dos furos de sondagens com espaçamento médio de 200 metros. O modelo gerado dos contatos litológicos, comumente, não incorpora as oscilações em curtas distâncias das elevações (Z) entre furos, o que influencia na fase de modelamento geológico, logo, na previsão dos fatores de diluição e perdas de minério. Este trabalho propõe agregar dados de curta distância, aumentando as informações entre furos de sondagens e, a partir das medidas de cota no topo e base da camada de minério, melhor refletir a geometria do corpo de minério. Assim a metodologia se divide em: criar modelos de superfícies interpoladas irregulares de topo (SIT) e base (SIB), considerando as informações de curta distância; analisar elevações médias em cada superfície, a fim de pressupor superfícies planas de lavra no topo (SPT) e na base (SPB); verificar a amplitude entre essas superfícies - SITxSPT e SIBxSPB, mensurando os fatores de perdas e diluições de minério a partir da diferença entre as elevações. O produto final deste trabalho consistiu da quantificação dos fatores de diluição e perdas de minério, aplicadas ao planejamento de lavra de curto prazo, otimizando o aproveitamento dos recursos e, consequentemente, aumentando a vida útil da mina.

Aug 8, 2018

By Antônio Donizetti Giuliano, Fernando Codelo Nascimento, Viviane Tavares de Moraes, Cilene Cláudia Diógenes, Erivan Cardoso Rocha

Nos lagos ornamentais geralmente tem-se a dificuldade em controlar o crescimento de algas, pois existe a incidência de luz e a disponibilidade de nutrientes provenientes da ração fornecida aos peixes, os quais propiciam o crescimento e o desenvolvimento das algas. Uma alternativa de tratamento é o processo oxidativo avançado (POA) existente, a ozonização, com o objetivo de propor um processo de tratamento de água para controlar a proliferação de algas em um lago ornamental sem prejuízos à comunidade aquática, vivente no lago. A metodologia utilizada foi o estudo de caso do lago que envolveu as seguintes etapas: construção do lago ornamental; definição do sistema de tratamento; monitoramento de parâmetros como: a demanda bioquímica de oxigênio (DBO), a cor, o pH, a temperatura, a amônia (NH3) e o oxigênio dissolvido (OD) do lago durante três meses; aplicação do ozônio para controlar a proliferação de algas e monitoramento dos mesmos parâmetros durante o processo de ozonização. Dentre os principais resultados encontrados citam-se: a redução de 170 unidades de Cobalto platina (PCU) da cor esverdeada da água do lago; descimento de 60% da DBO; aumento de 16% da concentração de OD e a redução de 80 a 100% da concentração de NH3, eliminando assim odores desagradáveis e melhorando a qualidade da água. Por meio dos resultados obtidos conclui-se a aplicação de ozônio em lagos ornamentais é uma alternativa para a manutenção aquática e melhoria da qualidade da água..

Oct 2, 2019

By Tiago Ribeiro Costa

A Praxair é uma das três maiores empresas de gases industriais do mundo, com atuação em mais de 40 países e fortemente atuante na indústria siderúrgica. A Praxair possui experiência para fornecer produtos e serviços para todos os tipos de siderúrgica. Diversas tecnologias desenvolvidas pela Empresa, como o CoJet® (sistema para injeção de jato coerente de oxigênio em fornos elétricos e conversores), Slag Splashing (espalhamento de escória nas paredes de conversores, aumentando a vida útil dos refratários), AOD (processo para produção de aços especiais) e outros, encontram-se em operação comercial atualmente em diferentes partes do mundo. No Brasil, a PRAXAIR é a controladora da White Martins, maior empresa de gases industriais da América do Sul, presente em nove países do continente. Seu portfólio inclui gases atmosféricos, produção de gás carbônico, acetileno, hidrogênio, gases especiais e medicinais, misturas para soldagem, cilindros de aço sem costura, equipamentos para aplicação, transporte e armazenamento de gases. A empresa também opera uma unidade para liquefação de gás natural. Além de tecnologias e processos, a White Martins também pode fornecer soluções e equipamentos para medição, controle e injeção de gases, atendendo às rígidas normas de segurança e padrões de qualidade. O Objetivo deste trabalho é apresentar e discutir sobre a solução para o fornecimento de mistura para atmosfera de fornos de tratamento térmico através de um painel misturador de gases hidrogênio e nitrogênio. Será discutida a operação do equipamento e abordadas às características construtivas.

Jul 31, 2018

By Luiz Flávio Pereira Costa

O espessamento de lamas no processo de beneficiamento de minério de ferro é de fundamental importância para a recuperação de água de processo, pois 75% da água é recuperada nesta etapa. Além disso, a qualidade da mesma interfere diretamente no bom desempenho das demais etapas do processo, principalmente na etapa de flotação. Vários são os parâmetros que interferem para obtenção da clarificação ideal do overflow, como: pH, dosagem de coagulantes e floculantes, percentagem de sólidos na alimentação, etc. O pH pode ser considerado o mais importante, pois a partir dele é que se determina as dosagens de coagulante e floculante referentes ao ponto ótimo de coagulação reduzindo assim os efeitos negativos na etapa de flotação. O teste de sedimentação em proveta é uma forma simples e rápida de realizar uma análise da velocidade de sedimentação e clarificação da água frente a diferentes combinações dos parâmetros citados. A Samarco resgatou e implementou na rotina dos operadores da área de espessamento a realização de testes de sedimentação em proveta com o objetivo de reduzir o tempo decorrente de coleta de material, envio ao laboratório e espera pelos resultados. Após a implementação dos testes na rotina operacional, observou-se motivação da equipe em redução de custos, embasamento teórico e assertividade na tomada de ações, diminuição de incidência de eventos de má clarificação da água overflow e diminuição do consumo de floculante em cerca de 30%.

Aug 16, 2017

By Fábio Dian Murari, Antônio Adel dos Santos

The effect of reheating temperature of slabs on the precipitates dissolution and mechanical properties of Ti-Nb microalloyed steel was investigated in pilot scale. It was verified, by means of transmission electron microscopy, a significant decrease in precipitates formed during the solidification of the steel as the reheating temperature increased from 1100°C to 1200°C. No significant changes in size and shape of the precipitates were observed with further temperature increase up to 1280°C. In line with the precipitates dissolution behavior, an increase in strength was observed with the elevation of the reheating temperature up to 1200°C, due in part to the reprecipitation of fine Nb-rich precipitates during the hot rolling. At 1200°C the presence of deformed ferrite on the microstructure contributed to the additional increase in strength. After reheating above 1200°C up to 1280°C, a decrease in strength of the rolled plates was noticed. This effect has been credited to the absence of deformed ferrite grains and also to a small increase in the low angle grain boundaries size. The results were in agreement with Thermo-Calc and Dictra simulations.

Oct 1, 2019

By Davidson Marcos de Oliveira, Antonio Adel dos Santos, Vicente Tadeu Buono

The benefits of using the controlled rolling process followed by accelerated cooling (TMCP), currently used in the main rolling mills in the world are already well known and metallurgically based. The need to obtain mechanical properties with a high degree of homogeneity means that in some situations the ends of the rolled material are discarded, negatively affecting the metallic yield of the process. Therefore, this work focused on the determination of the mechanical properties variation at the ends of thick plates processed by TMCP of steels for application in oil and gas pipelines, in order to map the extent of these differences and to correlate them with the microstructure obtained, the profiles of temperature and cooling rates in these regions. To perform the work, two slabs of the studied material were rolled, and the temperature profile was recorded along the plate in the controlled rolling and accelerated cooling processes. The ends of the material were sampled in sections at every 100 mm and subjected to tensile test, hardness and the Charpy V-notch impact test, as well as dilatometry and microstructure evaluations. For the used process conditions, the results indicated the formation of a banded microstructure, basically consisting of polygonal ferrite and bainite, occasionally containing small fractions of perlite. The mechanical properties in the top and the base were higher than the values found in the plate middle, justified by the microstructure found. The work allowed understanding the relationship between the mechanical properties, microstructures and process conditions at the ends, helping the team to improve the process in order to result in a high degree of homogeneity of the product and, thus, lead to optimization of the metallic yield.

Oct 1, 2019