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By D. Harrington

Near the close of the nineteenth century electricity was introduced underground, and the mining industry automatically was confronted with another potential source of fatalities and injuries to mine workers. Electricity has become an increasingly vital factor in the production of goal, particularly in recent years, because of the greatly extended mechanization that has taken place underground. The enlarged use of electrical equipment for cutting, loading, and hauling coal unquestionably increased the potentiality of shock and explosion hazards underground. Electricity may be used in coal mines with minimum danger if electric equipment and power-carrying wires are chosen properly and installed and kept protected by proper safeguards; on the other hand, if vigilance is relaxed in the slightest degree accidents may result. Electrical accidents are caused chiefly by direct contact with electrical equipment or power-carrying wires, by ignition of explosive gas or dust, and by fires of electrical origin. Electricity now ranks fourth as a cause of coal-mine fatalities, not including deaths from explosions or fires of electrical origin.

Jan 1, 1936

By D. J. Singleton

Erosion corrosion of 12 alloys in phosphoric acid waste water was studied by the Bureau of Mines. Tests were conducted on oblate spheroids or cylindrical specimens in 12-and 60-cm-diam ball mills by grinding phosphate rock in gypsum pond water with a starting pH of 1.6. For comparison, tests were conducted while grinding phosphate rock in plain water. Static corrosion tests in gypsum pond water also were conducted. For all alloys, the wear by erosion-corrosion (milling with gypsum pond water) was greater than the sum of erosion (milling with water) plus static corrosion. Erosion-corrosion wear was about 1,500 to 3,000 mpy for the alloyed white cast irons, 1,000 to 1,400 mpy for commercial steel ball material and type 316 stainless steel, and 600 to 900 mpy for nickel-base alloys and a high-manganese, nitrided stainless steel. Alloy costs per unit of phosphate rock 'processed favor a low-alloy, high-carbon steel or a high-manganese, nitrided stainless steel.

Jan 1, 1985

By Constantine C. Popoff

This report reviews and analyzes, by a simple analytical and logical reasoning, the conventional methods of reserve computations of mineral deposits described in various domestic and foreign publications. It brings together, formulates, and evaluates the principles underlying interpretation of exploration data; and ties such principles to the proposed classification of methods. The material is discussed in sufficient detail to allow general application.

Jan 1, 1966

By C. T. Anderson

In July 1947, the U. S. Bureau of Mines, in cooperation with the Air Materiel Command, started an investigation of zirconium alloys with the object of determining the suitability of such alloys for high-temperature applications. This report covers the preliminary study of about 25 zirconium-rich alloy systems with respect to preparation, fabrication, tensile properties, metallographic structures; constitution, and heat resistance. Obviously, each system could not be investigated thoroughly, and this publication can be regarded only as a first approach. The more promising individual alloy systems will be studied in greater detail and reported in subsequent publications. The study of zirconium alloys on such a scale has been made possible by the U.S. Bureau of Mines developments in the past 5 years On producing zirconium metal. This basic process is similar to that developed by Kroll for producing ductile titanium metal and consists essentially of reducing zirconium chloride by means of molten magnesium. The Northwest Electrodevelopment Laboratory at Albany, Oreg., has produced several thousand pounds of ductile metal in this manner and has a pilot plant producing over 300 pounds of metal per week. Alloys were prepared by melting Bureau of Mines zirconium and the best available grade of alloying element in graphite, with suitable provisions for preventing oxidation. The ingots were quartered longitudinally and sheath-swaged at 850° c. to 3/8-inch diameter rod. Two of those rods were send to Wright Field for room-temperature and 1,200° F. tensile properties. The remaining two sections were used for metallographic, hardness, heat-treatment, and heat-resistance studies. The salient features of this investigation are summarized in table 1.

Jan 1, 1950

[~lis is the f'fth in a ~erieG of reports on properties of commercial motor fuels, made in accordance 1,'Vi t:h fl cooperative ae,ree-ment betwGon tho Cooperative Fuel ReRRarch (e.F.R.) Committee and the Bureau of I ines of the Dcpart~ent nf the Interior. The first report gave data on motor r-asolino~ sold during the wintor of 935-36.31 Thi~ report covers 84 brands of ga~oline represented by l,722 samples exclurling the Pacific Coast. T 3)Se J.rom th~. ?~'tcific Coast IV .ro avnrL)f:od b~r tho Pacific Coa!3t tecilnical group "bofore o8ing submi ttcd ruld arc p~.lbl:'shcd GX Gtl~r as they were submi tted. In some areas r~lJort~ . erc roceivod f~om ~ ix to eicht compD.l1ie~ on the same brands of gasoline. whoruar. in other areas only one company reported on a brond. Thut., it CU .. "! be senn that BO .. 0 uf the dnt ;.U'e more rCY>l'c entat vc thM others. The inclusion of r~0rts fro:n several ci tie. w' thin somo of tho di stricts has ir.rpr,)vcd the report by reducinc; tr.e numb~r of brand rcportel by only ono company. ]

Jan 1, 1938

[~lis is the f'fth in a ~erieG of reports on properties of commercial motor fuels, made in accordance 1,'Vi t:h fl cooperative ae,ree-ment betwGon tho Cooperative Fuel ReRRarch (e.F.R.) Committee and the Bureau of I ines of the Dcpart~ent nf the Interior. The first report gave data on motor r-asolino~ sold during the wintor of 935-36.31 Thi~ report covers 84 brands of ga~oline represented by l,722 samples exclurling the Pacific Coast. T 3)Se J.rom th~. ?~'tcific Coast IV .ro avnrL)f:od b~r tho Pacific Coa!3t tecilnical group "bofore o8ing submi ttcd ruld arc p~.lbl:'shcd GX Gtl~r as they were submi tted. In some areas r~lJort~ . erc roceivod f~om ~ ix to eicht compD.l1ie~ on the same brands of gasoline. whoruar. in other areas only one company reported on a brond. Thut., it CU .. "! be senn that BO .. 0 uf the dnt ;.U'e more rCY>l'c entat vc thM others. The inclusion of r~0rts fro:n several ci tie. w' thin somo of tho di stricts has ir.rpr,)vcd the report by reducinc; tr.e numb~r of brand rcportel by only ono company.]

Jan 1, 1938

By Jr. Reed

Cassiterite was discovered in Coosa County, Ala. in 1880 by Judge John S. Bentley. Since that time intensive surface prospecting has revealed the presence of cassiterite in pegmatite bodies that occur in a zone about 20 miles long and 3 miles wide. Numerous trenches and test pits and several shafts were sunk, and one attempt was made to nine and concentrate the cassiterite commercially. The problem of a domestic tin industry and the question of the extent of the Alabama tin deposits have long been of public interest and concern. The deposits have been examined by numerous geologists and several governmental agencies, including the Geological Survey of Alabama, the Geological Survey and the Bureau of, Mines. of the Department of Interior, and others. The Bureau of Mines and the owners of the properties, Charles A. Dean and Robert A. Russell, investigated the Coosa County tin deposits under a cooperative agreement from October 1, 1948, to June 10, 1949. Sixteen hand trenches totaling 527 linear feet and 33 machine trenches totaling 6,780 linear feet were dug. Two shafts wore sunk for a total of 72 feet, and 44.4 feet of drifting was done. Thirty-one diamond-drill holes totaling 2,776 feet were drilled.. Four hundred thirty samples, representing 1,192.6 linear feet, were taken for assay and wore analyzed by the Southern Experiment Station at Tuscaloosa, Ala.

Jan 1, 1950

By Donald W. Ross

Petroleum oils of widely different grades have long been clarified or decolorized by contact with fuller's earths. More recently, so-called activated clays have also been used for this purpose. Still more recently ouch clays have been used in the form of nodules termed "catalytic pellets." Clays of varied appearance and from different localities possess the desired bleaching qualities, but evaluation of such clays, so useful to the oil industry, has not been simple. Previous methods of identification and evaluation have largely followed procedures of production methods and were not primarily based upon the fundamental properties of the clays. Thus) a false assumption has grown up that) bleaching clays probably have no common properties on which a-method of comparison can be based. Fuller's earths and activated clays have a large absorptive capacity for the color constituents of petroleum and its products decolorizing is accomplished by bringing the oil into intimate contact with the clay and later separating the decolorized oil from the clay with its load of absorbed coloring matter. Former practice in absorbing "color" was to use the clay as granules or In' powdered form. More recent practice is to use clay pellets that are more abrasion-resistant than the granules. The oil is either filtered through a bed of clay, percolation method, or agitated on contact with the clay, contact method. Viscous oils are decolorized at an elevated temperature, so that their viscosity is lowered to the point at which thorough contact with the clay is insured. Nonhumidifying, nonoxidizing gas, such as dry steam or dry nitrogen, is used to seal such hot oil masses from the atmosphere.

Jan 1, 1948

By T. F. Curry, L. B. Berger, H. A. Watson, S. J. Pearce

The conduct of work at elevated air pressures , such as in caissons and in tunnel - driving in subaqueous strata , poses safety problems not encountered in mining and tunneling operations at ordinary atmospheric pressure . This publication discusses some of the problems involved and presents information on the following subjects : ( 1 ) Physiological effects of gases at elevated pressure . ( 2 ) Use of respiratory protective equipment in rescue or recovery operations in event of fire or other emergency in pressurized tunnels . ( 3 ) Effect of elevated pressure on performance of some gasdetecting instruments ; interpretation of the results . Various types of respiratory protective devices are discussed in relation to their possible use at elevated pressures , especially the 2 - hour , selfcontained , recirculating - oxygen - breathing apparatus , which has had wide use in the United States during rescue and recovery work in the mining industry . A modified procedure that eliminates the hazard of oxygen poisoning enabling the safe use of this apparatus at elevated pressures , up to 45 pounds per square inch , gage , and tests to verify its practicability are described . procedure involves control of the partial pressure of oxygen in the breathing

Jan 1, 1964

By R. L. Brown

This report, the seventeenth in an annual series, summarizes Bureau of Mines research and technologic work on coal and related investigations for July 1, 1951, to July 1, 1952. It 1s based largely on publications issued during the fiscal year, although 10 some instances data are presented that have not been published previously. Footnote references are given to the publications so that further details on the work may be obtained. Bureau of Mines research on the mining, preparation, and utilization of coal is directed toward developing and encouraging safer and more efficient mining practices and preparing and utilizing coals to the best advantage.

Jan 1, 1953

By M. J. Sheridan

"INTRODUCTION In December 1942, the-Bureau of Mines reported favorably on a proposal to grant Government assistance-in constructing an access road (consisting principally of a timber-pile bridge across the Rio Grande at Hot Springs, N. Mex.) to the property under lease to the United States Fluorspar Co. At that time the property was being developed actively, and there appeared to be no immediate-need for exploratory or metallurgical assistance by the Bureau of Mines.Because milling facilities were inadequate; the access-read project was eventually disapproved, but prior to disapproval the company had discontinued operations. In June 1943, exploration was resumed by the Humphreys Gold Corporation of Denver, which had subleased the property. Difficulty of access continued to interfere with exploratory progress. In July 1945, at the request of the lessee, the Bureau of Mines directed sampling, using company employees.At the completion of this sampling program, the Bureau of Mines concluded that the property was potentially a important source of fluorite but that further development for production appeared to depend largely on the establishment, by exploration, of adequate reserves. Because of the relatively easy position-of metallurgical-grade concentrate and ores, it also was deemed advisable to investigate the possibility of producing acid-grade concentrate from the ore, for which a demand was becoming evident. Accordingly, a program of trenching, diamond drilling, and metallurgical testing was undertaken by the Bureau. The results of its investigation are reported herein."

Feb 1, 1947

By H. A. Doerner

Tellurium is a silver white solid with metallic luster, the e17atal.line torm being ver., brittle aud e.g,s!ly powdered. It has a specific gravity of 6,27, melta at 45a0c. and boils at red het, giving off a. golden 1ellow vapor when air 11 excludei. When heated in air, telluri'UiD burns with a bl\te name tinged with green, and evolves wh1 te vapors ot tellurium dioxide. An amorphous form of tel­lurium, obtained by red.uction and precipi ta.tion from so).ution, haa II specific gr1.vity ot 6,015, and when heated ia cho.nged to the cry:.,talline variety. Telluri,a 11 insoluble in water, c&rbon diaiJ.phido, or h;rd.rochl oric acids, but it 11 41a-1olved bJ nitric or concen t1·ated. sulphi.U·ic acid. It 1..oea not tamiah in moiet ah•• 11 ree11tant to alkaline solutions, e,;:ctpt concentrated KOB, but it 11 cliaaolvecl by tuaed. &lkl 1••. I ts 11.to!!lic weight h..'l.a been the "J.Ubject ot mch controverq, bu\ t.he value 137 .5 :.a bl!ten generally accepted, Tho chflmietr:, of tellurium ia eim1lar to that ot IUlphur. It tonne throo xid.ee TeO, To02, and Te0 , al10 tellur14ea, t•llurite,, and. tellur1.t11, A number of halide compoWld.1, a 3iulph1de, and. a .ulpbat.e are known.

Aug 1, 1922

By C. V. Davis

In the lnvestlg::ìt1on of mAthods for aSS8.7ing platin",. conducted by the Bureau ot MinAs, reoent experiments have d~velopad tha~ with ce..tain orei, especially when thr, quantity Of platinum 1s eonlidarablfl, nit'!le acid w111 not etfßct a iepard-Han of platinum and pa11adium. 'lhe following m;lthod has been found to be accurate and to reiu1 t in a complete S''lun''ation of' th~3:l metals. It is therefo 1" '!eeommei:ed that 1 t ba followed rath::r- than the method of separation with nitrio acid, givèn in Technical Pape'! 270.* At line 22, pagi 14, of that paper, bAglnnlng with ~tarm th,~ metals '.'ith dilute¡ nitrio acid," strikE out the rest of the paragraph, and substttutt~ the pro_t cedure g1 ven below. ?lunder and Thuringer.. have developed mnt¡iods for th"i sflparation of palladium from all the platinum metals exoept platinum bj m ,ans of dlmethy- 19lyoxlme. They state that the~ is no action for several hours if an excess of dimeth¡lglyoxime is added to an aqueous solution of ohloroplatinic acid in the cold, alio that only on boiling is the platinum pTecipi ated ¡~d than only PST't of the platinum i srenoved from the sUut1on. They found that palladium 1s p~ecipi tated quati tat! vely in the oold as (CaH 4N40 Pd) which is insoluble tn water, dilute hydroohlorio acid, dilute acetIc aofd or in 50~ ethyl alcbhol. All of their pT'90ipi tations we~p Carl". ied out ~hile the solutions were being heated. This caused a pal"tia~recipltation of the platinum along wi th the

May 1, 1922

By G. S. Scott

[The Duretiu of Kinen, as :) pr<r"Yof its :;encr:rL propan clealini: with the causes, behavior, n.ncl tor-trol of o1:t1?;.?cite-mine fires, hns investic:&apos;lte3 I varionr. Te:.nr, for Je tec tin:: iccj.r)ic:~ t he;, tint; :,:.zqdergro-.:rid and of <~e termining the trend of the hen tir..: once -I i&apos;i re j 7 knnm tr, he nrcsc~t.]

Jan 1, 1938

By G. S. Scott

[The Duretiu of Kinen, as :) pr<r"Yof its :;encr:rL propan clealini: with the causes, behavior, n.ncl tor-trol of o1:t1?;.?cite-mine fires, hns investic:&apos;lte3 I varionr. Te:.nr, for Je tec tin:: iccj.r)ic:~ t he;, tint; :,:.zqdergro-.:rid and of <~e termining the trend of the hen tir..: once -I i&apos;i re j 7 knnm tr, he nrcsc~t.]

Jan 1, 1938

By L. R. Burdick, J. F. Barkley

The inherent heating value or the amount of heat that will be produced when a coal is completely burned is measured in British thermal units (B. t. u.) per pound of coal . This standard heat unit is the quantity of heat required to raise the temperature of 1 pound of water 1 °F . at about 60 °F . The amount of inherent heat is determined by burning a small quantity of the coal in a heat meter or calorimeter , which gives results in British thermal units . The exact manner of making this test is standardized by the American Society for Testing Materials.4/ The value so determined is the total heat developed by complete burning, with all the products of combustion cooled down to the temperature of the calorimeter . The calorimeter is kept at about room temperature . This total heat is sometimes called the " high" or gross heat value , because it includes the latent heat given up by the water vapor in the products of combustion when the vapor condenses to water in the calorimeter . The heat as measured is reported as the heat of combustion at constant volume , since the burning is carried out in a tightly closed calorimeter chamber whose volume does not change . In actual use , coal is usually burned in an open - end chamber at constant pressure , generally somewhere near atmospheric . As the heat of combustion of coal at constant pressure is very slightly higher than the heat of combustion at constant volume , it might be considered that the heat at constant pressure should be used as the standard reference base . For an ordinary eastern coal the heat at constant pressure is about 16 B. t . u. per pound higher than the heat at constant volume . Calorimeter corrections , ordinarily not considered , that could have been subtracted from the heating value before reporting , may amount to about as much . Hence , the value reported is apt to be more nearly the true heating value at constant pressure than at constant volume .

Dec 1, 1941

By L. M. Burman

The phase-boundary pressure required to maintain a natural hydrocarbon fluid in a single phase must be considered in planning the recovery of reservoir liquids by miscible-phase processes. The change in the phase-boundary pressure at reservoir temperature that results when a light component or a mixture of light components is added to a reservoir fluid is an especially important consideration. The cricondenbar pressure (maximum phase-boundary pressure) and the critical pressure are unique correlated pressures that have been utilized to calculate the change in phase-boundary pressure that may result when the composition of a reservoir liquid is altered by an additive. In this study one reservoir oil and three gas-condensate fluids are used as examples. Correlations pertaining to the critical and cricondenbar states in chapters 4 and 5 of Bureau of Mines Monograph 10 (3)5 were used to demonstrate how butane and lighter components added to these reservoir fluids affect their phase-boundary pressures.

Jan 1, 1962

By E. R. Palowitch

This report is the result of a series of coal-cleaning tests using a dense-medium cone-type washer. Detailed results are given for 2 tests using a magnetite medium and 4 tests using a pulverized-refuse medium. Approximately 120 float-and-sink tests and over 500 separate chemical analyses were made in conjunction with these tests. In these tests higher recovery efficiencies and sharper separations were obtained when using a magnetite medium, especially on coal sizes below one-half inch. When sizes above 1 inch at low specific gravities of separation are cleaned, the pulverized refuse medium compared favorably with the magnetite medium.

Jan 1, 1956

By A. E. Back

[Several processes for recovering manganese from low-grade ores have been proposed3/4/5/ in which an aqueous slurry of the ore is leached with gas containing nitrogen, oxygen, and sulfur dioxide as obtained from burning sulfur or roasting sulfide ores. The manganese dioxide is dissolved, and most of the sulfur dioxide is oxidized to sulfate, but an appreciable quantity of dithionate is usually formed, together with acid from oxidation of the sulfur dioxide. The over-all reactions may be represented as follows: (1) Mn02 + S02 = Mn++ + S04--. (2) Mn02 + 2S02 = Mn++ +S206--. (3) H20 + So2 + 1/2 02 = 2H+ 5S4--. (4) H20 + 2S02 + 1/2 02 = 2H+ + S206---.]

Jan 1, 1952

By Jeffrey A. Aldinger

This U.S. Bureau of Mines report presents an analysis of surface coal mining accidents involving mobile equipment for the years 1989 through 1991. Mobile equipment is defined as haulage trucks, front-end loaders, bulldozers, scrapers, and road graders. These five pieces of mining equipment accounted for 20 pct of all surface coal mine accidents and 41 pct of the fatalities. The general discussion of these accidents covers the accident causes, the primary activity of the accident victims, and other contributing factors. A more detailed analysis of accidents associated with each piece of mobile equipment is also provided. This report will provide mine managers and mine safety personnel with a better understanding of the hazards associated with mobile mining equipment. It identifies where improvements in mobile equipment safety can be made and those areas requiring additional safety emphasis, such as safety training, work procedure changes, or engineering changes to the equipment or work environment. The analysis was performed by a team of researchers using accident data and narratives provided by the Mine Safety and Health Administration.

Jan 1, 1995