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By W. P. Yant

The widespread use of toluene in industry and the importance of air analysis in industrial-hygiene surveys have created a need for a simple and accurate method for determining toluene vapor in air. Most of the methods used to determine small quantities of toluene in liquid or vapor form are based on the measurement of its physical properties. Methods based on fractional distillation, determination of specific gravity, use of the interferometer, use of the spectrograph, and sorption on solid sorbents with subsequent determination of gain in weight have been employed. Distillation and specific-gravity methods are not applicable to the small quantities of toluene found in the air, and use of the interferometer, spectrograph, and sorption methods either are not specific for toluene in the presence of other volatile substances or require expensive equipment.

Jan 1, 1936

By F. R. Cattoir, R. E. Cumings

Columbium metal was electrorefined in a fused - salt electrolyte . Excellent results were obtained in lowering the impurity content in a 94 - percent columbium anode feed material to produce a 99.8- percent - pure metal . The reductions of the major impurities follow : Oxygen from 19,800 to 500 ppm , carbon from 9,700 to 25 ppm , iron from 9,200 to 630 ppm , nitrogen from 2,100 to 90 ppm , and silicon from 750 ppm to not detected . Columbium with a purity of 99.9 percent was produced from 99.5- and 99.8 - percent grades of columbium. The investigation was devoted to the evaluation of a fused - fluoride - salt electrolyte ( KF - NaF- K₂ CbF, ) for electrorefining columbium. The effects of the columbium concentration and the voltage upon the product's purity were investigated . The effect on the cathode current efficiency of ampere - hours of deposition and the formation of a dual valence state of the columbium was also investigated .

Jan 1, 1964

By John R. Bartels

Jan 1, 2009

By S. J. Broderick

[The term "nonmetallic minerals? as commonly used is the mining industry, refers to those minerals of industrial importance that are mined essentially for uses other than for the metals contained. The field comprises several hundred rod minerals of industrial importance, of which 70 have can adequately described in the textbook Industrial Minerals and Rocks. A few o f the more important nonmetallic products are sand and gravel, salt, phosphates, clays, refractories, limestone, and cement materials. Some of the minerals, such as bauxite and pyrolusive, have both metallic and nonmetallic applications, but in this report only the nonmetallic mineral phases are considered. In the organic field of nonmetallics only coal is considered, as, the others - petroleum, natural gas, natural bitumens, and hydrocarbons - are of no importance in water softening.]

Jan 1, 1941

By Thomas L. Chapman

The San Manuel is a deposit of low-grade disseminated copper ore. It was brought to the attention of the government in October 1942 through an application to the Reconstruction Finance Corporation for a development loan, supported by a report by Henry W. Nichols. Nichols' sampling of two outcrops containing copper silicate and his geologic map indicated that a minable body of copper ore might be developed. The Federal Geological Survey was requested to examine the property. The Survey mapped the geology in March 1943 and cut a few check samples, which substantially confirmed Nichols' sampling of the outcrops and a few shallow workings. The geologists of the Survey recommended some test drilling by the Bureau of Mines. The property was examined by the author and Wm. D. Hughes, associate engineer of the Bureau of Mines on March 22 and 26, 1943, and a preliminary drilling campaign was recommended. Five shallow churn-drill holes totaling 1,480 feet were put down under the supervision of Chas. A. Kumke, one of the Bureau's engineers, from November 23, 1943, to January 13, 1944. This work indicated that the deposit extended deeper than the 350-foot depth attained in the deepest hole and might have very considerable areal extent. Additional funds were allotted, and the drilling contract was extended twice to a final maximum of 17,000 feet with 2,000 feet maximum depth of hole. Drilling was continued by the Bureau of Mines until February 2, 1945, when 15,844 feet of hole had been drilled. The Magna Copper Co. took options on this and adjoining property in September 1944 and commenced drilling with two machines. It also engaged the two contract drills used by the Bureau after it stopped drilling. It exercised its options in August 1945 and organized the San Manuel Copper Corp. to operate the property. That company is continuing to explore the ore body with six churn drills. Thomas Lyon took options early in 1945 on holdings adjoining the San Manuel property on the east and is operating two churn drills. Exploration up to the completion of the last holes started by the Bureau of Mines indicated a block of ore 3,100 feet long, 400 to 800 feet wide, and 500 to 900 feet thick, and averaging about 0.8 percent copper. Subsequent drilling showed that the ore body extends considerably beyond this block. The axis of the ore body strikes about N. 61° E. Copper minerals are disseminated in hydrothermally altered quartz monzonite and monzonite porphyry. Ore outcrops in two small areas over the northeast part of the block. Elsewhere the copper-bearing rocks are capped by Gila conglomerate, which thickens toward the west and south. Drilling showed that the ore is in a thick, tabular body with a steep dip to the south. The ore body lies near the surface in the northeastern part of the block. The south side of the block is much farther below the surface than the north side. There the upper part of the copper-bearing rocks is lightly mineralized, so that the hanging wall of minable ore lies deeper than the base of the conglomerate cap, which thickens southward.

Aug 1, 1947

By Thoms L. Chapman

The San Manuel is a deposit of low-grade disseminated copper ore. It was brought to the attention of the government in October 1942 through an application to the Reconstruction Finance Corporation for a development loan, supported by a report by Henry W. Nichols. Nichols’ sampling of two outcrops containing copper silicate and his geologic map indicated that a minable body of copper ore might be developed. The Federal Geological Survey was requested to examine the property. The Survey mapped the geology in March 1943 and cut a few check samples, which substantially confirmed Nichols’ sampling of the outcrops and a few shallow workings. The geologists of the Survey recommended some test drilling by the Bureau of Mines. The property was examined by the author and W. D. Hughes, associate engineer of the Bureau of Mines on March 22 and 26, 1943, and a preliminary drilling campaign was recommended. Five shallow churn-drill holes totaling 1,480 feet were put down under the supervision of Chas. A. Kumke, one of the Bureau’s engineers, from November 23, 1943 to January 15, 1944. This work indicated that the deposit extended deeper than the 350-foot depth attained in the deepest hole and might have very considerable areal extent. Additional funds were allotted, and the drilling contract was extended twice to a final maximum of 17,000 feet with 2,000 foot maximum depth of hole. Drilling was continued by the Bureau of Mines until February 2, 1945, when 15,844 feet of hole had been drilled. The Magma Copper Co. took options on this and adjoining property in September 1944 and commenced drilling with two machines. It also engaged the two contract drills used by the Bureau after it stopped drilling. It exercised its options in August 1945 and organized the San Manuel Copper Corp. to operate the property. That company is continuing to explore the ore body with six churn drills. Thomas Lyon took options early in 1945 on holdings adjoining the San Manuel property on the east and is operating two churn drills. Exploration up to the completion of the last holes started by the Bureau of Mines indicated a block of ore 5,100 feet long, 400 to 800 feet wide, and 500 to 900 feet thick, and averaging about 0.8 percent copper. Subsequent drilling showed that the ore body extends considerably beyond this block. The axis of the ore body strikes about N. 61º E. Copper minerals are disseminated in hydrothermally altered quartz monzonite and monzonite porphyry. Ore outcrops in two small areas over the northeast part of the block. Elsewhere the copper-bearing rocks are capped by Gila conglomerate, which thickens toward the west and south. Drilling showed that the ore is in a thick, tabular body with a steep dip to the south. The ore body lies near the surface in the northeastern part of the block. The south side of the block is much farther below the surface than the north side. There the upper part of the copper-bearing rocks is lightly mineralized, so that the hanging wall of minable ore lies deeper than the base of the conglomerate cap, which thickens southward.

Aug 1, 1947

By Irving Hartmann

At the 9th International Conference of Directors of Safety in Mines Research a paper6/ was presented describing the initial phases of research by the Safety in Mines Research Establishment at Buxton, England, on the remote control of timber fires with high-expansion foam plugs in a rock tunnel. The work received extensive publicity, and great interest was aroused by the implied possibility that the method might be used successfully to control coal-mine fires, which for various reasons cannot be approached and attacked by standard fire fighting measures and frequently require sealing extensive, valuable coal properties and lead to loss of production and coal reserves and occasionally loss of lives. To investigate the practicability of the foam-plug technique under American min¬ing conditions, with room-and-pillar-type extraction and multiple entries, the Bureau of Mines in 1957 began an investigation at its Experimental Coal Mine, Bruceton, Pa, In preparation for this work it was necessary to rehabilitate and reinforce an elliptical tunnel in the mine where studies had been made, many years ago, leading to development of a ventilation system used in the Holland Tunnels between New York and New Jersey, and in many other vehicular tunnels.

Jan 1, 1958

By D. W. Butner

The blast -hole method for drilling and breaking ground is not new to the mining industry . For several years it has been used rather extensively in Canada , particularly in the gold mines , where it was first developed and where the major advances in the technique as applied to present - day mining problems have been made . At present , 40 mines in Canada and the United States are using the method in one form or another , and from all indications its use will increase in the future . In two California mines , blast -hole diamond drilling is now used for a part of or for all stoping operations , and in one of these it is used to some extent in development work . At the Mountain Copper Co.'s Hornet mine in Shasta County, about 50 percent of the pyritic sulfide ore produced is mined by the blast - hole method , and the U. S. Vanadium Corp. mines 80 percent of the ore produced at its Pine Creek tungsten mine in Inyo County by this method . At Pine Creek , long -hole drilling and blasting is used for mining pillars also , and in pre - stoping development . The blast -hole diamond - drilling method is not applicable to all types of ore bodies . A third property in California , the El Dorado Limestone Company , El Dorado County, tried the method for several months in 1943 and 1944 , but , owing to certain factors that greatly increased mining cost , the company soon returned to conventional mining methods .

Feb 1, 1948

By K. P. Wang

SIGNIFICANT general developments took place in the Far East during 1964, with far-reaching repercussions on the mineral and industrial economies of individual countries and the region as a whole. Japan, during this, "the Year of the Open Door," ushered in the era of industrial maturity, greater independence in economic policy, and expanded technical assistance to less developed countries. Symbolic of its dynamic economic growth is the fact that Japan out-produced the Federal Republic of Germany in steel during 1964 to take over a third-ranking world position. Mainland China, recovering from the "Leap Forward" debacle, made significant gains in industrial output. Mainland Chinese trade with Japan was on the upswing, and discussions were held between the Chinese and the Soviets for possibly resuming Soviet aid in industrial and mineral development. Meanwhile, United States aid to Taiwan was being phased out because of progress achieved. Rapprochement between South Korea and Japan was imminent late in 1964, a factor which may well affect South Korean mineral development. The Indonesian-Malaysian confrontation created economic difficulties in both countries. The war in Viet-Nam seriously disrupted industrial activities, particularly in the south.

Jan 1, 1966

By J. Sammarco

Proper illumination is critical to a miner?s ability to detect hazards in underground mines. Moving hazards are often located in the miner?s peripheral field-of-view, while slip/trip/ fall hazards are often located in the forward field-of-view. The objective of the research described in this paper was to determine if light-emitting diodes (LEDs) improve visual performance as compared to traditional incandescent (INC) cap lamps. The research presented focuses on comparative studies of a National Institute for Occupational Safety and Health (NIOSH) prototype LED, a commercial LED and an INC camp lamp. Thirty subjects participated in these studies, with ten subjects in each of the following age groups: 18 to 25 years, 40 to 50 years and 51+ years old. Visual per­formance was quantified by the subjects? speed and accuracy in detecting hazards, while visual performance for disability glare was quantified by the use of contrast sensitivity tests. Results suggest that LEDs with a visible spectrum containing a higher concentration of the shorter wavelengths can enable visual performance improvements with respect to disability glare, the detection of moving hazards in the peripheral field-of-view and the detection of floor hazards in the forward field-of-view. The NIOSH prototype LED cap lamp provided the best visual performance improvements for the older age groups in every test.

Jan 1, 2009

By David F. Smith

[The U. S. Bureau of Mines at its Pittsburgh Experiment Station is frequently called upon to determine by laboratory tests the explosibility of suspensions in air of various dusts encountered in mines and elsewhere. Not all dusts which are combustible or contain combustible material will form explosive mixtures with air under ordinary conditions of temperature and pressure. They may not be highly combustible enough. They may contain a considerable amount of inert or non-combustible material or, the dust particles may not, be fine enough to form explosive mixtures. A knowledge off the chemical composition of a dust together with a determination of the size of the particles often gives valuable indications. But in many cases actual explosibility tests are necessary. Such a case is evidently that of powdered soap, whose explosibility hazard the Bureau was recently called upon to determine, Although an explosion which occurred in a soap plant as early as 1890 was attributed4 to powdered soap, it is apparent, due to the great number of inquiries received by the Bureau, that the hazard presented by powdered soap has not been at all generally appreciated. To the writers' knowledge, no extensive investigation of the explosibility of powdered soaps has been made. It is only recently that pure powdered soap has been manufactured on a large scale. The familiar "soap powder" in the past was usually a mixture of soap with a relatively large quantity of sodium carbonate. Often it contained large amounts of moisture and abrasive material. Even a highly combustible dust when mixed with large quantities of inert dust will not form explosive mixtures with air. Pure powdered soap, however, presents a different aspect. Pure soap is formed by combination of alkali (incombustible material) with fatty acid (combustible material). Toilet soap fray also contain a certain amount of glycerin and essential oil winch, being combustible influence the explosibility]

Jan 1, 1928

By K. E. Hjelmstad

During an underground mine fire, air can be rapidly depleted of oxygen and contaminated with smoke and toxic fire gases. Any delay in warning miners could have disastrous consequences. Unfortunately, present mine fire alarm systems, such as stench, audible or visual alarms, telephones, and messengers, are often slow, unreliable, and limited in mine area coverage. Recent research by the U.S. Bureau of Mines has demonstrated that ultra low frequency electromagnetic signaling can be used for an underground mine fire alarm. In field tests of prototype equipment at five mines, electromagnetic signals from 630 to 2,000 Hz were transmitted through mine rock for distances as great as 1,645 m to an intrinsically safe receiver. The prototype system uses off-the-shelf components and state-of-the-art technology to insure high reliability and low cost. When utilized, this. technology would enable simultaneous and instantaneous warning of all underground personnel, regardless of their location or work activity, thereby increasing the likelihood of their successfully escaping a mine disaster. This report presents the theoretical basis for through-the-rock ultra low frequency electromagnetic transmission, design of the prototype transmitter and receiver, and the results of in-mine tests of the prototype system.

Jan 1, 2010

By E. J. Gleim

[of- ac tore affecting the e -success of recent conveyor miningsystems forLt. extraction. 1 GL C ,_tfreedom shoot &apos;_)`u 2--ethe.1 is coal while e en othershot firers re:7 t _e&apos; _U-tin , w J, e coal .Z- 311.ing States conveyors because ;-.;lax .ca requires thatblasting be limited to when c .. men os. _o tend neces¬sary officials 1 s . re out c-z ,r 7t ...y e:e l z<: woes no t a -¬#to 1 C" such restriction on blasting conveyor miningbeen extendedWhere ere t ere. re no _ c: t&apos;_ _c tit-----! . kind cutlasting;,1CL?; C&apos;. _ z)carried anI-7LC. AT continuouslyHowever, unless et._&apos;0:, precations are taken under r&apos;t e , accidents, n is or such, as111 electricity r 1C- from.J--_,._.1t ,° =&apos;1?without usingholes, as well as numerous-o _&apos;1&apos;-1 -= e troublehe record of mineexplosions (some of themSo so _C&apos;_ °:&apos;,v 0f rock- dusting]

Jan 1, 1941

By A. B. Hooker, Ilsley. L. C.

"Several writers have called attention, in the technical press, to the possible failure of flame safety lamps in coal-dust laden atmospheres. Such writers question the safety or a flame lamp that has been proved only in atmospheres containing methane, believing that the resistance of the lamp to explosion would be lessened it coal dust constituted a part of the explosive mixture.If this be true, it follows that any series of tests devised to prove the safety of flame lamps for use in gaseous and dusty coal mines should not only embrace tests in mixtures containing various proportions of methane, but also in some of the tests the effect of adding coal dust to the explosive gaseous mixtures should be investigated.Some attention has been given this question by investigators, but the more common practice has been to make all tests in gas and air mixtures only, using methane when it was readily available. Apparently the English Accident Committee (1879-1886) who conducted tests upon 250 different lamps did not use coal dust in their tests. The first British requirements for the testing of safety lamps, issued as a result of the Coal Mine Act of 1911, made no mention of tests with coal duet.The Austrian Fire-damp Committee (1890) conducted a series of tests in which coal dust was used in some of the tests. In certain tests, the addition of coal dust apparently lowered the resistance of the lamp 1 meter per second. The Belgium investigators, Messrs. Watteyne and Stassart, conducted a series of tests in 1904 in which coal dust was used in a few tests without any marked difference in safety."

Dec 1, 1920

By Aner W. Erickson

"Preliminary examination of tungsten deposits on the Mountain View property near Hyder, Alaska, was made by Neal M. Muir, an engineer of the Bureau of Mines daring the summer of 1942. Fifteen samples were cut, rough esti¬mates of ore reserves were made, and it was proposed to extend the drift on scheelite-bearing vein 300 feet in a northwesterly direction.From May 22 to October 24, 1944, an exploratory project was conducted on the property by the Bureau. In the course of this work, the camp buildings were rehabilitated; the dam, hydraulic line, and machinery were repaired; 226 feet of drift was driven; 80 groove samples aggregating 3.9 tons in weight were cut; a 6,000-foot surface and underground traverse was run; and the area was mapped in detail.In its program of exploration of mineral deposits, the Bureau of Mines has as its primary objective the more effective utilization of our mineral resources to the end that they make the greatest possible contribution to the national security and economy. It is the policy of the Bureau to publish the facts developed by each exploratory project as soon as practicable after its conclusion. The Mining Branch, Lowell B. Moon, chief, conducts preliminary examinations, performs the actual exploratory work, and prepares the final report. The Metallurgical Branch, R. G. Knickerbocker, chief, analyzes samples and performs beneficiation tests. Both these branches are under the supervision of Dr. R. S. Dean, assistant director.Special acknowledgment is doe Neal W. Muir, project engineer, and Robert S. Sanford, acting chief, Alaska Division, Mining Branch, for their supervision of the field work and revision of the report.Acknowledgment is also made to Silbak Premier, Ltd., for rendering valuable assistance in the repair of equipment and for extending various courtesies to Bureau of Mines personnel during the conduct of this project.The Mountain View property is located at latitude 55° 59' north, and longitude 130° 03' west in the Salmon River mining district of southeastern Alaska, about 5 miles in a northwesterly direction from the town of Hyder, which lies at the head of Portland Canal, as shown in figures 1 and 2. Vein outcrops and surface workings are at an elevation of 950 feet and occupy the west flank of a low ridge between Skookum and Fish Creeks, as shown in figure 3. The portal of the long adit exposing the vein at depth is on Skookum Creek about 550 feet north of the confluence of Skookum and Fish Creeks.Access to the property is over a 4-foot wide trail built and maintained by the United States Forest Service. This trail is suitable for pack animals and is adequate for transportation of supplies and material for exploratory work. During the periods of camp construction and past exploratory operations a 4,000-foot, single-cable, aerial tramway, now in disrepair, served for transportation of materials and all machinery from the Salmon River Highway to the property. The cost of such hauling was high, amounting to $12 a ton. Topography is suitable for construction of a ""cat road"" 2 miles in length, connecting the property with the Salmon River Highway. It is estimated that such a road could be built for $5,000 a mile, and supplies, machinery, and concentrates could be haled over it at a cost of less than $2.50 a ton."

Sep 1, 1946

By Donald O. Rausch, Robert H. Merrill, David W. Wisecarver, S. Jackson Hubbard

Results are reported for stress - relief borehole - deformation measurements made in three underground openings near open - pit mines in the Ruth mining district , Nevada . A total of 134 deformation measurements were made in 8 boreholes . These measurements determined the regional stresses in the horizons above , below, and at the elevation of nearby open - pit mine floors ; knowledge of these stress conditions is considered essential information relative to certain aspects in the designing of stable pit slopes . The determinations indicate that the stresses in the district are due to the gravitational load of the overburden in a confined stress field .

Jan 1, 1964

By R. V. Higgins, H. C. Miller

"INTRODUCTION The development of methods for determining the total quantity of crude oil that a given pool could be expected to produce in the future and the well-spacing and drilling programs most likely to result in the recovery of the maximum quantity of oil at the minimum cost became problems of acute concern to American oil producers and petroleum engineers during the second decade of the twentieth century, The United States faced what seemed at that time to be a serious shortage of petroleum, and it appeared that the constantly increasing demand for petroleum and its products could not be adequately supplied. Undrilled prospective acreage, which until then had been plentiful, seemed to be getting scarcer, competition was increasing, the margin of profit to the producer was shrinking, and the need for developing constructive policies of conservation appeared paramount. As a result of physical and economic changes then taking place within the petroleum industry prompted by the seemingly uncertain future, accurate knowledge pertaining to the probable future production of oil wells and of oil lands especially was needed and greatly desired. Furthermore, the need for obtaining the maximum quantity of oil from known fields caused technical information - which up to that time had not been deemed essential to the successful and profitable operation of oil lands - to be sought eagerly. The need for technical information, such as methods for determining future reserves of oil and the rate at which the oil could be obtained under a specific program of drilling, was emphasized further with the passage of the Revenue Act of 1918, and oil producers with enough income to place them in the taxable class were compelled, for the first time, to report their taxable income 4/ to the Treasury Department."

Nov 1, 1939

By D. G. Kesterke

The electrolytic reduction of uranium dioxide to molten uranium in fluoride baths at approximately 1,200° C was demonstrated. Electrolyte constituents were BaF2, UF4, and either MgF2 or LiF. Preliminary laboratory-scale experiments were made in which the uranium oxide was added continuously for 3 to 5 hours to the cell during electrolysis. Over 1,000 grams of metal of 99-8 percent purity was made in some tests, Major impurities were aluminum, barium, iron, silicon, carbon, and oxygen. The effects of cell design, geometry, and bath composition were investigated. Electrode arrangement was the most important factor in cell performance.

Jan 1, 1963

By R. L. Crosby, L. W. Higley

Magnesium- rich magnesium- aluminum- zirconium alloys in the cast and in the extruded and heat- treated condition were studied to identify the phases present and to determine phase distribution . In cast alloys , two intermetallic compounds were identified : ZrAla by X- ray diffraction ; and Mg₁ Al₁₂ by microscopical observation . Based on microscopical comparisons between the known phases in the cast structures and the phases in the structures of extruded and heat - treated rods , ZrAl₂ and Mg1 , Al12 were identified in the structure of the latter . The presence of these intermetallic compounds in rod specimens could not be confirmed by X- ray diffraction . ZrAl₂ was observed in the structure of extruded and heat - treated rod specimens containing as little as 0.01 weight - percent zirconium . The presence of aluminum restricts the solubility of zirconium in magnesium because of the strong tendency to form ZrAla . This intermetallic compound segregated in clusters of small particles in the matrix of cast alloys , and only slight improvement in distribution was noted when the alloying techniques were varied .

Jan 1, 1964

By Bowles Oliver

"Modification of Quarry Process.Limestone beds are formed by processes of nature, processes that have been in operation for thousands and perhaps millions of years. Therefore, their com- position and physical properties are long-established and unalterable features over which man has no control. He must take them as he fields them.It is undoubtedly true that the character of lime depends largely on the nature of the parent limestone. A high-calcium lime cannot be manufactured from a dolomite, nor can a pure lime result from the calcination of an impure raw material. However, in the process of turning limestone into lime man is not entirely helpless in his control of quality. Even though a deposit is variable in character a single lime product of uniform quality may be produced by judicious quarrying. A single grade of product may not always be desired, the producer may wish to supply the needs of a variety of users each demanding U different grade or quality of lime such a series of graded products may be produced in part at least by modifying the quarry method. Thus, by changes in quarry practice a single product or a variety of products may be made. The latter problem will be considered at a later time, and the present paper devoted to the first named question' that of producing a single grade of lime from a deposit of variable rock,It is realized of course that uniformity in the product is influenced greatly by manufacturing processes such as calcining' hydrating' grinding or storage, but the present discussion is confined to the influence of raw materials only. In considering the various devices that may be employed it is realized that much remains to be learned, and it is hoped that many operators will contribute to the discussion as they have already done in connection with previous papers of this series."

May 1, 1923