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By A. Gene Collins

The Bureau of Mines conducted a research study of the geochemistry of the Smackover Formation to determine what geochemical relationships are useful in exploration for and production of oil and gas. Samples of oil, gas, brine, and rock were collected and analyzed. The oilfied brines were analyzed by methods recommended by the American Petroleum Institute and by tentative methods of the American Society for Testing and Materials. The crude oils were analyzed by Bureau of Mines methods; the gas, by Bureau of Mines methods; and the rocks, by wet-chemical, atomic absorption, and neutron activation methods. The results were correlated and interpreted, and several geochemical relationships useful in exploration and production were found. These include the type and class of brine, organic constituents in the brine, redox potential, in situ temperature and pressure of brine, degree of sulfate and carbonate saturation of brine, and halide concentrations in the brine.

Jan 1, 1974

This report summarizes the work performed by the Bureau of Mines on the development of analytical procedures for determining metallic and interstitial impurities in high-purity tungsten. Fourteen published methods and seven unpublished methods are briefly described. Carbon, hydrogen, nitrogen, and oxygen, in microgram to higher quantity levels, can be determined by several methods. Trace levels of 29 metallic impurity elements can be determined by optical spectrography, X-ray spectrography, and other instrumental methods.

Jan 1, 1968

By M. M. Tilman

The Federal Bureau of Mines developed a rolling method that improves creep resistance and yield strengths of lead alloys containing up to 5 wt-pct Sb. The 0.69-inch-thick slab-cast alloys were breakdown-rolled to 0.226 inch and finish-rolled to 0.063 inch at 5-or 20-pct reduction per pass. Rolling was at room temperature to simulate conventional cold rolling, and at 75°, 125°, and 175° C. Two alternative methods evaluated consisted of (1) a single cold final pass followed by annealing and (2) a single hot final pass. Two additional processing methods involving percipitation strengthening were included for comparison. Compared with conventional cold rolling, hot rolling at 125° and 175° C with multiple light passes vastly improves creep resistance and raises yield strengths. Tensile strengths are less affected. The other treatments also improve creep resistance significantly and generally improve tensile properties; magnitudes vary with treatment and composition.

Jan 1, 1975

By C. E. Hennig

On January 1, 1960 there were 310 petroleum refineries in the United States, with a crude-oil capacity of 9,901,424 barrels daily, according to the Bureau of Mines' annual survey. Compared with a year ago, this represents a net decrease of three in the number of refineries and an increase of 81,578, barrels per day in crude-oil throughput capacity. Continuing the trend to fewer units with greater individual throughput, the capacity of the average refinery in the United states increased during 1959 from 31,373 barrels per day to 31,740 barrels per day. Compared with the previous year, total crude-oil capacity of refineries on January 1, 1960 was lower in the Appalachian No. 1, Other Rocky Mountain, and Texas Gulf refinery districts. All other districts showed slight increases in capacity. At the beginning of 1960 the industry had under construction facilities that would increase the crude-oil capacity in the United States by 70,947 barrels per day. This was the smallest capacity increase under construction at the beginning of the year since 19460 Included in this construction of additional capacity were two new refineries, one in Michigan and another in Hawaii. In addition, the industry was constructing facilities to replace 50,250 barrels per day of existing crude-oil capacity.

Jan 1, 1960

By Jr. Herty

Ferromanganese continues to be an indispensable requirement in steel manufacture. Approximately 470,000 of the 80 per cent ferro-alloy was consumed in 1929 and increasing amounts will be required annually by the steel industry unless some satisfactory substitute is found. An average of 14 pounds of metallic manganese is used for each ton of steel produced, The principal use of manganese is for de-oxidation of the metal in the steel refining processes, although a considerable amount is also used for the production of special manganese steels. Unfortunately, domestic production of manganese ore is inadequate to meet normal peace-time requirements, not to mention increased abnormal war-time demands. The rather large quantities of low-grade manganiferous iron ores which occur in the Coruna Range in Minnesota have for a number of years greatly appealed to those interested in the development of a domestic source of the supply. The North Central Experiment station of the Bureau of Mines has made an elaborate study of the possibilities of the pyrometallurgical treatment of ores from these deposits and much of the valuable information secured by them has already been published.

Jan 1, 1930

By C. H. Herty

[Ferromanganese continues to be in indispensable requirement in steel manufacture. Approximately 470,000 tons of the 80 per cent ferro-alloy was consumed in 1929 and increasing amounts will be required annually by the steel industry unless some satisfactory substitute is found. An average of 14 pounds of metallic manganese is for each ton or steel produced, The principal use of manganese is for deoxidation of the metal in the steel refining processes, although a considerable amount r s also used for the production of special manganese steels. Unfortunately, domestic production of manganese ore is inadequate to meet normal peace-time requirements, not to mention increased abnormal war-time demands.]

Jan 1, 1930

By John Henderson

If you missed this year?s Texas State Holmes Safety Association meeting, you missed a great one. On January 23 & 24, 2009, we held the meeting that was rescheduled when Hurricane Ike threatened Corpus Christi in September 2008. Sixty-five persons from across the state attended the meeting held at the Holiday Inn Emerald Beach. The weather was 82 degrees, and the sky was clear and perfect for a safety meeting. Evaluations submitted by the attendees gave the presentations, the networking, and even the food top marks. There were eight councils represented; Big Country, Central Texas, Costal Bend, Heart of Texas, Hill Country, North Texas and North Central. Presentations included Workplace Examinations, Emergency Preparedness, Screen Safety, Contractor Responsibilities, Powered Haulage, Supervising for Safety, and Basic Inspections of Slings and Rigging. Mr. Edward Lopez, SC MSHA District Manager, gave the State of the District Address.

Jan 1, 2009

By John C. Hartley

Three systems that monitor ventilating fans are described. These electronic monitoring systems automatically perform most of the operations required to conform with the provisions of the Federal Mine Safety Code in the event of fan failure or slowdown.

Jan 1, 1964

By H. E. Blake

An evaluation was made to determine the economics of utilizing waste fluosilicic acid for production of (1) calcium fluoride, and (2) anhydrous hydro-gen fluoride. Two versions of each process were considered and compared. The evaluation showed that both products could be produced and marketed competitively. Lowest estimated product sales prices required to yield a 25-percent return on investment before taxes (discounted cash flow basis) was $339.34 per ton of hydrogen fluoride and $48.64 per ton of calcium fluoride.

Jan 1, 1971

By W. R. McDonald

The Bureau of Mines, U.S. Department of the Interior, conducted small-scale field tests on acidic copper tailings as part of its effort to develop, improve, and demonstrate technology for stabilizing mining and mineral-processing wastes. Two successful demonstration revegetation plots were established on an abandoned copper-tailings pond located on public land adjacent to Holden Village, Wash. The tailings were neutralized with treatments of either dolomitic lime or limerock and fertilized with processed sewage sludge and/or commercial fertilizer. Excellent plant growths covering 70 and 24 percent of the surface were achieved on 1/8-and 1-1/2-acre test plots planted in 1973 and 1974, respectively. Regar brame, Tegmar intermediate wheatgrass, and tall wheatgrass provided the best plant growth and surface coverage. The target pH of tailings neutralization was 6.8; however, good plant growth occurred in areas where the soil pH ranged from 2.9 to 5.8.

Jan 1, 1978

By Terry J. Close

The highly-mineralized 43,700-ha Rapid River study area, on the southeast side of Hells Canyon Wilderness and west of the village of Cuprum, in Adams County, western-Idaho, was investigated in 1992 by the USBM (U.S. Bureau of Mines) in conjunction with its Idaho Land Assessment Program. The 1992 study updated data gathered during the USBM's 1974-76 Wilderness investigation. The studies consisted of the evaluation of 61 mineralized sites and the estimations of tonnages, grades, and minability of these sites. Most of the sites studied are in two mineralized locales--Windy Ridge and Jackley Mountain. A few isolated sites, peripheral to the two locales, were also examined. The 61 sites contained more than 340 mine and prospect workings, including about 10,300 meters (34,000 feet) of underground workings, plus 134 drill holes.

Jan 1, 1993

By R. L. Crosby

The effect of indium on the solid solubility of calcium and of silicon in magnesium was studied using metallographic, X-ray diffraction, and electrical resistivity techniques. The addition of 2 weight-percent or more of indium reduced the solid solubility of calcium in magnesium by forming a compound containing indium and calcium. Indium additions have no perceptible effect on the solid solubility of silicon in magnesium.

Jan 1, 1963

By H. P. Greenwald

About mid-December 1936, the safety director of a large coal corporation visited the authors at the Bureau's Experimental coal mine to discuss a rock-dust barrier he had invented primarily for use in trackless entries of coal mines. The rock dust in this device was carried in its original paper containers and means were provided for ripping these open so that the dust might be scattered in the path of an explosion. The inventor termed the device a "bag barrier", and this term has been adopted in the present paper for convenience. At that time the device was in an early stage of development, and the inventor felt that the barrier should be tested to determine whether it had enough promise of being successful to justify further development. The matter was taken under consideration and finally three tests were made during the week of February 15, 1937. It was concluded that while the device did stop an explosion in two of the three tests, it was much loss effective than ordinary rock dusting, and that too few data were obtained to permit direct comparison with tests of other barriers. Apparently, the conditions under which the device could, be successful were somewhat limited, out the limits could not be defined without additional tests.

Jan 1, 1938

Preventive maintenance practices are listed in the manufacturers' instruction books. In general, equipment that requires frequent and extensive preventive maintenance is generally the most costly. The manpower spent on these frequent trips to remote areas is such that it is usually better to invest in a more costly system which requires little preventive maintenance. The best preventive maintenance for the system is a good installation. 7.2 Preventive Maintenance and Inspections With any system, periodic inspection is required because of the corrosive atmosphere and adverse conditions that exist in underground mines. These inspections can spot potential trouble in the system. Repair or replacement at that time averts the possibility of losing effectiveness of all or part of the system. 7.2.1 Cables Approximately once per month all cables in the communications system should be inspected for kinking, chafing, cracking, wear, stretching, or other signs of physical abuse. Particular attention should be paid to cable glands at the entry or exit points to the various units in the system, where the cable goes around sharp corners, in the vicinity of holding cleats which may be clamping the cable too tightly causing potential damage, and across the areas where the cable is exposed to physical damage from outside sources, such as equipment or falling objects. If a cable is damaged, it should be replaced as soon as possible. It is mandatory that the ground leads and connections to carrier current phones be thoroughly inspected and maintained in good condition, since considerable hazard may exist to the operator or equipment if a ground connection is broken. 7.2.2 Pager Phones The most readily available test set to determine if a pager telephone is operating correctly is the pager phone itself. The following physical check of the system can be performed at any phone station. 7.2.2a Listen Circuit Remove the handset from its cradle and listen to determine if the circuit is functional, as indicated by the presence of noise or conversation on the line. If no noise or voice signals are present at the handset receiver, take the following corrective action: 1. Operate the handset press-to-talk switch several times. Any corrosion on the contacts of this switch may cause a receiver to be temporarily inoperative. Repeated operation may clear the condition. 2. Open the cabinet and see if the battery cables are properly connected and are making firm contact. Check the handset cable and its connections in the cabinet of the pager phone, and see if there is any evidence of a break in the cable, corroded contacts, or poor connections. 3. Remove the handset receiver earpiece by unscrewing it counterclockwise (to the left), and remove the receiver from the socket. Examine the handset cavity; in some units, a patch of cotton batting or floss is used as a barrier to reduce acoustic feedback in the handset. If the cotton patch has absorbed moisture, remove it and replace with a crumpled ball of soft rubber, stuffed just far enough into the handset so it will not touch the receiver or switch terminals. 7.2.2b Page Circuit and Talk Circuit Push the page switch, squeeze the handset press-to-talk switch, and call any other phone. Release the page switch

Jan 1, 1984

By James A. West

COUNTRIES of the Near East, with the world's largest and insist prolific petroleum resources, produced nearly 277 percent of the world's estimated total output of crude& oil in 1964 and accounted for about 60 percent of world exports of this commodity. Although petroleum largely dominated the mineral industry of tine area, production of antimony, chromium, copper, mercury, boron, potash, and phosphate rock was of world significance. Production of crude oil in Near East countries reached a record high of 7,520,000 barrels per day in 1964, an increase of nearly 11 percent over that of 1963. Kuwait maintained its position as the leading producer, accounting for almost 28 percent of the area's output. Saudi Arabia, Iran, and Iraq followed with 22.5, 22.2, and 16.5 percent of total area output, respectively. Despite record production, the Near East, proved crude oil reserve remained in excess of 211 billion barrels, or more than two-thirds of the estimated world proved crude oil reserve.

Jan 1, 1966

By E. J. Ostrowski

The Bureau of Mines experimental blast furnace, Bruceton, Pa., was operated to determine the feasibility of replacing part of the burden coke requirements with solid fuels injected directly into the smelting zone. This report describes preliminary experiments and information resulting from such an interchange. These experiments were made on an all-sinter burden, using two parts sinter to one part fuel. Anthracite fines were injected intermittently into the smelting zone of the furnace by compressed air through auxiliary tuyeres. The interval between injection periods ranged from 5 to 15 minutes. A maximum of 28 percent of the stock column coke bur-den was replaced. This percentage replacement caused furnace malfunction, but the overall percentage of these experiments indicated that 20 to 24 percent of the coke requirements could be replaced in this way. The metallurgical coke consumption was decreased by as much as 377 pounds (25.3 percent) per ton of pig metal produced. Buckwheat anthracite No.4 was used in this experiment; however, such solids as bituminous coal or coke fines also could be used. The frequency as well as the quantity of solid fuel injected has a direct bearing on furnace performance.

Jan 1, 1960

By R. A. Beall

A series of 45 zirconium ingots has been cast by the consumable electrode arc melting process with the object of analyzing the effects of power input from 50 to 230 kilowatts and reduced pressure furnace atmosphere to improve the quality of regular 8-inch-diameter production ingots made thereby. Electrode consumption rate, molten pool volume, melting efficiency, sidewall quality, arc stability, and yield efficiency are considered. The use of direct current and alternating current is studied. In conclusion, reduced pressure furnace operation is shown to promote electrical efficiency, ingot homogeneity, high metal yield, and are stability. INTRODUCTION Zirconium is a particularly difficult metal to melt because of its affinity for atmospheric gases and its solvent properties when molten. In addition, zirconium sponge as produced by the boll process contains minor amounts of magnesium chloride, which cause severe spattering luring melting, because of these difficulties with zirconium, and its sister metal titanium, near techniques have been developed to permit production of commercial size ingots. Among the more promising is the consumable electrode arc melting method.

Jan 1, 1955

By Harold C. Pierce

"INTRODUCTION During the years 1941 to 1945, the United States produced less than one-half of one percent of all primary nickel, whereas the nation's consumption of the metal amounted to nearly three-fourths of the world's supply. Although postwar nickel consumption probably will be less than wartime consumption, trade- estimates for the next 10 years are well above the average established during the 1930-1940 decade. The greatest consumption is expected in nickel alloys, particularly nickel-alloy steels. 3/ The greater use of nickel cast irons and nickel-clad metals also signifies an expanding nickel market. In anticipation of the postwar demand for nickel, and realizing the seriousness of the ""have not"" position of the United States with respect to this metal, the Bureau of Mines, sent an engineer 4/ into the lower Copper River region of Alaska during the summer of 1944 to investigate the nickel deposits near the head of Canyon Creek. Samples from the Spirit Mountain nickel prospect were sufficiently encouraging to justify more intensive exploration. As a result, a program of surface trenching, systematic sampling, and detailed mapping of the property was adopted and directed by a Bureau of Mines engineer 5/ in the summer of 1945."

Aug 1, 1946

By D. S. Colby

The productive capacity of natural gasoline and cycling plants in the United States or. January 1, 1954, was 926 thousand barrels per day, according to the Bureau of Mines biennial survey. This represented an increase of 114 thousand barrels per day during the 2-year period since the last survey. In the previous 2-year period, capacity had increased 164 thousand barrels per day. The total number of plants increased from 521 on January 1, 1952, to 535 on January 1, 1954. The number of operating plants increased from 506 to 521. The major increases in capacity took place in Texas, Illinois, Oklahoma, Louisiana, and New Mexico, with the absorption-type plant continuing to account for most of the new construction. In 1954, however, 6 plants reported using a refrigeration process whereas only 1 plant reported this in 1952. The number of operating compression-type plants continued to decline and combination plants showed a decline this year because a number of these plants were reclassified as absorption-type.

Jan 1, 1954

By A. J. Kraemer

The Bureau of Mines for a number of years has been carrying on an investigation of properties of crude petroleum from producing, fields in the United States and the Western Hemisphere, and has published a series of reports on these fields, including oil fields of Oklahoma2. Acknowledgements Thanks are due to R. R. Brandenthaler and Peter Grandone, of the Petroleum Experiment Station of the Bureau of Mines, at Bartlesville, Oklahoma, who reviewed the manuscript and contributed valuable suggestions. The samples were analyzed under the direction of E. C. Lane at the Bartlesville station of the Bureau of Mines.

Jan 1, 1927