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By V. E. Homme

Low- and high-temperature reduction techniques were employed by the Bureau of Mines in study of conditions favorable to the formation of massive titanium crystals. '1,1,2 low-temperature method, feeding molten sodium to solidified titanium lower chloride-sodium chloride, produced higher quality and high quantity crystalline metal. The percentage of crystalline titanium was increased with increasing reactor diameter, melt depth, and titanium dichloride concentration. The high-temperature technique, feed molten sodium to melts above 8000 C, producing needle-type crystals of lower quality and with less consistent results than the low-temperature method. Layers of titanium foil, sponge, fine needles, wool, and crusts of sin-tered granules were formed during the earl, -art of the low-temperature reduction, and massive crystals were produced beneath this barrier in the latter part of the reduction. Crystalline titanium having an average hardness of Bhn 76 and representing 58 percent of the total titanium was obtained. Lamellar crystals up to 1 1/2 inches long with a hardness as low as Bhn 54 were also produced. A second-stage reduction for reclaiming titanium from offgrade sponge is described. Titanium produced by this method was comparable in quality to that from sodium reduction of titanium tetrachloride.

Jan 1, 1966

By Margaret R. Egan

The U.S. Bureau of Mines conducted experiments in the intermediate-scale fire tunnel to assess the influence of air velocity on the gas production and smoke characteristics during smoldering and flaming combustion of Pittsburgh seam coal and its impact on the detection of the combustion products. On-line determinations of mass and number of smoke particles, light transmission, and various gas concentrations were made. From these experimental values, generation rates, heat-release rates, production constants, particle sizes, obscuration rates, and optical densities were calculated. Ventilation has a direct effect on fire detection and development. The results indicate that, in general, increased air velocity lengthened the onset of smoke and flaming ignition, increased the fire intensity, but decreased the gas and smoke concentrations. Increased air velocity also lengthened the response times of all the fire sensors tested. Rapid and reliable detector response at this most crucial stage of fire development can increase the possibility that appropriate miner response (fire suppression tactics or evacuation) can be completed before toxic smoke spreads throughout the mine.

Jan 1, 2010

By William P. Diamond

In this U.S. Bureau of Mines study, production trends have been analyzed for 82 gob gas ventholes on 7 longwall panels in the Lower Kittanning Coalbed, Pennsylvania. Cumulative production from individual holes was found to vary considerably, ranging from 0.03 x 106 to 10.1 x 106 m3. Peak production rates were generally about 0.03 x 106 to 0.06 x 106 m3/d, but rates over 0.10 x 106 m3/d were observed. The variability of gas production from individual holes can be attributed to' several factors, including completion practices and problems, the extent of fracture development in the strata above the extracted panel, water production, and location on the panel. Of particular significance is hole location. Holes on the ends of the panels, where overburden strata are in tension because of the support of the surrounding pillars, were generally the highest and longest producers. This observation led to the experimental placement of gob gas ventholes in the zone of tension along the margin of a panel, instead of in the traditional centerline location, which is in compression. Analysis of 7 months of gas production data indicates that the experimental near-margin holes produced 77 pct more gas than did centerline holes on the same panel.

Jan 1, 2010

By Juel H. Stears

Research was done to determine if a hydraulically operated penetrometer developed by the Bureau of Mines could be used to estimate the roof-bolt anchorage capacity of mine roof rock. Tests were conducted both in the laboratory using cement cylinders and underground in shale rock. Hardness readings were measured by the penetrometer around the periphery of the bolt holes at the anchorage horizon. Roof bolts Nere then installed and subjected to an anchorage test. The results showed that the penetrometer readings could be used to determine the optimum stratum for roof-bolt anchorage but could not be used to make an accurate estimate of the anchorage capacity.

Jan 1, 1965

By Foster Fraas

The electrical conductivity of minerals increases with increase in temperature as a result of the thermal activation of the electrons. Some oxidizable minerals have a change in the stoichiometric proportions after heating in air, and the conductivity does not return to the original value after cooling. Similar changes occur in reducing atmospheres. Other minerals, such as carbonates and hydrates, are completely decomposed. Electrical resistivity measurements on single particles when compared to standard separation measurements show that minerals having resistivities above 1013 ohms respond as nonconductors. Those below 1011 respond as good conductors.

Jan 1, 1956

By Harold J. Polta

This Bureau of Mines publication considers the feasibility of augmenting the present transportation system by pipelining taconite concentrates from the Mesabi Range to the Chicago area. The cost of pipelining in the hypothetical system using water as the carrier is estimated to be between $3.66 and $3.97 per long ton. This appears competitive with the 1970 rail-vessel transportation rate of $4.08 even after allowing a few cents per ton for barging from the terminal to existing furnaces. Political obstacles requiring solution before such a pipeline could be built and the feasibility of using crude oil as the carrier fluid are also discussed. FORTRAN routines used to calculate unit transportation cost for specific estimated values of cost items and for a range of values are presented. The effect of deviations from estimated values of cost items on the total unit transportation cost are shown graphically.

Jan 1, 1971

By E. W. Newman

The Bureau of Mines, in cooperation with the U. S. Geological Survey, developed the property of the Tungsten Metals Corp. by surface trenching and diamond drilling from November 1940 to June 1941 and from August 1943 to December 1943. The purpose of the work was to determine possible reserves of tungsten in the downward extension and lateral eastern extension of three major tungsten-bearing quartz veins. The property is 50 miles south of Ely, White Pine County, Nev., in the Minerva Mining District. Tungsten ore was discovered in the district in 1915, and mining started in 1916. The tungsten ore bodies occur as shoots in quartz veins that occur along faults in limestone. With the exception of a small-scale leasing operation in 1932, the property was idle from 1919 until 1936, when Tungsten Metals Corp. was organized to acquire the mines. Production ceased in May 1945, and the mines were idle until leased in 1947. Development by the Bureau of Mines during 1940 and 1941 consisted of surface trenching, sampling, and diamond drilling 37 holes for a total of 6,959 feet. Subsequent drilling of eight holes, totaling 3,067 feet, in 1943 disclosed additional reserves. This report sets forth in considerable detail the exploration work completed by the Bureau and briefly describes the mining and milling methods employed. Diamond-drill halo logs and sample analyses are shown graphically in the illustrations that accompany the report.

Jan 1, 1950

By Robert S. Sanford

In April 1948, the Bureau of Mines was requested to evaluate the graphite deposit' known as the Benjamin Franklin and Just mines in Chester County, Pa. After preliminary investigation, it was recommended that the Bureau core-drill, trench, and sample the deposit and make beneficiation tests on the ore. During the first and second World Wars, flake graphite was in short supply, and a number of deposits in the United States were exploited. In 1942, the Defense Plant Corporation, through its lessee, the Benjamin Franklin Graphite Co., purchased 70.263 acres of graphite-bearing land and built a complete mining and milling plant with a capacity of 300 tons of crude ore per 24-hour day at a cost of $426,250 (Plancor No. 1254).

Jan 1, 1949

By J. M. Kuchta

Experimental data are presented on the autoignition temperature (AIT) characteristics of the hydrocarbon jet fuel, JP-6, in various oxygen-nitrogen atmospheres under conditions of constant volume and constant pressure. AIT's of this fuel in air varied little with fuel injection pressure but increased greatly with decreasing fuel content at low fuel-air-ratios. They also increased with decreasing oxygen content of the fuel vapor-oxidant atmosphere. Consistent with thermal ignition theory, the ignition temperatures increased with decreasing initial pressure, ignition delay, and vessel radius; expressions are given which define the observed variation of AIT with these variables for JP-6 fuel vapor-air mixtures. The significance of autoignition temperature data obtained using various ignition criteria is discussed to show the usefulness of such data in evaluating fire and explosion hazards. In addition, data are presented on the extent of oxidation that occurs prior to autoignition of this fuel in air at various temperatures.

Jan 1, 1965

By Fred N. Kissell

Air recirculation caused by dust scrubbers at coal mine working faces was examined by the Federal Bureau of Mines with regard to the potential hazards caused by a possible buildup of methane gas. A theoretical analysis indicated that there was no apriori way to predict the effect of scrubber recirculation on methane concentration levels. Experiments conducted in a full-scale model of a working face area indicated that methane levels were dependent to a great extent on the location of the scrubber exhaust, but that the scrubber recirculation did not substantially increase the methane concentration above those levels that would have prevailed were the scrubber not in operation. An analysis of two underground scrubber trials showed that the scrubbers had no significant effect on methane levels, and a review of explosions attributed to recirculation showed that these were characterized by a lack of fresh air as well as recirculation. It was concluded that high methane levels are due more to a lack of fresh air than to recirculation.

Jan 1, 1975

By F. J. Gallagher

Some serious fires have occurred in bituminous-coal mines because of short circuits on direct-current power systems that do not have adequate circuit-breaker protection. The writer's observation of circuit-breaker installations in numerous coal mines leads to the conclusion that many persons am not properly informed as to the true functions, limitations, and operation of circuit breakers. Faulty protection results in fire hazards that endanger lives and property. Proper circuit-breaker protection would greatly minimize or, in many instances, eliminate the hazards; moreover, many operating advantages of proper application of modern circuit breakers would be gained. The purpose of this circular is to show why fire hazards exist in many mines despite the use of circuit breakers and how, the hazards may be overcome. A method is given for determining whether additional circuit-breaker, protection is required for a specific 250/275-volt direct-current distribution system, and, if so, the approximate locations and capacities of the required supplemental breakers.

Jan 1, 1951

By L. C. Brichta

The Tri-State zinc-lead catalog, compilation of which was initiated by the Bureau of Mines in August 1949, is designed to provide a continuing record of avail-able drill-hole logs and maps of mine developments in the zinc-lead district in southwestern Missouri, southeastern Kansas, and northeastern Oklahoma. The maps and data thus preserved constitute a reservoir of factual information readily available to individuals and firms interested in planning mineral explorations, to Government agencies for formulating estimates or ore reserves, and to the mining industry in the district for general uses. The areas to be included in the catalog embrace the explored and mined tracts within 760,000 acres of the more active western part of the district. The consensus among local mine operators, geologists, and mining engineers is that over 100,000 boles, costing more than $30,000,000, have been drilled in the district. Records of some of the early drilling and mine developments are destroyed or lost, but the Bureau of Mines has copies of about 47,500 drill-hole logs and is accumulating and recording on microfilm those that are currently available. As of May 1, 1954, the logs of approximately 28,000 drill holes had been microfilmed and are available for inspection at the Bureau of Mines office, Joplin, Mo.

Jan 1, 1955

By John W. Chandler

The property of the lava Cap Gold: Mining Corporation is in the Nevada City-Grass Valley mining district about 5 miles east of Crass Valley, Calif. At present (July 1940) the plant is mining end milling about 390 tons of gold-silver ore a day; about 310 men are employed. This paper describes the mining methods used and presents mining costs for 1939, when 60,704 tons were mined by cut-and-fill stoping and 55,676 tons by square-setting.

Jan 1, 1941

By Seth T. Reese

THE INJURY DATA and experience at coke ovens in the United States for 1952 are presented in this bulletin under the following general sections: (A) General injury experience: Tables 1 to 9: Contain current and comparable data on operating statistics, number and classification of injuries, frequency rates, and accident agencies involved in causing injuries. Data are given for the industry as a whole, for each type of oven, and for the States in which coke is manufactured. (B) Selected injury experience: Tables 10 to 15: Contain comparable injury data in the coking industry covering 5- and 10-year periods on the number of injuries, accident agencies, and severity of injuries. (C) Historic injury experience: Tables 16 to 19: Contain data on the number of injuries, frequency rates, and employment at coke ovens from the earliest records through 1952, Operating statistics from 1929 through 1952 are given in table 19.

Jan 1, 1955

By Jerry W. Ramsey

The Bureau of Mines examined a low-, a medium-, and a high-volatile Pennsylvania anthracite by densimetric methods using four mesh si.s of each anthracite. Using high-pressure mercury the macropore volumes and distributions of these pore volumes determined, densities in mercury were calculated, and specific pore vo1.r. ware obtained from these mercury densities in conjunction with helium densities. The helium densities were also used with the ultimate analyses of these anthracites in calculating structural parameters by statistical densimetric methods. The effect of 106 or 108 rads of gamma irradiation in the presence of air and in vacuum upon the properties studied with two mesh sizes of each anthracite. Results of the statistical densimetric method seem to show some breakdown of condensed ring structural units at the lower irradiation level, with subsequent polymerization at the longer period of gamma irradiation. The structural parameters obtained also indicated that in going from high- to low-volatile anthracite, either the number of condensed rings per structural unit increased, or the degree of polymerization increased.

Jan 1, 1965

By Nicholas Kyriazi

A joint effort by the U.S. Bureau of Mines and the U.S. Mine Safety and Health Administration (MSHA) was undertaken to determine how well self-contained self-rescuers (SCSR's), deployed in accordance with Federal regulations (30 CFR 75.1714), survived the underground environment with regard to both impact damage and aging. This report presents findings regarding laboratory-tested SCSR's from 1982 through 1990. The SCSR's were tested on human subjects and on a breathing and metabolic simulator (BMS). These results indicate that most of the apparatus, if they pass their inspection criteria, perform as expected except for units with manufacturing defects or design deficiencies. However, when the apparatus are carried in and out of the mine daily and stored at the working section, they may suffer abuse. Physical signs of abuse, unless extremely obvious, are frequently not detected by the miners or mine operators. This poses a potential danger to a user in an emergency. Recommendations include improved training in inspection procedures.

Jan 1, 2010

By R. W. Geehan

The Yellow Pine zinc-lead mine, situated about 3-1/2 miles northwest of Goodsprings, Clark County, Nev., was explored by core drilling during the fall of 1942 and the summer and fall of 1944 by the Bureau of Mines in cooperation with the Federal Geological Survey. The Yellow Pine district was located in 1855. The original claims covering the Yellow Pine mine were located in the following years: Rover, 1892; Hilo, 1897; Bybee, 1900; Radio and Como, 1906. The mine was operated by the Yellow Pine Mining Co. from 1906 to 1929. This company was dissolved in 1935. At a later date, S. E. Yount and the Security First National Bank of Los Angeles, Calif., acquired ownership of the mine. Since 1939, the mine has been operated in a small way by leasers. Production has been at least 175,000 tons averaging about 10 percent lead and 25 percent zinc, with a gross yield of $5,785,174. Virtually all ore produced by this mine consisted chiefly of oxidized zinc and lead minerals and came from long, pipelike shoots in the 100-foot thick Yellow Pine limestone. Ore shoots are sharply defined; elsewhere, the limestone is nearly barren. Numerous faults cut the mine into blocks. Ore is now mined in an open stope, but in the past, large tonnages wore mined in stopes by square-set methods. Ore produced recently was shipped direct to smelters unprocessed; in the past, it was milled by gravity and produced separate lead and zinc concentrates.

Jan 1, 1949

By Walter E. Lewis

This circular presents the method of making tests and apparent results of comparing performance of tungsten carbide insert bits and steel detachable bits by the Cleveland-Cliffs Iron Co. at the company's mines on the Marquette iron range of Michigan. The mines are at Ishpeming and Negaunee, Mich., and include the Cliffs Chaft, Mather "A", Cambria-Jackson, and Mather "B". There are four general characteristic types of high-grade iron ore on the Marquette range. B. H. Boyum2/ classifies the Cliffs Shaft as "hard-ore" and the Cambria-Jackson and Mather "A" as "soft-ore" types of deposit. Shaft sinking through Jasper, slate, and graywacke was in progress at this writing at the Mather "B", with completion at 3,100-foot depth in August 1949. The many different kinds of rock and ore at the mines of the Cleveland- Cliffs Iron Co. and the experimental work being carried on with carbide in- sert bits make it possible to compare, generally, the carbide insert and steel detachable bit. The type of "hard ore" at the Cliffs Shaft mine re- quired close study of the possible use of the insert tit, and their records are more complete than those of the "soft-ore" mines. History and development of tungsten carbide tips inserted in rock drill bits have been covered by R. W. Adamson, C. H. Vivian, R. C. Sullivan,5/ and others. Tungsten carbide insert rock bits have only recently been introduced to the domestic mining industry. Although unusual performance records are being reported at operations employing the insert bits, the general adaptability of the tool to all rock types and the advantages to be gained by using carbide insert tits remains to be demonstrated. Insert-bit performance is being observed at numerous mines and quarries throughout the United States The several mining operations at the Cleveland-Cliffs Iron Co. at Ishpeming, Mich., is one site where exhaustive comparative tests of insert and conventional steel detachable bits are currently in progress. Results to date are sufficiently impressive to be of general interest to the mining

Mar 1, 1950

As part of its regular program to provide timely information on domestic mineral commodities, the Bureau of Mines conducted an engineering appraisal of more than 1,300 lode and placer gold deposits in the United States to deter-mine their gold production potential. While these deposits were estimated to contain over 400 million ounces of gold, only 9 million ounces, or slightly more than 2 percent, was found to be producible at $35 per ounce under prevailing mining and metallurgical technologies. The study revealed that any significant increase in available gold in the United States is most likely to come from the discovery of new sources, intensive exploration and development of the more promising known mineralized areas, and development of new or improved mining and metallurgical techniques.

Jan 1, 1967

By H. H. Schrenk, L. B. Berger, Robert L. Beatty

"INTRODUCTION Toxic oxides of nitrogen 5/ are formed or liberated in many industrial process and may constitute a definite hazard to the health of persons exposed to the atmospheres thus produced. Oxides of nitrogen occur in the gases involved in the use of explosives, in the gasoline products of welding operations in the exhaust of internal-combustion engines, in the vicinity of electrical discharges, in the combustion of nitrated materials, and in chemical process involving nitration or the use of nitric acid, Itis evident that oxides of nitrogen may constitute an occupational hazard in many industries, and therefore it is important that those concerned with the control of such hazards be equipped with a technique suitable for the determinations of oxides of nitrogen in the concentrations of,hygienic significance."

Feb 1, 1943