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By H. A. Tucker

This Bureau of Mines investigation was conducted to determine the appropriate quantities of rare-earth methals (REM) in the form of silicides to add to an alloy steel for the purpose of increasing toughness and ductility. The work was conducted in a vacuum induction furnace with the rare-earth additions required to deoxidize and desulfurize a simulated basic oxygen furnace (BOF) vacuum-degassed steel initially containing 0.013 to 0.016 percent sulfur. The product proved to be as good or better than the best basic electric furnace steel of the same composition made by the steel industry. Twenty-three experimental heats of 5 Ni-Cr-Mo-V steel were made, cast into 50-1b ingots, and hot-worked in a press and a rolling mill to ½ inch plates which were then heat-treated to 130/150 ksi4 yield strength. Impact and tension tests showed that the addition of 0.025 to 0.100 percent, or ½ to 2 lb per ton, respectively, of rare-earth metals when compounded with silicon were appropriate for increasing toughness and ductility. These quantities resulted in retained cerium contents between 0.014 to 0.025 percent, and increased the Charpy V-notch energy absorption and the percent reduction of area significantly as compared with base heats at the same sulfur content levels. All the test heats, including those with additions of REH of as much as 4 lb/ton, had greater Charpy V-notch energy absorption values than the base composition could have developed at the starting sulfur range of 0.013-0.016 wt pct.

Jan 1, 1968

Determine safe practices for surface mine blasting near pressurized gas, oil, and water transmission pipelines. Background Surface mine blasters regularly have to address the issue of how blasting affects transmission pipelines that run near and sometimes through their permit areas. Regulatory approaches to blasting have ranged from no regulation at all to strict limits intended to prevent cosmetic cracks in plaster interior walls of homes, but they have not directly addressed the impact of blasting on nearby pipelines. Concerned with both productivity and safety, the mining industry and its regulators have requested guidance on safe practices for mining near pipelines. The Pipeline Research Group of the American Gas Association has sponsored studies of the effects of small close-in blasts because of vibration concerns related to the installation of new pipes into existing pipeline right-of-ways. By contrast, the recent study in which the U.S. Bureau of Mines (USBM) took part is the first addressing large-scale mining blasts.

Jan 1, 1995

By E. W. Dean, W. A. Jacobs

"The petroleum division of the Bureau of Mines in its laboratory investigations, has had occasions to develop a number of types of electrical heating equipment. It was found that electric heaters could be used to particular advantage in the standard distillation test for gasoline. (Dean, E.W., Motor Gasoline, Properties, Laboratory Methods of Testing and Practical Specifications, Bureau of Mines Technical raper 214, 1919, 33 pages.) In order to assist in rendering this type of heater available for general use, a description of the apparatus developed by the Bureau was published. (Dean, E.W., A convenient electric heater for use in the analytical distillation of gasoline,. Jour. Ind, and Eng. Chem., Vol.10, 1918, page 823.) Shortly after the article was printed a chemical supply house undertook the manufacture of an electric heater suitable for gasoline distillation. A preliminary model was examined and tested by the Bureau and modifications were suggested that were incorporated in the type of heater that was finally marketed.Description of the Bureau of Mines-heater: The electric heater developed by the Bureau has an inverted conical resistance Plament surrounded by a layer of heat-insulating material and mounted in a metal case having a top of hard asbestos (Transite) board. The resistance element is a helix of nickel-chromium alloy wire held by a molded core of alundum. The Bureau heaters are generally of about 330 watts capacity and are used with stock types of regulating rheostats capable of reducing the effective wattage to about 43 the full-load maximum."

Jun 1, 1920

Provide a method for obtaining in situ measurements of coal cutting forces which are needed for mining machine design. Approach A portable in-seam testing device is carried to the face of an underground coal mine heading to measure the cut-ting force encountered by a continuous miner pick directly at its maximum depth of cut. How It Works The tester frame is attached directly to the coal surface with four one inch diameter threaded studs resin-bolted into 1-1/4 inch diameter holes which are drilled 30 inches deep. Spherical nuts and washers compensate for misalignment between the bolts bearing plate, and traverse beams. Spacers can be placed over the studs to assure that the traverse beams remain in the same plane. Cutting forces are applied by a hydraulic cylinder that moves the pick of the tester through a twin-chain arrangement which gives a 20-inch cutting stroke with

Jan 1, 1982

"Fire fighting in metal mines under the best of conditions is a dangerous, a slow, and a difficult task. Certain gases generated from combustible material burning in restricted areas are poisonous, even in small quantities, and can not be breathed without serious and often fatal results. In addition to poisonous gases, smoke is given off which obscures the vision of the fire fighter and frequently prevents him from gaining access to the fire area. Many fire-fighting crews have had to turn back because their vision was so impaired by the dense smoke that the fire area could not be located and there was danger of them becoming lost in the mine.In mines having mechanically controlled ventilation - that is, mines not dependent entirely upon natural air currents - the gas and smoke can be forced ahead of the fire-fighting crews, thereby facilitating exploration of the mine and saving the time, energy and oxygen of the mine rescue apparatus crews.Where currents of fresh air can be circulated up to points near the fire without danger of seriously spreading the fire, fresh air bases can be established in the immediate vicinity, and a more intelligent campaign for fighting or controlling the fire can be mapped out.Positive air currents through forced ventilation may also result in saving the lives of miners who otherwise might have been trapped in smoke and poisonous gases.It is generally known that comparatively few metal mines have attempted to regulate or control air currents, with the result that when a fire occurs underground, the normal ventilation may be reversed, short circuited, or the air current may be in one direction one minute and in the opposite direction the next; or, generally speaking, the ventilation can not be depended upon, and smoke and poisonous gases may accumulate in any part of the mine or ""drift"" on the fire-fighters or on the miners endeavoring to escape."

Apr 1, 1921

By Fred N. Kissell

A self-sealing brattice intended for use during coal mine rescue and recovery operations has been designed and tested by the Bureau of Mines. The major design difference between self-sealing and conventional brattice is that the fabric is cut and sewn BS a hemisphere instead of as a flat sheet. This new type of brattice offers reduced weight, leakage, and installation time. Preliminary testing indicates that the concept is worthwhile, but that further developmental research is required.

Jan 1, 1976

By J. W. Thompson

The Sullman, Picard & Ballot patent, No. 835120, is a process of concentrating ore which consists in mixing the powdered ore with water, adding a small proportion, a fraction of 1 per cent on the ore, of an oily liquid having a preferential affinity for metal- liferous matter, agitating the mixture until the oil-coated mineral matter forms into a froth and separating the froth from the remain- der by flotation. The process is known as an air-flotation process which consists in the use of a frothing agent in conjunction with such agitation of the ore pulp as will distribute the metallic particles of the ore throughout the mixture and produce bubbles of air and bring them in contact in the mixture with the metallic particles so dis- tributed. The bubbles will become attached to such metallic par- ticles, carrying them separately from the particles of gangue up through the surface of the mixture where they can be readily collected by skimming, by overflow, or by the use of other well-known devices. The air-flotation process was a patentable invention in the discov- ery made in March, 1905, and was not anticipated and is valid. Prior to that time there had been no suggestion in the arts that a propor- tion of 0.1 per cent of oil to ore or of any other fraction of 1 per cent of oil to ore would or might result in successful concentration. While the ascertainment that such a minute proportion of oil would affect a successful concentration of ore through a flotation process was a discovery, it was nevertheless of such a character, viewed with respect to the circumstances under which it was made, as to involve inven- tion and confer patentability. Claims 1 and 12 of the Sullman, Picard & Ballot patent, No. 835120, for a process of concentrating ore, known as the air-flotation process, are valid; but claim 9 is so indefinite as to render the claim void. The object of the Sullman, Greenway & Higgins patent, No. 962678, dated June 28, 1910, for improvements in ore concentration, is to separate metalliferous matter, graphite, and the like from gangue by means of oil, fatty acid, or other substances which have a prefer- ential affinity for metalliferous matter over gangue, and it is valid. The Greenway patent, No. 1099699, dated June 9, 1914, for improve- ments in the concentration of ores is invalid, as in view of the prior art the omission to use acid in the process can not confer patenta- bility.

Jan 1, 1917

By John Durkin

Owing to the daily exposures of uranium mining personnel to 222Rn daughters, a device is needed that will continually monitor individual exposure. Such a device has been built and tested by the Bureau of Mines and is known as a radon daughter dosimeter. This is an electronic instrument using a solid-state detector and circuitry. The concept of the instrument, which is a personal device worn throughout the working shift, is to evaluate an individual's cumulative exposure to airborne radon progeny, expressed in units of working level hours. Since the instrument is in close proximity to the miner and measures continual exposure, it avoids the errors caused by the present technique of spot checking of the environment and provides a more accurate account of total cumulative exposure.

Jan 1, 1977

Control respirable dust in underground coal mines through selection of optimum water spray pressures. Approach Through underground trials at longwall and continuous mining operations, the relationship between operating water spray pressure and respirable dust levels at the machine operator's location was determined. Defining the Application Water sprays are used for two significantly different control applications. On longwall mining machines, sprays are commonly installed both on the body of the machine and on the cutting drum. Sprays on the body of the machine are used to redirect dust which has already become airborne away from the machine operator. Each spray acts as a small fan, directing the primary airflow over and around the machine and towards the face, away from the operator. The energy of this system is directly related to the spray pressure. Higher pressures move more air, but care must be taken not to cause turbulence and boilout into the walkway. Sprays mounted on the drum are, effective at suppressing the respirable dust at the bit/coal interface and preventing it from becoming airborne. Again, these sprays must not impart excessive energy to the dust particles thus stirring up more dust than they suppress. While mounting sprays on the shearer drum is standard industry practice, there is no reliable technology available to successfully mount water sprays on the cutting drum of continuous miners. Instead, sprays are mounted on the machine body, close to the drum, and directed at the cutting head. This allows the water to reach the bit/coal interface and mix with the cut material. Here again, care must be exercised to prevent these sprays from imparting excessive energy to the dust particles and stirring up more dust than they suppress. These sprays can also cause dust "rollback" from the face, toward the operator, if operated at too high pressures.

Jan 1, 1986

By George S. Rice, O. P. Hood

The need of protecting mines from the danger of inflow of natural gas from neighboring wells has become more apparent each year since it was found that oil and gas underlie the productive coal measures of Pennsylvania, West Virginia, Ohio, Indiana, Illinois, Kansas, Oklahoma, Colorado, and Wyoming, and, to some extent, the coal measures of other States. The proximity of the known gas and oil areas in the United States to the coal fields and the manner in which the fields overlap in certain States are shown in the map comprising the frontispiece (Pl. I). As the result of many requests received from various sources a conference to consider the protective measures necessary to insure the safety of mining operations in gas and oil fields was called by the Director of the Bureau of Mines to assemble in Pittsburgh, Pa., Feb- ruary 7 and 8, 1913. To this conference were invited a considerable number of gas-well, oil-well, and coal-mine operators within conven- ient distance from Pittsburgh, as well as State geologists and State mine inspectors from a distance. Gas and oil wells are also found near other kinds of mines, such as shale and limestone mines in western Pennsylvania, but these cases are so few that for this and other reasons it was deemed best to con- fine the present inquiry to the consideration of the questions involved in connection with coal mines. It was also not thought advisable to consider the protection of mines from other kinds of bore holes than those for gas and oil, such as coal-prospecting holes, drilled either with churn or diamond drills, or salt wells and artesian wells, because little trouble has been ex- perienced in mining operations from these classes of wells. There- fore the following papers and discussions concern almost entirely the following relations between coal mines and gas and oil wells: (1) Protection of coal mines froin gas and oil wells penetrating -through: (a) Open workings; (b) inaccessible spaces or goaves; (c) pillars, or coal which may be left as pillars. (2) The manner of drilling gas and oil wells passing through workable coal beds so as to provide protection for future mining. The preliminary inquiries of the engineers of the bureau had dis- closed that there was no uniformity in the methods of protecting mines against the leakage of gas from wells, that thousands of wells in coal fields are abandoned yearly without adequate plugging, and without surveys or records being kept to show the location of the holes, from which the casings are generally pulled. According to the State geologist of Pennsylvania, as many as 3,000 wells are being drilled annually in Pennsylvania, 2,000 of these holes being aban- doned within a single year. It is such unplugged, uncharted wells that are the greatest menace in mining. The quantity of gas that the wells produce, although not sufficient to be commercially avail-

Jan 1, 1913

By Yael Miron

Coal mines that undergo self-heatings, and specifically mines that sustain both floor heave and self-heatings, would benefit from the use of sealants to minimize air ingress to susceptible areas. The U.S. Bureau of Mines (USBM) evaluated three sealant systems for this purpose, bentonite-water mixtures, silicate gel, and guar gum gel. The guar gum-based gel was the only sealant that possessed the desired properties of elasticity, ease of preparation, adaptability to the mine, and a long life. In addition, since the gel consists mostly of water, it could quench or cool nearby heatings. Optimal formulations were determined in laboratory tests, and then tested in the USBM Safety Research Coal Mine. Two for-mulations resulted in stable gels that lasted for at least 12 months in the mine. Semicontinuous preparation of gel using an eductor was evaluated and appears feasible. Although guar gum gel is expensive, selective use to prevent heatings in specific areas would be cost-effective, both in terms of productivity and enhanced mine safety.

Jan 1, 2010

By Raymond M. Kacmar

This report presents the Bureau of Mines research on the hardware reliability prediction for two Bureau monitoring projects. The basic concepts of reliability predictions are introduced along with the reliability models and assumptions used for this particular evaluation. The results of the reliability predictions are for ground-fixed and naval-sheltered environments.

Jan 1, 1986

By A. B. Hooker

Investigations at the Pittsburgh Experiment Station have shown that the satisfactory operation of aflame safety lamp depends not only upon proper design and assembly of the lamp but upon the kind of fuel used, and that much of the trouble experienced with permissible flame safety lamps at mines is due to the common use of motor gasolines, none of which is suitable in the present types of permissible flame safety laps. This report gives the results of a limited study to determine what satisfactory fuels are available, the specification limits of such fuels, and to suggest modifications of assembly and care of the lamps to improve performance with any satisfactory fuel.

Jan 1, 1938

Develop a full-length-anchored roof bolt that is economical, nontoxic, nonflammable, and non-allergenic. Approach Grout roof bolts with a storable mixture of ultra-fast setting inorganic cement and water. How It Works A loose mixture of dry cement powder, and pinhead-size water droplets encased in waxy globules, are pack-aged in sausage shaped cartridges for storage and use. After the cartridge is inserted Into a drilled hole, the roof bolt is thrust In and rotated to mix the cement and water. The cement hardens in seconds, providing usuable anchoring strengths in minutes. Prior to filling of the sausage shaped cartridges, the microcapsules of water are Intimately mixed with the dry cement. The currently used grouting consists of a mixture of one part water (minimum) with three parts alpha-type gypsum cement and a minor amount of accelerator.

Jan 1, 1978

By David Hoadley, Kenneth R. Maser, Ashok B. Boghani, James E. Billar, D. Randolph Berry, Mackenzie Burnett, Robert H. Trent

C. 7 Emergency Rescue Hoists There is a need, especially in mine development areas, for portable, on-call, man-rated equipment capable of lifting men through several hundred feet. Wire rope climbing equipment as shown in Figure 37 appears particularly suited to this need. It is portable, weighing approximately 100 lbs. , is currently man-rated for numerous above ground applications and can be electric or air powered. Commercial units currently have a lifting capacity of 1000 lbs. , and can be fitted with bosun' s chairs. Lifting speeds are in the 20-30 FPM range and the equipment is not depth limited. In a situation where miners are unable to climb to the top of a shaft this equipment could rapidly be anchored to the top of the shaft and lowered to them by hand. Since the self contained unit is controlled by the person travelling in the shaft he would be able to negotiate shaft obstruction himself. This would not be possible with other forms of easily deployed free-hanging equipment. Typical manufacturers of this type of equipment are Ohio Hoist Mfg, Co, 321 South Beaver St. Lisbon, Ohio 44432 216-424-7283 Sky Climber Inc. 17311 South Main St. Gardena, California 90248 213-321 -6414

Jan 1, 1976

By A. E. Wells

A critical study of the wet Thiogen process for extracting sulphur from the smoke of smelters is one of several investigations related to the general smelter-smoke problem that are being conducted under the direction of the Bureau of Mines. Part of the work done in the pyrometallurgical section of the cooperative metallurgical exhibit of the Bureau of Mines at the Panama-Pacific International Exposition during 1915 related to this investigation, and at the expiration of the exposition, the work was continued in the labora- tories of the Bureau of Mines in the Hearst Memorial Mining Building of the University of California, Berkeley, Cal., where a mining experiment station of the bureau has been established under the cooperative agreement with the University of California. Early in the spring of 1915, when plans were being made to co- operate with several metallurgical interests, the Thiogen Co. proposed to the Bureau of Mines that, along with the studies of various pro- posed methods for eliminating sulphur dioxide from smelter smoke, there should be included a study of the wet Thiogen process. In the study as outlined it was proposed to determine whether it would be technically and commercially feasible to use the, process for the recovery of elemental sulphur from the sulphur dioxide in waste smelter gases. Although there had been no large-scale work with the process, either in the laboratory or at a smelter, representatives of the metallur- gical and mining industry had shown considerable interest in the proposed method, and the desire had been expressed that a better knowledge of the possibilities of the process should be obtained. Thus, cooperation with the Thiogen Co. seemed justified by the in- terests of the metallurgical industry, and by the conservation promised by the recovery of a product of market value from what is otherwise a waste, and in some instances a serious nuisance. In accepting the responsibility for directing this investigation, the officials of the Bureau of Mines were necessarily free to conduct the work in the manner they considered necessary to determine the facts. It was also understood that any information obtained was to be made available to all who might be interested and might be printed in a Bureau of Mines report. To cover the cost of laboratory equipment and supplies, and the payment of salaries of assistants, other than Bureau of Mines employees, the Thiogen Co. in May, 1915, deposited with the cooperative metallurgical exhibit fund a sum considered sufficient to warrant starting the laboratory investi- gation. The origin and organization of this fund has been described by Clevenger and the author." In outlining the program for this investigation it was hoped that ultimately a small complete plant would be erected and the investi- gation center around the operation of the plant. However, pre- liminary to the erection of the plant, a laboratory study of the proc- ess was considered necessary, as the technical features of the process could be determined, it was believed, as satisfactorily on a smaller scale as on the scale first proposed. However, it was realized at the time that it would not be possible to determine so satisfactorily or definitely the commercial possibilities of the process on the scale of work adopted as in the larger operating plant. With this fact in mind it was planned that, if the study of the technical features on a laboratory scale gave sufficient promise of the process being commer- cially feasible, an operating unit should, if possible, be constructed later, and that more definite information concerning the commercial prospects should be determined. The investigations were started in June, 1915. In June and July work was confined entirely to small-scale laboratory tests, in which a careful study of the chemical reactions involved was made. In August, tests on a larger scale were started, and these were con- tinued until December, small-scale tests being made at the same time. On December 1, 1915, all work on the Thiogen process was discon- tinued temporarily, as the close of the exposition necessitated moving the laboratories. Work on the Thiogen process was started again in January, 1916, in the laboratories of the new mining experiment sta- tion at Berkeley, Cal., and was continued during the spring of 1916 until a point was reached where it was felt that the essential parts of the process had been carefully covered, and that some definite state- ments concerning the technical features and possibilities of the process, as given in this report, were warranted.

Jan 1, 1917

Predict the cumulative hydrologic impact of mining on the environment. Approach A comprehensive set of computer models has been developed to predict the impact of mining on ground water. Mine inflows, drawdowns in aquifers, and ground water quality can be predicted. How It Works The Prickett-Lonnquist finite-difference groundwater model was specially modified for the hydrologic problems of mining. This model, developed at the Illinois Water Survey in the 1960's,

Jan 1, 1982

By C. W. Smith

Research was conducted by the Bureau of Mines to determine the effectiveness of various types of crushers for use with the Bureau-developed pneumatic concentration technique for mica. Three types of crushers were investigated in this study, a roll crusher, a jaw crusher, and a hammer mill. All the mica concentrates produced contained over 82 percent mica, but recoveries varied considerably. The roll crusher gave the lowest recovery of 46 percent of the mica followed by the jaw crusher with a recovery of 50 percent of the mica. The hammer mill proved the most effective, producing four concentrates with recoveries of at least 70 percent.

Jan 1, 1981

By H. W. Frevert, A. C. Fieldner, S. H. Katz

"The Bureau of Mines, in its investigations of as masks for use in mines and allied industries tests masks that are voluntarily submitted by manufacturers for examination, and issues approval certificates for masks that meet the bureau's specifications. This paper describes the tests that were conducted on an ammonia gas mask by the Bureau of Mines, which successfully met all requirements and tests for ammonia, masks. The mask tested, known as the GMD ammonia gas mask, is manufactured by the Mine Safety Appliances Co., Pittsburgh, Pa. This ammonia gas mask, which forms a pocket over the face and allows breathing through the nose, consists of a face-piece with non-shatter eyeglasses; this is attached by means of a corrugated rubber tube to a canister supported on wearer's chest by a harness. The canister is green in color and is of tinplate construction. It was a disc valve at the bottom to prevent exhalation through the canister. The filling of the canister consists of a specially impregnated activated charcoal, about 750 c.c. in volume and weighing about 520 grunn. The material is supported above the check valve by a dome of wire screen covered with toweling. Above the granular material is a filter of absorbent cotton screens, and all materials are hold firmly in place by pressure from strong"

May 1, 1926

By C. E. Jordan

Under its program of advancing minerals technology, the Federal Bureau of Mines has invented a laboratory apparatus for continuous separation of minerals based on differences in dielectric properties. The separator consists of a rotating drum electrode and a wire screen electrode positioned 3 mm apart. A high voltage applied across the electrodes that are immersed in a dielectric fluid produces a high-gradient electric field. The high-dielectric-constant (K) minerals are attracted to and conveyed through the separator by the rotating drum electrode, while the low K minerals settle through the screen electrode. Several design and operating parameters, such as electrode configurations, the dielectric liquid and its dielectric constant, electrical voltage and frequencies, feed rates, and particle sizes were studied. In addition, 28 different mineral mixtures were tested with the dielectric separator. In typical tests, a sample of rutile and quartz gangue containing 10-percent rutile was concentrated to 62-percent rutile with 94-percent rutile recovery. A second-stage dielectric separation of the rutile concentrate produced a 92-percent-rutile concentrate. The overall rutile recovery for the two-stage dielectric separation was 86 percent.

Jan 1, 1980