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By H. Carroll

An ozone detector was built and evaluated for its applicability in smog-chamber studies. The detection method is based on the reaction of ozone with ethylene and the measurement of resultant chemiluminescence. In the first phase of evaluation, the detector's response to ozone was studied as a function of several instrument parameters, and optimum conditions were defined for the maximum and most stable responses to ozone. In subsequent evaluations, the method was checked for sensitivity, precision, and interferences and was compared with two alternative methods. Results showed the chemiluminescence method to be acceptably sensitive and precise for smog-chamber studies and superior to the Mast ozone meter and KI (colorimetric 1 percent neutral-potassium iodide method) methods in that it is specific for ozone.

Jan 1, 1972

By D. G. Kesterke

Research was conducted to determine the feasibility of extracting elemental oxygen from silicate-bearing melts by high-temperature electrolysis. The method was based on a modification of existing processes for electrowinning metals from their oxides dissolved in molten halide systems. Electrolyses were performed at temperatures ranging from 1,050° to 1,250° C in boron nitride cells that incorporated a silicon carbide cathode and an iridium anode. The electrolytes contained volcanic scoria as the oxygen source, plus mixtures of BaF2 and LiF as fluxing agents. Cell gases containing almost 14 volume-percent oxygen were obtained. The average anode current efficiency for several experiments of extended duration was calculated to be 55 percent. Cell design and operating conditions are described, and some of the problems associated with the process are discussed.

Jan 1, 1971

Develop a full-length-anchored roof bolt that is economical, nontoxic, nonflammable, and non-allergenic. Approach Grout roof bolts with a storable mixture of ultra-fast setting inorganic cement and water. How It Works A loose mixture of dry cement powder, and pinhead-size water droplets encased in waxy globules, are pack-aged in sausage shaped cartridges for storage and use. After the cartridge is inserted Into a drilled hole, the roof bolt is thrust In and rotated to mix the cement and water. The cement hardens in seconds, providing usuable anchoring strengths in minutes. Prior to filling of the sausage shaped cartridges, the microcapsules of water are Intimately mixed with the dry cement. The currently used grouting consists of a mixture of one part water (minimum) with three parts alpha-type gypsum cement and a minor amount of accelerator.

Jan 1, 1978

By L. J. Froisland

An integrated process for recovering metal from nonmagnetic auto-shredder reject scrap was investigated by the Federal Bureau of Mines. The methods used were air classification, water elutriation, screening, magnetic separation, handpicking, and heavy-media separation. Metal recoveries in this process were projected at 39 percent copper and copper alloys, 53 percent aluminum, 96 percent iron, and 98 percent zinc die cast. An economic evaluation of the conceptual process indicated that a facility designed to reclaim the reject scrap from 200 shredded automobiles daily could be profitable. Total investment in this plant was estimated at $321,000; the discounted rate of return before taxes was 53 percent.

Jan 1, 1975

By Jack C. White

The Bureau of Mines, in its efforts to insure the continued viability of the domestic minerals economy, has been engaged for several years in research on the extraction of alumina from domestic, nonbauxitic resources. Hydrochloric acid leaching of kaolin is one of the more promising technologies being studied for recovering alumina for feedstock to existing aluminum smelting capacity; 93 pct of this feedstock is currently imported either as bauxite or alumina. Organics contamination of pregnant leach liquor, originating during solvent extraction for removal of iron from aluminum chloride solution formed during hydrochloric acid leaching, causes rapid deterioration of the semihard rubber lining of process equipment. These organics were removed by a skimming tank-coalescer-activated carbon adsorption system. Organic levels of less than 10 ppm from the coalescer and less than 0.5 ppm from carbon adsorption were achieved. Analytical methods employing CC14 extraction and infrared spectrophotometry were developed to determine the organic content of both the liquor and the carbon. Mass transfer zones delineated in the carbon columns provide adsorption data for the design of larger systems.

Jan 1, 1981

By R. V. Ramani, V. T. Burgos, J. A. McClay

The systems contributing to the cost analysis, and the flow of data input and output related to these systems, are brought into focus in Figure 6. The various sub-systems of the Master Design Simulator provide the raw operating data basic to the cost model which, operating independently, accumulates the raw input, assigns costs to this data by standard or modified costing procedures, manipulates the costs into standard formats and outputs the data for managerial evaluation. Cost Modeling Direct costing methods are not complex in the sense that elemen¬tary arithmetic is employed using the same basic relations for each cost category. The basic cost model relations described above are illustrated in Figure 7. The greatest difficulty encountered in the transition from a dy¬namic systems simulation model to a costing model is the time frame of the input and output data. Dynamic simulation models utilize a small time increment, on the order of seconds or fractions of seconds, to analyze system operations and interactions. On the other hand, for cost computation and reporting, the smallest relevant time unit is the shift, with reporting periods expanding to days, weeks, months, and years. Complications arise in the accumulation of data for the various report periods due to the use of the Gregorian calendar by modern so¬ciety. The potential for simulation for the life of the mine, possibly in excess of 50 years, increases the complexity of the costing process

Jan 1, 1975

Reduce dust on long wall faces by using a gob curtain to lower air leakage Into the gob and raise the airflow along the face. Approach A brattice curtain (gob curtain) Is hung between shield #1 and the rib in the headgate entry forcing the ventilating air stream to make the 90° turn and stay on the face side of the shields rather than leaking into the gob. How It Works Air leakage is greatest in the headgate area because the gob behind the first few shields remains open due to the roof bolts in the headgate entry. In addition to the open gob, there is a large gap between shield #1 and the rib. Prevention of air leakage behind the shields is accomplished by the Installation of a curtain between the first shield and the rib extending from the roof to the bottom. The curtain Is advanced with the shield line each pass and is helpful In maintaining a sufficient air quantity along the face. The biggest Improvement due to this curtain is seen in the first 25-30 shields where the Increased air volume lowers dust concentrations through dilution.

Jan 1, 1981

By Dennis Dolinar, Christopher Mark, Gregory M. Molinda

In 1999, 2,087 unplanned roof falls were reported from 841 mines. Nearly 55% of all mines reported at least one roof fall, and nearly 17% of the mines reported five or more falls. In order to investigate the variables that contribute to roof falls, the National Institute for Occupational Safety and Health (NIOSH) compiled a national database of roof performance from 37 coal mines. Geotechnical factors and their effect on roof fall rates were compiled from over 1,500 miles of drivage. The factor that is the best predictor of roof fall rate is the Coal Mine Roof Rating (CMRR). For a low CMRR (#30), almost all cases have high roof fall rates. Conversely, high roof fall rates are rare for strong roof rocks (CMRR $ 60). Roof fall rates were also higher in deeper mines, probably because of greater stresses. Intersections were much more likely to fall than roadways, and four-way intersections were more prone to fall than three-way intersections. In a controlled comparison of the effect of increasing bolt length on roof fall rates, it was found that longer bolts reduced the roof fall rates in 11 of 13 cases. A relationship between the roof fall rate, the intersection span, and the CMRR was also found. Finally, a systematic method for tracking roof performance and geotechnical variables was demonstrated.

Jan 10, 2000

By L. B. Berger, W. P. Yant, R. R. Sayers

"At the request of the Chesapeake & Ohio Railroad Co. a number of tests were made to determine the temperature, humidity, and composition of the atmosphere in certain tunnels of that railroad between Clifton Forge, Va., and Hinton, W. Va. The purpose of these tests was to determine conditions in the cabs of freight locomotives while pulling trains through these tunnels. Tests were made of two types of locomotives, classified by the railroad company as the H-6 and H-7. Both are of the Mallet type, but the H-6 class has one pair of cylinders operating at boiler pressure and the other pair compound, whereas the H-7 operates all four cylinders at boiler pressure, thereby exhausting steam at a higher temperature than the H-6. It was desired to determine the relation between conditions on the H-6 and H-7 engines under comparable conditions of operation. This information supplements previous tests by the Bureau of Mines, discussed in its Reports of Investigations Serial No. 2624, entitled, ""Temperatures in Cabs of Freight Locomotives Passing Through Tunnels of Chesapeake & Ohio Railroad, 11 by s. H. Katz and E. G. Meiter, July, 1924. Three incidental tests of passenger engines were also made."

Feb 1, 1928

By R. W. Stahl

Increasing use of continuous miners, especially the boring type, has focused attention on the inadequacy of face ventilation in coal mines. The bulk of the machine, the rapid advance of working faces, and the increased liberation of methane from the larger expanse of freshly exposed coal surfaces have created ventilation problems that were unknown with conventional mining equipment. Ignition of gas, especially that caused by machine bits striking hard rock or pyritic inclusions, have increased at an alarming rate. As the mines penetrate beds under thicker cover at an ever-increasing rate of face advance, this problem will probably increase unless face ventilation is improved. A previous survey, described in Bureau of Mines Report of Investigations 5414, Auxiliary Ventilation of Continuous Miner Places, disclosed that auxiliary fans with tubing generally improved circulation of air and removal of gas at the face. The study here reported attempts to examine, face ventilation at various mines and to note any plan or innovation of. air coursing that industry might adopt to reduce the danger of gas ignition. ACKNOWLEDGMENT The mines visited were very cooperative in the study-and-generously supplied any data requested.

Jan 1, 1960

Provide a low-maintenance, reliable means of generating bubbles and controlling bubble size for column flotation. Approach Commercial sparger systems used in flotation columns to process minerals provide only limited means of controlling the size of bubbles generated and the rate of air injection. Generally, these limitations are a detriment to flotation performance, particularly in recovering coarse or fine mineral particles. In addition, conventional bubble generation systems require frequent maintenance, often requiring shut-down of the column itself for repairs. To permit greater control of the bubble size generated in the flotation column and to eliminate the counter-productive problems associated with the operation of current air sparger systems, the Bureau of Mines investigated alternative methods for generating bubbles. Based on the investigation, an external bubble generation system was designed, developed, and laboratory and commercially tested.

Jan 1, 1987

By P. G. Barnard

Losses of alloying metals in furnace flue dusts, grinding swarfs, and mill scale produced during the manufacture of stainless steel are substantial. About 25 million lb Cr, 8.7 million lb Ni, and 150,000 lb Mo and other critical metals can be made available annually for recycling by a process developed by the Bureau of Mines. Stainless steel wastes pelletized with a portland cement binder were reduced in a small electric-arc furnace by a two-stage process to produce a recyclable alloy containing Cr, Ni, Mn, and Fe. The initial reduction was with carbon; the second, with ferrosilicon. Results are compared with previously reported laboratory induction melting tests. A 2,000-lb demonstration test of the process in a commercial electric-arc furnace is also described. Data are also presented on three 1,500-lb tests made using various slag conditions in the electric-arc furnace. Recoveries up to 99 pct of the Fe, Cr, and Ni contents of stainless steel wastes were obtained in using the process.

Jan 1, 1977

Hang ventilating air curtains so that they can be installed, moved, opened and closed more easily than curtains that are spadded or nailed in place. Approach Low-leakage plastic curtains fitted with grommets along the top were threaded onto a steel cable which is suspended from roof bolt plates. The system was tested in two mines. How It Works The curtains are threaded onto a steel cable which is suspended from roof bolt plates by S-shaped hooks. See Figure 1. The outby end of the cable is reeled off a hand operated winch; the inby end of the cable is anchored to a roof bolt plate by means of a cable grip and an S-shaped hook. To install the curtains the following procedure is used. First, the winch is located at least 5 feet outby the last open cross-cut. The base of the winch can be secured to the mine roof with short roof bolts, only about a foot long.

Jan 1, 1978

Increase the safety of underground mine workers by minimizing hazards associated with rerailing mine cars after derailment. Background and Approach A serious operational problem in underground mines is the task of rerailing mine cars. Current rerailing practices are not only hazardous but are inefficient as well. Most methods involve pulling the derailed car back onto the track with a locomotive. This causes damage to the road bed and is not effective on curves or in situations where the car's wheels are too far from the rails. Jacks, wooden props, and pry bars are also used to raise or lower cars back onto their tracks but methods involving these tools require much strenous manual effort by mine workers, thus posing possible serious injuries. The problem is further compounded by the cramped, narrow confines of the underground mine environment which allows no space to permit use of cranes or other surface railroad rerailing techniques. The Bureau of Mines, aware of these problems, investigated improvements in current underground rerailing methods. Through a cooperative effort with Hoesch MFD, a system was designed and modified that can be easily carried into the mine by workers and quickly assembled at the derailment site. The system is hydraulically and pneumatically powered rather than reliant upon manual operation.

Jan 1, 1986

Develop a training program to help mine workers effectively fight small fires in underground Goal mines. Training would enable miners to make rapid judgments on whether to attempt extinguishment, and how best to use the firefighting equipment on hand. Approach Fire reports were analyzed to define and delineate physical and behavioral variables which affect firefighting activities, and to determine effective procedures for extinguishing small fires. A course was then designed to train miners in such procedures. Finally, the course was reviewed by industry experts and administered to a group of miners to determine needed revisions and to validate the course. How It Works Analysis of fire data showed that six items should be emphasized in teaching proper fire response: 1. Alertness to fire potential. 2. Immediate power cutoff. 3. Internal, external communication. 4. Teamwork in fighting fires. 5. Role of ventilation and position of men inby the fresh air side. 6. Effective use of fire suppressant materials.

Jan 1, 1983

Provide an operator cab to assure protection, comfortable use of controls, and good visibility. Approach A cab which raises and lowers by pivoting about d horizontal axis was Installed on two S&S cleanup tractors and tested in two underground working mines. How It Works Hydraulic cylinders actuated by a lever inside the cab cause the cab to pivot about a horizontal axis. This action raises or lowers the cab height. The total cab excursion is 14 inches. A release valve in the hydraulic system allows the cab to lower automatically if struck by a roof load or overhead obstruction. The pivoting action of the cab is engineered so that the operator maintains comfortable use of all controls at all cab heights. The movement is such that the angular relationship of the operator's ankles With the tram and brake foot controls IS consistently within 90 to 100 degrees. Figure 1 outlines the approximate position of the operator at three cab elevations.

Jan 1, 1977

By Vijia K. Karra

The goal of aggregates producing companies across the United States is to ensure their workers go home safely each day. At the National Institute for Occupational Safety and Health (NIOSH), researchers are pursuing this vision of safety and health through a fact-finding approach for reducing injury illness in various mineral sectors. Surveillance data from Mine Safety and Health Administration (MSHA) has been the source for such analyses. It helps to focus research efforts on key machinery, workers, and their tasks. The second installment of this two-part series follows last month's focus on crushed stone.

By B. W. Madsen

Bureau of Mines research to recover arsenic from mining industry waste material and process streams is reported. Batch and column approaches were investigated for adsorbing arsenic from acid leach solutions and ion-exchange eluate solutions with hydrated titanium dioxide granules. A method for producing hydrated titanium dioxide granules was devised to provide material suitable for use in a packed adsorption tower. Selective adsorption of arsenic from acidic leach solutions was achieved. The loading capacity of arsenic on the granules was 14 wt-pct when synthetic solutions were used, but lower when actual leach solutions were used. Other elements in the leach solution were Zn, Cd, and In. The granules were used in an attempt to lower the arsenic content in a solution containing 0.95 g/l W and 0.027 g/l As from a process devised by the Bureau of Mines to treat Searles Lake brine. The arsenic content was lowered to less than 0.001 g/l, but unacceptable amounts of tungsten also were adsorbed by the granules. Adsorbed tungsten was partially stripped with pH 11.5 NaOH, and both tungsten and arsenic were completely stripped with 5M NaOH solution. Repeated loading and stripping of the granules had no effect on the loading capacity for arsenic.

Jan 1, 1983

Provide mine operators with a quick means of identifying the effect of cutting system changes on relative dustiness at the mine face, by developing an interactive computer program for drum-type coal mining machines. Approach A program which simultaneously evaluates machine parameters, coal seam parameters and mine operator-controlled parameters for their effects on relative dustiness has been developed for use on any minicomputer using BASIC computer language. How it works The interactive computer program allows mine operators to make one or more changes at a time to their cutting system to determine how these changes affect relative dustiness of the face. Using this program, mine operators can find the optimum cutting system configuration to minimize dust using their seam conditions and their equipment specifications. The mining machine variables include: number of vane bits, number of gage bits, number of starts, vane wrap, number of end ring lines, rpm, advance rate, ton/min, percentage of time spent cutting per shift, and airflow.

Jan 1, 1986

Reduce longwall equipment transfer time between panels by utilizing a predriven recovery room, and thus eliminate the premove preparation associated with most equipment recovery methods. Background and Approach The recovery point for a retreating longwall is a predetermined position near the end of the panel where mining is terminated and equipment is disassembled and removed. However, to prepare for equipment removal at the recovery point, bolting and wire meshing arc required before the recovery point is reached. Usually, preparations for equipment recovery begin about 35 ft from the recovery point, significantly impeding the normal rate of advance of the longwall and, consequently, production. Recently, BethEnergy Mines, Inc., and the Bureau of Mines cooperated to evaluate the applicability of utilizing predriven recovery rooms to improve longwall equipment recovery. A predriven recovery room is an entry driven parallel to the longwall face at the end of the panel, having standard dimensions (for that particular mine) and supported with bolts, wire mesh, and supplemental support. The preparation of this entry is completed before it experiences mining-induced effects from the approaching longwall face. This enables the face to continue to mine at its normal rate of advance until the panel is completed. The supplemental support is required to control the loads imposed by the front abutment and is the most vital component of the recovery room.

Jan 1, 1989