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By S. H. Ash

NINE-TENTHS of the total anthracite deposits of North America are in Pennsylvania. Corrosion of pumping equipment by acid mine waters has been experienced at tremendous cost by mining companies in the anthracite region of Pennsylvania, for many years in many ways. The design and specifications of the large centrifugal pumps as provided in the proposed mine-drainage system (7-35, 45, 46, 48, 54, 64, 70, 71)° make it imperative that a metal or alloy be recommended that has the highest corrosion resistance and, at the same time, acceptable properties suitable for general workability (welding and machining). This report presents data on the corrosive and erosive effects of acid mine waters in the anthracite region on metals and alloys for pumping equipment and drainage facilities necessary to remove or control this water.

Jan 1, 1955

By F. E. Armstrong

This Bureau of Mines publication reviews 237 papery on radiometric prospecting, which is the measurement of naturally occurring radioactivity in the earth's surface and its application to petroleum and natural gas exploration. Many theories and documented surveys are listed in both support and refutation of this reported phenomenon, and the Bureau of Mines is conducting research to obtain direct field information in order to determine the statistical credibility of a radiometric method of predicting petroleum accumulation.

Jan 1, 1973

By D. K. Caddel

Several problems exist with the present design of coveralls used by miners in low coal (seam height 48 inches or less). The back portion of the coveralls often tears when roof bolts or rough areas in the roof are hit. Movement in the shoulder area is restricted. Female low coal miners find it difficult to purchase coveralls that fit properly, and must remove both their hard hat and safety belt in order to urinate and defecate. The objective of this research was to design coveralls which would alleviate these problems. The following features were incorporated into the coveralls; padding in the upper back area to avoid tearing, an action pleat in the shoulders to increase mobility, an inseam zipper to more easily allow miners to perform their bodily functions, and reflective tape to increase visibi¬lity of the miner. A heavyweight denim fabric was used to increase warmth and durability of the coveralls. The coveralls were assessed K long four parameters (comfort, safety, worker productivity, and fabric suitability) using both an in-field assessment by low coal miners and simulation studies. The experimental coveralls proved superior to conventional coveralls along all four parameters. Work clothing sizes for female miners were developed.

Jan 1, 1982

By Oliver C. Ralston

The Nonmetals Division studies problems relating to the use of minerals, many of which are important to national defence for purposes other than the extraction of metals. In fact, virtually all of the work of the division has been diverted to investigations pertaining to better use of the Nation's natural nonmetallic is resources as weapons of defense. The experiment stations of the division are at Norris, Tenn.; Tuscaloosa, Ala.; Seattle, Wash.; and College Park, Md. Studies involving the application of electric power to the nonmetallic minerals are conducted at the Electrotechnical Laboratory at Norris, and investigations on mineral-dressing treatment are conducted mainly at the Southern Experiment Station at Tuscaloosa. The cleaning and preparation of coal are studied at both Tuscaloosa and the Northwest Experiment Station Lit Seattle (other projects relating to utilization of coal are conducted by the Coal Division of the Bureau of Mines). Problems covering the use of minerals and fundamental problems as to their properties are studied at College Park.

Jan 1, 1941

By Maria I. De Rosa, Charles D. Litton

The National Institute for Occupational Safety and Health (NIOSH/PRL) conducted a series of large-scale experiments to evaluate the effectiveness of optical flame detectors, photoelectric smoke detectors, and combined ionization and photo­electric smoke detectors for rapidly detecting mining equipment cab fires. The detec­tor alarm times were then used to trigger the discharge of a fire inerting system inside the cab to suppress cab material fires. This paper discusses the types of fire detectors tested, the experiments that Were conducted, and the results that were obtained. Con-" elusions are that rapid detection of equipment cab fires can be achieved to trigger the discharge of a fire inerting system inside the cab to protect the operator in the cab.

By Robert M. Doerr

The research objective was to determine the effect of vanadium alloy additions on the oxidation behavior of cobalt-nickel Alloys. Eighteen alloys were reacted with 0 2 at 0.5 arm and 1,351°, 1,389°, and 1,429° K. The alloy compositions consisted of Co-Ni master alloys (0, 22, 50, 70, 91, and 100 wt pct Ni) with V additions of 0, 0.9, and 2.7 wt pct. Large early deviations from, or changes in, the parabolic rate constant were encountered, but the reaction rate in most cases declined approximately in accordance with the parabolic rate law. Relatively, the vanadium degraded the oxidation resistance most at the highest nickel contents. In some cases, melting of the oxide was inferred from microscopic evidence and X-ray diffraction measurements disclosed the presence of low-melting vanadates.

Jan 1, 1970

By J. S. Dunning

One Federal Bureau of Mines research goal, to minimize requirements for domestically scarce mineral commodities through conservation and substitution, can be accomplished by utilizing more abundant elements such as iron, molybdenum, and titanium. An example of this research is the study of precipitation-hardening, iron-base alloys containing molybdenum and titanium, as substitutes for the high-tonnage stainless steels that are high in imported nickel and chromium. The precipitation hardened iron-base alloys are strengthened by a dispersion of the ternary Laves phase, Fe2 (Mo, Ti). Aluminum and chromium additions changed the solid solubility limits of molybdenum and titanium in a-iron and affected the composition of precipitating phases. A baseline composition of Fe-7Mo-2Ti was selected to study the effects of aluminum and chromium additions on the precipitation-hardening mechanism and microstructure and was also used in studies of mechanical properties and oxidation resistance. The study yielded workable, precipitation-hardening alloys, with elevated temperature strengths equivalent to or superior to types 304 and 316 stainless steels. Chromium and aluminum additions in combination were more effective in providing oxidation resistance than either addition was alone.

Jan 1, 1980

By Roy F. Abernethy

All samples tested showed some loss of heating value for the 5-month period under all 4 storage conditions. The losses increased as the time of storage increased, with the pan-storage samples showing somewhat greater losses than those in cans. The individual daily analyses for the first 2 weeks and the analyses every other day for the third and fourth weeks of storage vary within the approximate tolerance of the test for heating value. During the first 2 months of storage the changes in heating values were not Significant for the samples from Pennsylvania, Indiana, and Colorado. The Ohio coal indicated some loss by the end of I month, which increased to a value measurable with certainty by the end of 2 months. These data show that (1) small changes may occur even to samples in closed cans and (2) the laboratory sample should be handled as expeditiously as is practical until the analysis is completed. The statement by the ASTM that "If the B.t.u. determination is an important consideration in the sale of coal, the time elapsed between sampling and analysis shall not exceed 30 days,"3/ is quite adequate for 3 of the 4 coals tested. The change in the Ohio coal stored for 30 days is merely indicated and could not be determined with certainty by the techniques normally employed. The data on free-swelling indexes determined on can samples, after 30° C. air drying, show that only the Indiana coal lost more than one unit in free-swelling index number in 120 days. No significant changes were observed with the samples from Pennsylvania, Ohio, and Colorado in the 5-month period.

Jan 1, 1958

By F. G. Miller

[Petroleum technoloF;istz and 1 rot-re s s ive OT e:?ztors. con stantl;, are striving to increase the percentage of oil that y to recovered from reservoir rocks throe::;:: wells. The exhaustive studies that have been made of the function of natural r:; as in t h-_ T r odI action of oil, for cx<n.mTnle, have aidedd of.erators greatly in incroasin,&apos; the q-:Arrntity of oil recovered from reservoirs. i.rtural gas dissolv3d in ar--d otinerwwisa &apos;1s&apos;.,ocintjd under rre3suro with oil in roscrvoir roci.s, howover, i:; not the only source of energy available for moving oil through sa&apos;:&apos;l to wells. l becoming "reservoir-energy conscious&apos;t engineers hr-vo -d o^.rued t}:-Lt in many petroleum reservoirs the edgewater flanking t -,e oil accum.-,lation conetitutos a potential source of onergy capable, tL-ou;_h rro? gr control, oil&apos; increasing oil-recovery efficiencies materially. i o ]enter is ti-.-,, on-cronchinunt of water into the oil- and gas--fillod ?art of the reservoir considered as an evil to be combatted by devious mot&apos;:r:ci :i,.t r,ttL er a natural conseque::c4, incident to the withdrawal of oil nna gas from the wells, that nay be T.usod advantrt eou ;ly in lonr`t}toning tr e r&apos;lowin g lift of wells a.nd, i norcas in:; the economic recovery of oil and Little is known about the by which water off: oratos in driving nil throe:gh reservoir roc:-.:,, nd i:. a scorcity of rubli:;Lad informs-¬t .on nn rates of :)Ov.:m.,:- t of : r.tcr ..at v:1:11 res,-_lt in ^r i-nu oil recoveries. Bureau of :fines engine_:? ; - reciate. the r,aucity of scientific knowledge or. the &apos;test methods of a,r.lying the natural water arive to in¬crease oil-recovery efficiencies ant ,i.;?l __-itir?,~ ting irties that will, they hope, Contribute to t.1&apos;.e T ros?Jr.t. small _ %nd of information now av tilable on tt:e cubjoct. This r».crt a oyno-.::is or brief comrilnt.ion of r,ublished data and thought accuinulnt.~d so far, to la)or;~.tory ox-:erimnntrr¬tiorn and, further rosoarch on the z_rrinciplos unri;rlyir..g the natr.rr+1 eater drive no it nffocts oil recovery. :Lie writer:: Lore that t.i.c cx-nositiorn of a?rzilable inforr-at ion i rcs?r.toi in the rernrt r .-II .i ,.1rtt cor_jt_-i:ctive tho.-_.I_t and efforts loadir,-z to -:ard more con.r .ote extraction n;&apos; o tl from reservoirs.]

Jan 1, 1938

By G. L. Fitzpatrick

Preliminary results of an experiment in seismic holography indicate that the techniques of acoustical holography may be successfully used with seismic waves to determine the size and general shape of underground objects. This experiment was carried out under field conditions on a moderately large scale compared with the typical laboratory experiments in acoustical holography. The object to be mapped was a 100-foot-diameter, spherical, low-velocity zone of explosively fractured rock in oil shale at an average depth of 80 feet. The seismic wavelength of the Fourier component wave used in making the seismic holograms was 50 feet at a frequency of 140 cps. The hologram sampling aperture was 226 feet square and was sampled by 441 geophones in a 21 by 21 rectangular array. One novel aspect of the experiment was the use of a wide-band polychromatic explosive source of seismic waves rather than a narrow-band quasi-monochromatic vibrator source. A successful laser reconstruction of the object image from a lensless Fourier-transform hologram in the form of a 5/l6-inch-square photographic transparency is illustrated. The size of the underground object measured from the laser reconstruction of the object and the size inferred from a knowledge of the amount of explosives used to fracture the site and the tensile strength of the oil shale are found to agree.

Jan 1, 1972

By K. Y. Haramy

Coal mine bumps involve the violent, rapid failure of coal and rock around a mine excavation. Deep coal mines with strong roof and floor rocks and high-stress conditions frequently experience face and rib bumps. The bump problem is becoming more severe as mining depth increases, prompting efforts to control high stress in advance of mining. This Bureau of Mines report presents a review of the most widely used methods to detect and destress high-stress zones along coal faces and an investigation of stress-related bump problems and destressing techniques at a cooperating mine. Geotechnical instrumentation and microseismic methods were used to better understand bump occurrences in underground coal mines. Laboratory tests of the drilling-yield method for high-stress detection were conducted to determine the correlation between the volume of cuttings obtained and the magnitude of the applied stress at various confining pressures. A three-dimensional, multiple-seam computer modeling program, MULSIM, was used to evaluate the effectiveness of stress-relief methods. Modeling results indicate that dangerously high-stress areas can be controlled by either proper planning or destressing. Proper mine planning guidelines and destressing methods such as volley firing, hydraulic fracturing, and auger drilling are discussed.

Jan 1, 1988

To mine uraniferous sand-stone in an economically feasible and environmentally compatible manner without placing men underground. Approach Uraniferous sand is remotely extracted through a single borehole by cutting Into the are around the borehole with a high pressure water Jet, and pumping the resulting slurry to the surface. How It Works A 16-inch-diameter borehole Is drilled from the surface down into the burled mineral deposit, and the mining tool Is installed. High pressure water Is released as a jet from a nozzle In the mining tool to erode the are, forming a slurry that flows to the bottom of the cavity. The slurry Is drawn Into Inlets located near the bottom of the drill string. See drawing. After being pumped to the surface, the slurry is weighed, metered, and checked for radioactivity. It is then deposited Into one of a pair of sumps. Water collecting in the sumps drains Into an adjoining pond for reuse. Thickened are In the sumps is removed and placed In piles.

Jan 1, 1978

By T. N. Williamson

Most U.S. coal production is bituminous coal. Some 90% of current production comes from a geographical area enclosed in a circle with a 300 mile radius and its center at about Huntington, West Virginia. There are important underground coal production areas in the western parts of the United States as well. Most U.S. coal production comes from fairly level seams, many of which pitch rather uniformly only a few feet per mile. Usually there will be several overlying seams of varying thicknesses, separated by several tens of feet. Fig. 1. 1. Seams have minor local undulations but these? are small enough not to be a major consideration in a horizontal drilling research program.

Jan 1, 1970

By J. D. Davis

THIS REPORT gives results of an investi¬gation of the carbonizing properties of coals from Pittsburgh bed, Jamison No. 9 mine, Marion County, W. Va., and from Upper Freeport bed, Bull Run No. 1 mine, Preston County, W. Va. The study included Bureau of Mines-American Gas Association tests at 800° and 900° C. and various chemical and physical tests designed to evaluate the plastic, expanding, and agglutinating properties of coal. A blend of each coal was carbonized in the 500-pound slot oven. The carbonization sample of Pittsburgh coal contained 2.7 percent moisture, 35.8 percent volatile matter, 54.4 percent fixed carbon, 7.1 percent ash, and 0.9 percent sulfur. It contained 60.9 percent fixed carbon on the dry, mineral-matter-free basis and had a heating value of 14,780 B. t. u. per pound on the moist, mineral-matter-free basis. It therefore ranks as high-volatile A bituminous and was blended with low-volatile Pocahontas No. 3 coal. Upper Freeport coal contained 2.8 percent moisture, 27.7 percent volatile matter, 60.9 percent fixed carbon, 8.6 percent ash, and 1.0 percent sulfur, as carbonized. It contained 69.5 percent fixed carbon on the dry, mineral-matter-free basis and therefore ranks as medium-volatile bituminous. It was blended with high-volatile A Pittsburgh coal from Allegheny County Pa.

Jan 1, 1952

By G. N. Schrauzer

Work has been carried out in the development and testing of carbon monoxide (CO) detection devices which use silica-gel impregnated with metal salts. If carbon monoxide is present, the ?detection gel? (the treated silica-gel) changes from a yellow to a blue-green or blue color. The detection gel "regenerates", i.e., returns to its original yellow color, within 4-24 hours after removal from air containing CO. The detection gel exhibits a threshold of CO response which can be adjusted over a wide range of CO concentrations, typically from 50-500 ppm in air. The preparation of detection gel using salts of palladium, molybdenum and copper is described. Also reported are the results of testing the detection gel&apos;s response to carbon monoxide under varying conditions of temperature and humidity and in the presence of some potentially interfering gases. Low levels of hydrogen sulfide (~ 5 ppm)1 nitrogen dioxide (< 7 ppm), and acetylene (> 200 ppm) were found to affect the detection gel. Temperature and humidity were also found to affect the detection gel&apos;s response. Increasing temperature shortens the gel?s response time while increasing the humidity delays the gel?s response and alters the threshold of the gel. A brief discussion of the further research and development necessary to stabilize the detection gel?s desirable characteristics is included. Descriptions of testing equipment and procedures are covered in detail.

Jan 1, 1978

By H. C. Fowler

Hydrogen sulphide associated with the gasps and vapors from certain crude oils now produced in the United States has forced a serious health and safety problem upon the petroleum industry. Although the presence of hydrogen sulphide in or occurring with Mexican crudes has been known for some time, it was not until recently that crude oils which give off poisonous amounts of hydrogen sulphide have been produced to any extent in the United State. The injurious effects of this poisonous gas were first recognized by the refiners along; the Atlantic and Gulf Coasts upon receiving shipments of crude petroleum from Mexico. The problem of combating the hazards of the gases and vapors given off by this petroleum become more important as the use of Mexican crude increased. In 1925, the Bureau of Mines and Public Health Service under cooperative agreement with the American Petroleum Institute, studied the causes rend effects of hydrogen sulphide poisoning. Bureau of Mines Bulletin 2312 is report of this investigation, and although written with special reference to refineries, it nevertheless contains much information that is of value to the producer of petroleum.

Jan 1, 1927

By G. P. Houston

This is the final, report submitted for the Contract No. H0220002 with the U. S. Bureau of Mines for the design and development of a Permissible Automatic Data Acquisition System (PADAS) to measure and record roof stresses in underground mines Basically the PADAS is a portable, battery powered, 24-channel data acquisition system designed for safe unattended operation of up to 30 days duration in explosive environments. The unit will accommodate twenty-four pressure transducers or eight borehole deformation gages (or any combination) at distances up to 300 feet from the PADAS to measure pressures up to 10, 000 psig. All 24 channels as a selected group are scanned sequentially at one of several selectable rates.

Jan 1, 1973

Horizontal holes are drilled underground into coalbeds to control methane flow from ribs and active face areas and to make gas pressure measurements in coalbeds. Gas pressure measurements are made by drilling the same hole incrementally. After each increment, the hole is filled with some type of packers and allowed to reach equilibrium before a gas pressure reading is taken. As the length of hole increases, more packers are required to effect a seal and obtain a reliable pressure measurement. Problems have been encountered in obtaining satisfactory packer seals due to the friable nature of the coalbed. New methods of packing the holes must be used. Therefore, this project was established to evaluate materials and develop a new technique in which a semiliquid and/ or rigid type grout could be placed in the hole to provide satisfactory sealing.

Jan 1, 1972

By J. J. Lukasko

The U.S. Bureau of Mines developed an alternative electrochemical process for the production of calcium metal. The current industrial practice is costly, complex, and inefficient. The Bureau method involved electrowinning of a calcium-tin alloy followed by electrorefining to produce calcium metal. In the electrowinning cell, CaCI2 was fed to a KCI2-CaCI2 electrolyte. The calcium was electrowon at 6500 C into the pure molten tin cathode until the cathode contained 7.5 wt pct Ca. Current efficiency for electrowinning averaged over 90 pct. The resulting calcium-tin alloy served as the anode for the electrorefming cell, which employed a [CaC~-CaF2] fused salt as the electrolyte. Calcium metal was electrorefmed at 8500 C with a current efficiency of 85 pct based on calcium metal recovered. The calcium metal analyzed 99.2 pct, which is purer than commercially produced calcium.

Jan 1, 1990

The lignite deposits of the United States represent a huge potential source of fuel for power generation. It has been estimated that lignite constitutes about 24 percent of the remaining National reserves of solid fuel on a tonnage basis and about 15 percent of the reserves on a B.t.u. basis. (See sec. 3, part 1.) The major portion of these reserves is in North Dakota. Lignite has been used locally for domestic heating since the first settlers burned it at forts and fur-trading posts as early as 1855. Some of the first studies of the use of lignite in steam boilers were conducted by the Federal Bureau of Mines from 1910 to 1920 (15, 19) 1/ However, the commercial utilization of lignite as fuel for producing power developed slowly. Not until about 1925 was any really successful lignite industrial fuel-blaming equipment developed. Since then the commercial use of lignite as a fuel for producing power has been increasing steadily.

Jan 1, 1954