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By T. A. Kubala

Electric discharge ignition has been reinvestigated in a modified Hartmann apparatus for lycopodium powder with air. Minimum stored energy to ignite air dispersions of lycopodium was 25 to 30 mj; ignition occurred with 1 gram of lycopodium dispersed into the 2.7-liter vessel. Ignition energy was measured as a function of the weight of powder used, although some reservations are expressed concerning the uniformity of the lycopodium-air mixtures. In particular, wall layers of lycopodium, remaining after dispersal of 1 gram of lycopodium, were as easily ignitable as the most easily ignited air dispersion. Thus, an unanswered question has arisen concerning the role of surface coatings in the flammability of all marginally ignitable mixtures.

Jan 1, 1981

By F. Chen, L. J. Gaydos, D. C. Kuhn, Demersm L. M., S. C. Sun

"Summary: In this report the differential regulation of NF-KB and nitric oxide (NO) was investigated in the mouse macrophage cell line RAW 264.7 following exposure to a mineral dust (silica) and /or an endotoxin (Lipopolysaccharide, LPS). The results indicated that silica and LPS can significantly induce the activation of NF-KB as well as elicit enhanced production of NO in RAW 264.7 cells as part of an early inflammatory response mechanism. A 24-hour time-course study showed that NO release from these cells continued to increase following the initial stimulus by LPS or silica. In contrast, activation of NF-KB was maximal at 6 hours and then showed a steady decline to 24 hours. The production of NO was suppressed by protease inhibitor and antioxidant, both of which block the activation of NF-KB. Surprisingly, the use of an NO synthase inhibitor resulted in an enhancement of NF-JCB activation. These findings suggest that NO produced in macrophage cells in response to an inflammatory stimulus like silica or LPS my be linked to a negative feedback role on the activation of NF-KB. It is now accepted that nitric oxide (NO) plays a pivotal role in the inflammation response process when macrophage cells are activated by a pro-inflammatory stimulus (l). Production of NO is dependent on the activity of the enzyme nitric oxide synthase (NOS). Up until now, at least three distinct genes have been described which encode different isoforms of NOS. NOS has been cloned from a variety of different mammalian cells, including constitutive neuron NOS, constitutive endothelium NOS and inducible NOS (2). Macrophages appear to be the principal cellular source for the inducible form of NOS (iNOS) activated in response to an inflammatory producing event. The mechanisms subserving the regulation of the iNOS gene and NO production have been under intense investigation in recent years (3-5). Several binding sites for transcriptional factors have been identified in the promoter region of iNOS gene, including NF-lCB, AP-1, NF-IL6, Oct-I to cite a few (5). NF-KB appears to play a"

Dec 1, 1996

By William H. King

Preliminary examination of the Virgin River manganese deposit was made by C. H. Johnson, Bureau of Mines engineer, in March 1941. During, April and May 8 trenches were dug, a 48-foot inclined shaft was sunk, and 719 linear feet of channel samples were cut. McKelvey and Wiese, of the Federal Geological Survey, completed mapping the deposit, including the entire area of overlying formations comprising the point of land between the outcrop and Lake Mead. The geologic maps, maps, and ore estimates resulting from these examinations formed the basis for a preliminary report by C. H. Johnson, who recommended further exploration by diamond drilling.

Jan 1, 1949

By Jr. Blake

This work was done to determine the technical feasibility of using the Pedersen process to produce cell-grade alumina and an iron byproduct from the high-silica and titania bauxites of the Pacific Northwest. Smelting of these bauxites with lime and coke at about 1,750° C in an electric arc furnace produced calcium aluminate slags in which at least 80 percent of the alumina was leachable by sodium carbonate solution. After a lime-desilication of the sodium aluminate leach liquors, neutralization of these solutions with carbon dioxide resulted in precipitation of an alumina hydrate of sufficient purity for calcination to cell-grade alumina. Recoveries of byproduct iron averaged over 90 percent; however, the iron contained about 1 percent phosphorous and would require additional refining. Additional small scale tests on these slags showed the following: (1) Titania had little effect on leachability if sufficient additional lime was added to form calcium titanate (CaO.TiO 2); (2) a slag containing about 14 percent silica required a slower cooling rate than one containing 7 percent silica for formation of high percentages of soluble aluminates; and (3) high-silica slags leached better at room temperature for long periods than at 65° C for shorter periods, but low-silica slags leached well by either method.

Jan 1, 1967

By David L. Bickel

Stress-relief techniques and instrumentation have been developed through many years of research in the Bureau of Mines and successfully used to determine the in situ state of stress in rock. This report describes the Bureau's three-component borehole deformation gauge and the drilling equipment and accessories used with it. Operation and calibration procedures for the deformation gauge are discussed in detail, along with site selection and overcoring procedures. Information and references included in this publication provide a guide to the Bureau's cover-coring method for determining rock stress.

Jan 1, 1985

By A. L. Murray, P. A. Surgeon

The Spring Canyon Mine Rescue Association is a cooperative association supported jointly by five coal-mining companies located in Spring Canyon, Utah. The properties of mining companies the Carbon Fuel Co, Rains , Utah, the Liberty Coal Co. , Latuda, Utah, the Standard Coal Co. , Standardville , Utan, the Spring Canyon Coal Co. , Storrs , Utah, and the Peerless Coal Co. , Peerless , Utah about a mile apart and normally employ a total of 915 men , 733 underground 182 on the surface . and The Association was organized on July 5, 1921 , and Rudolph Clark, fomerly first - aid miner on U. S. Bureau of Mines Rescue Car 11 , was placed in charge. as manager . A board of directors made up of a representative from each of the cooperating companies (usually the mine superintendent ) is the governing body of the Association and the expenses are prorated on a basis of the production of each of the five mines . The Association maintains eight sets of Gibbs rescue apparatus and a motor truck fitted up as a combined rescue truck and ambulance . Additional apparatus are to be purchased . Standardville is the central camp in the canyon and has been made the headquarters of the Association . The apparatus are now kept and the truck housed in a small station, but plans have been prepared for a large station which will be built this summer . This new station will have a large apparatus room , a test chamber, a suitable room. for training, and a garage on the first floor, while above will be the living quarters of the manager . There is a good road through the canyon and the other camps are all within two and one -half miles of Standardville .

May 1, 1922

By L. C. IlsLey

A list of permissible mine equipment, tested and approved p or to July 1, 1934, was published in Bureau of Mines Information Circular 6813/. The present list4/ includes virtually all the electric air compressors, coal drills, mining machines, loading machines, conveyors, mine pumps, room hoists, mine telephones, rock-dusting machines, switches, electric cap lamps, flame safety lanes, electric hand and trip lamps, electric flood lamps, methane detectors, blasting units, storage-battery locomotives, tandem locomotives, mower trucks, and concrete mixers tested and approved by the Bureau to January 1, 1937. The system under which these devices were tested permits the manufacturer, after his equipment has passed certain tests prescribed by the United States Bureau of Mines, to mark his equipment with a seal showing that it has been approved by the Bureau. These tests are designed to insure that equipments have the minimum requirements for safety in use. The only object of the bureau in making such tests and publishing lists of permissible equipment is to help decrease the hazards of mining.

Jan 1, 1937

By J. D. Ramsdell

The study described in this report was undertaken to obtain information on the character and effect of antimony additions to titanium. The availability of high-purity, low-hardness titanium metal, resulting from fused-salt electrorefining techniques, permitted a reassessment and evaluation of the physical behavior of titanium-antimony alloys. Alloys, based on several grades of titanium containing up to 10 percent antimony, were arc-melted and processed to sheet by hot and cold rolling. Properties and characteristics were evaluated by hardness tests, hot and cold rollability, annealing treatments, metallographic examination, and tensile tests.

Jan 1, 1960

By S. S. Clarke

This paper on methods and costs of mining at the Westside mine, in the Tri-State zinc-and lead-mining district (Missouri-Kansas-Oklahoma), is one of a series being prepared by the Bureau of Mines on mining practices, methods, and costs in various mining districts of the United States. Methods and equipment used in drilling, loading, and underground transportation have changed radically since the latest Bureau of Mines publications2/ on mining methods in the district were published more than 20 years ago. More efficient methods and machines have been developed in order to maintain low operating costs in the face of rising labor and supply costs and lower grade ore. The rate of conversion to mine mechanization was disappointing at times; local conditions required the development of special equipment, and available rock-moving machines had to be remodeled and strengthened.

Jan 1, 1957

By Donald F. Reed

In its investigation of old, abandoned, lead-zinc mines at which records of operations are not available, in 1914 the Bureau of Mines dug surface trenches anti', in 1947 It diamond-drilled three holes at the Albright Farm deposit in Sinking Valley. Some good lead-zinc ore had been extracted from veins in dolomitic limestone during the time of the American Revolution and as late as 1870. Since that time the only activity was sporadic prospecting and developing. Thu Bureau of Mines disclosed two additional veins by surface trenching, but diamond drilling failed to find significant lead-zinc mineralization.

Jan 1, 1949

By N. S. Dalal, X. Shi, P. M. Gannett

"Chromates are known to induce tumors (1, 2), mutations (3), and DNA damage (4-6). However, the underlying biochemical mechanism(s) is (are) not fully understood (6). Recent studies have indicated that hydroxyl (·OH) radical may play an important role (7-11). The mechanistic studies of Cr(Vl)-related ·OH radical generation in biochemical systems have shown the reaction of a Cr(V) species with hydrogen peroxide (H20 2 } through a Fenton-like mechanism to be one of the important steps (9-11): Cr(V) + H20 2 - Cr(VI) + ·OH + OH-. (1)In biological systems the Cr(V) species are generated via the reduction of Cr(VI) by a variety of components, such as microsomes (12), mitochondria (13), mitochondrial electron transfer complexes (14), and at least three flavoenzymes (glutathione reductase (GSSG-R),3 lipoyl dehydrogenase, and ferredoxin-NADP+ oxidoreductase) (9, 15, 16). In the case of flavoenzymes, Cr(V) formation is accompanied by the reduction of molecular oxygen ( 0 2 ) to H20 2 • The Cr(V) species then reduces H20 2 to generate •OH radicals and Cr(VI) (16).To understarid the mechanism by which Cr(V}-generated ·OH radicals cause cytotoxicity, Aiyar et al. (8) investigated the reaction of Cr(VI) and H20 2 to generate ·OH radical and its reaction with 2'-deoxyguanine (dG) to form 8-hydroxy-2'-deoxyguanine (8-0HdG}:"

Mar 1, 1992

By William K. Tolley

The U.S. Bureau of Mines (USBM) is investigating hydrometallurgical processing techniques to recycle metals from semiconductors and other advanced materials. Cadmium and tellurium were recovered from mixed CdTe/CdS scrap produced in the manufacture of thin-film photovoltaic devices. Selective cadmium dissolution was achieved using oxygen-pressure leaching in dilute sulfuric acid. Leaching the scrap for 90 min at 110° C in 2.2NH2S04 under 400 psig 02 yielded 97% Cd extraction; however, cadmium content of the residue ranged between 4% and 7%. Soluble iron was added to the lixiviant to catalyze oxidation of the CdS component. Tellurium and sulfur remained in the leach residue primarily in the elemental form. The iron and tellurium were removed from the cadmium-rich leach liquor by adjusting the pH to 5.3. The cadmium was recovered as cadmium sulfate crystals by evaporating the solution. Alternative leaching and purification schemes are discussed.

Jan 1, 2010

By Wilbur I. Duvall, Thomas C. Atchison, Joseph M. Pugliese

Short cylindrical charges were detonated in drill holes in rock to determine the effect that decoupling ( defined as the ratio of the radius of the hole to the radius of the charge ) has on the strain - generating abilities of explosions in rock . The amplitude and period of the strain pulses produced in the rock were studied as a function of distance , size of charge , and decoupling . The main results of these studies were that , for a given distance and size of charge , the amplitude of the strain pulse decreases as decoupling increases and the period of the strain pulse decreases at first and then increases as decoupling increases . A simplified theory of decoupling is presented that satisfactorily explains the experimental results . The information presented makes it possible to predict the effect of decoupling on explosiongenerated strain pulses in rock and thus helps the explosives user evaluate the effect of decoupling on his blasting .

Jan 1, 1964

By J. M. Gomes

The Bureau of Mines investigated electrolytic techniques for preparing diborides of the group IV B metals. TiB2, ZrB2, and HfB2 were electro-deposited from their respective oxides dissolved in borate-chloride-cryolite electrolytes. Titanium diboride was also electrodeposited from rutile (Ti02) dissolved in a Na2,B4O7-Na2C03-Na3A1F6-NaC1 electrolyte at 1,050° C; 14 kW-hr were required to produce 1 pound of TiB2. Major impurities in the TiB2 produced in a 10-deposition cycle experiment, in weight-percent, were Al, 0.2; Cr, 0.3; Fe, 0.1; V, 0.3; C, 1.4; and 0, 1.0. Zirconium diboride was electro-deposited from zircon (ZrSiO4) dissolved in a Na2B407-NaOH-Na3A1F6-NaCl-NaF electrolyte at 1,050° C. The ZrB2 produced in a 10-deposition cycle experiment contained the following impurities in weight-percent; Fe, 0.1; Si, 0.5; C, 0.3; and 0, 0.6. Energy required to produce 1 pound of ZrB2 was 9.3 kW-hr.

Jan 1, 1975

By Michael R. Kennedy

This report describes the demonstration of longwall mining in a seam dipping 27 to 34'. Equipment was selected on the basis of capability, compatibility, and co t. Snowmass, Bureau of Mines, consultants and manufacturers were involved in the selection process. The equipment arrived in early 1981, prior to completion of development for the first panel; therefore, the equipment was operated on the surface for training. The surface training paid off with a fast, efficient installation and start-up of the face. The longwall equipment operated very well on the steep pitch with an average equipment downtime of 21.9[9]. Coal handling outby the face was a problem which caused an additional downtime of 19.5%. Development for the panels proved to be the major problem in the economics of longwall mining on a steeply dipping seam. During the first 9 months of operation the longwall averaged 71.9 TPMS and development averaged 0.6 TPMS for an overall average of 14.1 TPMS. Had mining continued, timing of development would have been another major problem. Monitoring of subsidence, pillar stability and shield loading was done in connection with mining, but little useful information was gained from the monitoring.

Jan 1, 1987

By J. D. Ramsdell

The purpose of this investigation was to determine the effects of the impurities, oxygen, nitrogen, carbon, and iron (in low percentages) on the mechanical properties of electrolytic titanium. The strength and hardness of binary Ti-O, Ti-N, and Ti-C alloys are linear functions of alloy content in the composition range investigated. Compared to oxygen and carbon, nitro-gen is the most effective strengthener and hardener, followed by oxygen, then carbon. When the carbon concentration is above 0.10 percent, carbides are present, and strength and hardness are relatively unchanged. For equivalent hardness levels, Ti-Fe alloys are stronger than binary titanium alloys containing oxygen, nitrogen, or carbon. However, the strengthening is related to the presence of transformed beta in the structure.

Jan 1, 1960

By W. W. Adams

"Although rock-dust is an effective and generally recognized preventive of wide-spread explosions in bituminous-coal mines and although in explosions many lives have been saved by its use that almost certainly would have been lost otherwise, yet more than two thirds of the yearly production of bituminous coal from underground mines in the United States is still being obtained from mines that do not use rock-dust, and more than two thirds of all men that work underground in bituminous mines are employed in nonrock-dusted mines. These facts are revealed by a statistical survey of all mines in the United States that were in operation during 1930, 1931, and 1932. The survey was conducted by the Demographical Division of the Health and Safety Branch of the United States Bureau of Mines and was based upon reports from operating companies received in connection with the Bureau's annual statistical surveys of accidents in the mining industry.In 1932, the latest year for which complete figures are available, rock-dust was used, to some extent at least, in 393 bituminous-coal mines whose total production of coal during the year was 83,632,327 tons, or 30.6 percent of the entire output of bituminous coal from all mines in the United States not including opencut mines. The number of men employed underground at mines that used rock-dust was 25.7 percent of the total number employed underground at all bituminous mines, and the number of man-hours worked at these mines was 27.1 percent of the total number of man-hours worked underground at all bituminous mines during the year."

Nov 1, 1934

By Helen W. Lang

This report describes a monitoring system applied by the Bureau of Mines to provide rapid, continuous determination of the main constituents of exhaust gas during the Bureau's approval schedule testing of diesel engines for under-ground use. Commercially available continuous analyzers with strip chart readout are employed for nitric oxide (mass spectrometric), carbon dioxide (nondispersive infrared), methane (NDIR), carbon monoxide (NDIR), and oxygen (polarographic). Good correlation is obtained between the continuous instrumental results and those obtained by batch chemical and gas chromatographic methods.

Jan 1, 1969

By G. Stecklein

This report summarizes the results of research into the areas of the fragmentation and entrainment of Airborne Respirable Dust (ARD). The objectives of this program were four-fold: first, to review the present state of knowledge regarding ARD; second, to expand this state of knowledge through the identification of hypothetical microscopic mechanisms by which the coal is fragmented and the dust becomes entrained; third, to specify the informational requirements to verify or nullify these hypotheses; and fourth, to relate experimental techniques that will produce that required information. Additionally, insights are provided regarding potential methods of extraction and/or treatment which may reduce the concentration of ARD.

Jan 1, 1982

By D. A. Reynolds

Yields of ammonium sulfate obtained in the carbonization of coal frequently vary from plant to plant, because ammonia is an unstable compound at high temperatures and therefore sensitive, to changes in carbonizing conditions. Differences in byproduct yields of ammonium sulfate obtained at different plants generally are accounted for by variations in plant procedure, either in preparing the coal or in its carbonization. However, technicians of one large corporation,- which frequently obtained higher yields of ammonium sulfate in its Alabama plants than ever were attained in its Ohio plants, "could not reconcile the differences in yields with their plant operations. These investigators suspected that the Alabama, coal used in their southern plant yielded more ammonia because its composition differed inherently from that of the Pennsylvania and West Virginia coals fused in their Ohio plants, although this concept could not be proved readily in their large-scale operations. Their view is supported by experimental data obtained A Beau of Mines-American Gas Association (BM-AGA) carbonization tests) -21 of a large number of coals including those carbonized commercially in Alabama and Ohio.

Jan 1, 1949