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By Kenneth M. Earl

This report describes the results of a field study conducted by the Bureau of Mines during 1956 and 1957 on manganese-and iron-bearing mineral deposits in the southern district of Aroostook County, Maine. The work was undertaken to determine the extent of deposits largely concealed under glacial drift and to obtain subsurface samples for manganese mineral identification and research in ore dressing and extractive metallurgy. The investigation was confined to the Westford Hill-Daggett Hill area in Hodgdon Township and to the Stewart prospects and vicinity in Linneus Township. Over 50 magnetic anomalies were mapped by magnetometric surveys in the Westford Hill-Daggett Hill area, Hodgdon Township. The largest anomaly, as outlined by the 1,000-gamma contour, indicates a deposit 3,200 feet long with a maximum width of 350 feet. The smallest anomaly measures about 10 feet wide by 25 feet long.

Jan 1, 1962

By John K. Alley

Fibrous silicon carbide was produced by thermal decomposition of certain silicates contained in graphite crucibles. Induction heating was used to produce the necessary temperature and thermal gradients. Both green and white fibers were mainly the beta modification even though each color grew within a different temperature zone. Alpha silicon carbide, present in insufficient amounts for X-ray detection, was identified by electron diffraction. The white fibers formed in a zone between 1,365° and 1,634° C (±50° C). The green fibers (less contaminated) formed in a much more narrow zone between 1,650° and 1,672° C (±50° C). The average lengths and widths of microscopic fibers grown by this method were 1.5 mm/0.002 mm (white) and 1.2 mm/0.0035 mm (green); however, same fibers observed by electron microscope had cross-sectional measurements of 150 to 300 A. Both differential thermal analysis and thermogravimetric analysis showed that silicon carbide fibers oxidized in air at temperatures above 500° C. Fibrous silicon carbide was indexed as a cubic cell with the dimensions a = 4.358 A. The density calculated from X-ray data was 3.217 g/cm3.

Jan 1, 1963

By Joseph M. Pugliese

The U.S. Bureau of Mines has produced a generic in situ copper mine design manual, which contains a computerized cost model for in situ copper oxide mining. The model specifies (1) site-specific parameters, which must be quantified for mine design, (2) a method for minesite design based on those parameters, and (3) a procedure for assessing economic viability for the mine design. The menu-driven computer program performs calculations for developing commercial mine design specifications, as well as capital and operating costs. The default values are based on 1986 dollars, and indices for updating costs are included. The program also provides discounted-cash-flow rate of return (DCFROR) and allows for sensitivity analyses for an in situ mining operation at any specific undisturbed copper oxide deposit. This report is to be used with the 1990 version of the computer program, which has been made user friendly. It describes the flies, tutorial, input phase, help function, and monitor display of all calculated values and of the DCFROR table. The monitor-displayed discounted initial value of investment and annual operating costs are defined. The dual rate-of-return situation and sensitivity analyses are also briefly discussed. Information is provided on obtaining the computer program on diskette.

Jan 1, 1991

By Murray Greyson

A number of tests were made with various methanation catalysts in fixed-bed, conventional fluidized-bed, and multiple-feed, fluidized-bed equipment to develop catalysts and processes for methanation of synthesis gas. The results show: 1. Methanation reactions may be carried out in 1-inch, bench-scale equipment at high synthesis-gas throughputs with good temperature control of the reactions if a multiple-feed type of fluidized-bed design is used. 2. Nickel is superior to iron as a catalyst for the methanation of synthesis gas, unless the process is considered in terms of a combined operation that produces both gaseous and liquid products. 3. Techniques of catalyst preparation determine, to a large extent, the process life of nickel catalysts, and these techniques must be thoroughly investigated before any conclusions can be reached. 4. Enough data are available to indicate that the sulfur concentrations in synthesis gas that is used for methanation are extremely critical, and maximum process limits should be carefully evaluated.

Jan 1, 1955

By G. L. Neumann

"INTRODUCTION AND SUMMARYThe Guymard mine in Orange County, N. Y., is reported to have been discovered in 1862 and mined until 1876, producing 10,000 tons of lead and zinc ore. 2/The property was examined by an engineer of the Bureau of Mines 3/ in 1948. Development work was done by the Bureau in April and May 1949 and March 1950. During these two periods four drill holes totaling 2,090 feet were completed. The mineralized sections of the core were sampled and assayed.ACKNOWLEDGMENTSThe diamond drilling was conducted under the general supervision of McHenry Mosier, chief, Mining Development Branch, Minerals Technology Division, Region VIII, and the direct supervision of Kenneth M. Earl and the writer as project engineers. Drill cores were logged by Paul K. Sims of the Federal Geological Survey. Chemical analyses were made by the Bruce Williams laboratories, Joplin, Mo., and the Minerals Processing Branch, Minerals Technology Division, Region VIII, Bureau of Mines, under the general supervision of Paul M. Ambrose, chief, and the direct supervision of Howard F. Carl, chief, Physical and Chemical Section.LOCATION AND ACCESSIBILITYThe Guymard deposit (see fig. 1) is on the west slope of Mount Hope, Orange County, N. Y., 1,500 feet northeast of Lake Guymard.Graham station, near the deposit, is on the Erie Railroad about 8 miles north of Port Jervis and 4 miles south of Otisville."

Aug 1, 1952

By James W. Ballard

The facts are generally accepted that an atmosphere containing large quantities of any dust is objectionable to breathe and that some dusts are more dangerous than others. Therefore, knowledge of the com-position of dusts is important in evaluating the hazard entailed on exposure. At present, free silica, of which quartz is the most abundant form, is considered one of the most significant dusts, from the standpoint of pneumoconiosis, and one State5/ has established permissible limits of air dustiness on the basis of the free-silica content of rock. The amount 06 free silica in materials used for rock dusting also has been limited.6/ Determination of free silica or quartz, therefore, is important.

Jan 1, 1940

By R. J. Leary

Significant improvements in surface conditions or mechanical properties of steels have been attributed by several investigators to ladle additions of small quantities of rare-earth metals or their oxides. To investigate systematically these effects in wrought and in cast plain carbon and alloy mechanical steels containing approximately 0.35 percent carbon, heats of four representative compositions were melted by the Bureau of Mines in a 4-ton open-hearth furnace. Each heat was cast into three sets of ingots to exemplify respectively, treatments with (1) rare-earth metals, (2) rare-earth metal oxides, and (3) an untreated set as a control. The development of melting, casting and rolling practices is described and discussed. Lance injection of oxygen shortly after melt raised the temperature of the metal immediately as much as 500° F., principally because mechanical agitation exposed the high-carbon metal to the flame and furnace root. An exceptional degree of superheat in the metal at the termination of the refining period was attributed to oxygen injection during the refining period. Bath temperatures higher than industrial practice were permitted by the all-basic furnace lining. Rates of carbon elimination as high as 0.036 percent carbon per minute were achieved by oxygen injections.

Jan 1, 1961

By Ruth F. Brinkley

Principle activities of the Bureau of Mines Explosives Research Laboratory from July 1, 1960 to June 30, 1961 are reviewed briefly in Part 1. Part 1 also includes data obtained in connection with several minor investigations which are not sufficient to warrant separate publications. Part 2 gives brief abstracts of publications that appeared during fiscal year 1961; in general, the research reported in these publications antedates this period.

Jan 1, 1963

By L. A. Haas

The U.S. Department of the Interior, Bureau of Mines, is conducting laboratory-scale research to determine the leaching conditions required with sulfuric acid for extracting base metal from a matte with a copper-to-nicke1 ratio of 6 to 1. The matte (61.2 pct Cu, 9.7 pct Ni, 3.3 pct Fe, 21 pct S, and about 5 oz of precious metals per ton) was prepared from Duluth Complex (Minnesota) ore by smelting a bulk sulfide flotation concentrate. The matte was pre leached at atmospheric pressure to selectively extract 20 pct of the nickel, and the undissolved solids were referred to as the matte residue. Autoclave leaching of the matte residue extracted over 95 pct of the nickel, copper, and iron. The remaining leach residue in the autoclave contained over 100 oz of precious metals per ton. The leaching conditions required were matte grind of greater than 98 pct minus 325 mesh, pulp concentration of 50 g/1, total pressure of 100 psig with oxygen at 150° C or 400 psig with air at 180° C, 50 g/1 H2S04, 700 rpm agitator speed, and 6 hours of leaching time. The leaching time was decreased to 2 hours by increasing the agitator speed to 1,300 rpm. Sulfuric acid concentration greater than 50 g/1 did not appreciably enhance the base metal extraction, but with less acid, residues with higher iron concentrations were obtained. Supersaturation of the liquor was prevented at 150° C by using a 1ixiviant that contained 30 g/l Ni and 20 g/1 Cu.

Jan 1, 1979

By James S. Browning

The Bureau of Mines conducted laboratory batch and small-scale continuous flotation tests of weathered mica pegmatite ores from Alabama and North Carolina to determine the technical feasibility of recovering commercial-grade mica concentrates. A new anionic-catonic method was developed for recovering mica in the presence of clay slimes. In continuous tests, concentrates containing 98.1 percent mica were obtained from the Alabama pegmatite ore; the North Carolina pegmatite ore concentrates contained 97.2 percent mica. The recoveries were 83.8 and 81.6 percent, respectively.

Jan 1, 1965

By S. R. Zimmerley

Recent investigations of finely ground materials have verified Rittinger's law of crushing.4, This law states that the surface produced is proportional to the work expended in the crushing operation. Thus, for a unit of work applied to crushing quartz a definite amount of surface will be produced. Obviously, this amount of work applied to some other mineral will not produce equivalent surface. It follows that in an investigation of mill practice, where ore is being crashed, the relative crushing resistance of the component minerals must be known. In a previous investigation of the Rittinger law,5 the crashing resistance that is, the work required to produce a unit of surface - was accurately determined for quartz. The surface values were obtained by means of the rite of dissolution of quartz in hydrofluoric acid.6 If it were possible so to measure surface on other minerals the determination of relative crushing, resistance would be a simple matter; however, the results obtained on minerals other than quartz by a dissolution method were not encouraging. Moreover, if accurate values could be obtained by dissolution this method could probably never be used on a mixture of minerals such as occurs in an ore.

Jan 1, 1929

By Graham W. Marks, Clyde A. Bridger

"INTRODUCTION An electrolytic process for the preparation of metallic cobalt has been developed recently in the Bureau of Mines Experimental Station at Boulder City, Nev. Chemical analysis shows this cobalt to contain impurities in small percentages, chief of which is nickel. It is desirable to be able to determine these impurities spectrographically. This report is concerned with a procedure for the spectrochemical determination of nickel in cobalt.Previous spectrographic work on cobalt was done by Breckpot and Mevis,/ who used the method of homologous pairs of lines. However, it was felt that a more detailed investigation was needed, employing the method of internal standards.ACKNOWLEDGMENTWe are indebted to B. G. Knickerbockor and his staff at the Boulder City, Nev., station of the Federal Bureau of Mines for their cooperation, and particularly to Richard W. Lewis and Robert G. Sanderson, who prepared nickel-free electrolytic cobalt for us."

Feb 1, 1948

By Dennis R. Dolinar

Physical property tests were conducted on drill core from three exploratory holes on the Naval Oil Shale Reserve near Anvil Points, Colo. Data and regression analysis curves are presented. Data obtained above the Mahogany zone were used to estimate the potential zone of surface effects from under-ground mining. Single specimen testing was primarily used to obtain Mohr's envelope and subsequent rock properties. The technique is shown to provide satisfactory results for this rock type with a significant reduction of core preparation and testing time.

Jan 1, 1981

By Henry J. Kellner, Michael J. Brnich

This U.S. Bureau of Mines report addresses issues involved in using a limited number of training apparatus to give hands-on self-contained self-rescuer (SCSR) training to a succession of miners, and provides guidance regarding methods for minimizing the spread of infectious diseases. Procedures used for preventing the spread of infectious organisms in dentistry, cardiopulmonary resuscitation (CPR) training, and scuba training are examined. The sanitizing methods of three organizations that require individuals to insert the mouthpiece as part of the SCSR donning sequence are discussed. It was found that each of these organizations was able to render their mouthpiece assemblies microbe free simply and inexpensively.

Jan 1, 1989

By R. L. Marek

The number of persons fatally injured in the California petroleum industry in 1932 was 24, a decrease of 6, or 20 percent from the number killed in 1931. The decrease in the number of fatalities occurring in 1932 caused the fatality curve of the California petroleum industry to reach its lowest point in 10 years. Changing conditions in the oil industry - reduced personnel, decreased active field development, and curtailed production - have undoubtedly caused a part of this decrease, but continued accident-prevention efforts by the industry have also contributed to the reduction in the number of fatalities for 1932. The Bureau of Mines has analyzed and reported annually the fatalities in the California petroleum industry for a period of 10 years. Figure 1 shows the trend of fatal accidents during that period. Fatality statistics for 1932 show that the drilling and producing, pipe line and transportation, and refining and natural gasoline divisions of the industry had fewer accidents in 1932 than in 1931, sales and marketing being the only division that showed an increase over 1931. The number of fatalities by divisions for 1931 and 1932, percent of total, and percentages of increase and decrease are given in Table 1.

Jan 1, 1933

By Chas. F. Jackson

During the past year a special study was made of shrinkage stoping A large number of mines in the United States and Canada which employ this method were visited and their practices were discussed with the operating staffs. The operating data obtained are appended hereto. Data were also abstracted from the literature on other mines and are combined in tables with data personally secured by the author. References are made to these published articles, some of which have appeared as information circulars of the United States Bureau of Mines, in the Transactions of the American Institute of Mining and Metallurgical Engineers, and the Engineering and Mining Journal. Several of the mines referred to which have not been described in individual papers will be described in detail in information circulars to be issued by the bureau. Eventually it is planned to combine and condense the information in these circulars and present the data in bulletin form.

Jan 1, 1930

By G. R. Strimbeck

Experimental work is report on the gasification of 90-percent through 200-mesh, strongly coking Sewickley-bed coal with oxygen and with steam in three temperature ranges, namely, 2,700° to 3,400° F., 1,600° to 2,000° F., and 230° to 250° F. Thirty-one runs have been made, during which 56,000 pounds of coal have been charged to the generator at feed rates of 200 to 450 pounds of coal per hour. The average results, not the optimum results, are given in the following tabulation:

Jan 1, 1950

By Richard L. Sayrs

The Eve Mills deposit is in Monroe County, Tenn., near the southeastern corner of the State. The deposit was examined in February 1943 by a Bureau of Mines engineer, and drilling the property was recommended to increase the on: reserves enough to justify mining should war needs require it. The deposits were explored, by 32 diamond-drill holes totaling 11,649 feet during the periods from July 1943 to November 7, 1945, and from April 1944 to August 17, 1944. The drilling campaign disclosed a large area of mineralization. The ore, however, is apparently confined to long, narrow sheets. The indicated grade of the ore bodies blocked cut by the Bureau of Mines is 4.o8 percent zinc and 2.10 percent iron.

Jan 1, 1949

By Ruth F. Brinkley

Principle activities of the Bureau of Mines Explosives Research Laboratory from July 1, 1960 to June 30, 1961 are reviewed briefly in Part 1. Part 1 also includes data obtained in connect ion with several minor investigations which are not sufficient to warrant separate publications. Part 2 gives brief abstracts of publications that appeared during fiscal year 1961; in general, the research reported in these publications antedates this period.

Jan 1, 1963

A revolutionary development in blasting materials has occurred in recent years. Ammonium nitrate, sensitized by the addition of a small percentage of No. (class) 2 diesel fuel or other suitable petroleum product, has been adopted as a low-cost, efficient blasting agent2 in a wide variety of mining, quarrying, and heavy construction operations. Moreover, the ready availability of the component supplies throughout the Nation, together with the ease of formulating them into effective blasting agents, has made it possible for the blaster himself to prepare the mixes at the site of use. Recently, most established explosives manufacturers have begun supplying premixed AN-FO (ammonium nitrate-fuel oil) or a comparable product to various mining operations. However, many individuals and small business establishments are marketing premixed products prepared in facilities that are often poorly constructed and poorly located. Although these blasting agents have partly or wholly displaced explosives such as dynamites in many applications, there are some blasting operations in which the fuel-sensitized ammonium nitrate agents do not appear to be well adapted. As long as the hazards they present are clearly understood and respected, ammonium nitrate-based blasting agents have important safety characteristics when prepared under competent factory control or field-mixed under equivalent close control. This publication attempts to summarize the knowledge of those hazards and to incorporate practical ways to cope with them.

Jan 1, 1963