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By L. A. Johnson

The Bureau of Mines analyzed three cores from the south Seep Ridge area of the P. R. Spring tar sand deposit of northeastern Utah. Four tar sand zones are indicated in the area. The zones range in average thickness from 13 to 24 ft. The total net thickness of the tar sand in the three coreholes ranges from 71 to 112 ft. The tar sand occurs between the depths of 27 and 254 ft. It has good porosity, 25.6 pct of bulk volume; high permeability before and after oil extraction, 819 and 2,218 md, respectively; but a relatively low oil saturation, 36.5 pct of pore volume. Gravity of the oil ranges from 8.20 to 16.5° API.

Jan 1, 1975

By E. G. Valdez

The Federal Bureau of Mines, in cooperation with Ford Motor Co., investigated the recovery of polyurethane foam and other assorted plastics from the nonmagnetic reject of automobile shredders. Preliminary studies were con-ducted on a 1957 hulk augmented with additional foam and assorted plastics. The proposed flowsheet developed by the Bureau from the preliminary studies consists of a combination of screening, water classification, and gravity separation. The process was then tested on reject from two shredded 1972 cars. All of the foam and between 52 and 70 pct of the assorted plastics were recovered. The composition of the reclaimed foam concentrates ranged from 46 to 66 pct foam; the concentrates were hydrolyzed in laboratory tests by Ford Motor Co. to produce a reusable liquid mixture of polyether glycol monomers and toluene diamine.

Jan 1, 1975

By Michael J. Sapko, Eugene M. Bazala, Eric S. Weiss, Kenneth L. Cashdollar

The data presented in this report are the results, to date, of an ongoing Pittsburgh Research Center Disaster5Prevention research program on the explosion hazards associated with blasting operations in noncoal mines. Laboratory and experimental mine tests have shown that oil shale and sulfide ore dusts can be ignited given the proper predispersed dust concentrations, particle size, and kerogen or sulfur content. Methane (CH) gas may also4be present in deep oil shale formations and can pose a significant added hazard to underground blasting operations. The most common explosive used for blasting in oil shale had been ANFO, a combination of ammonium nitrate and fuel oil; blasting in sulfide ore had used ANFO and/or dynamites. Tests conducted at the cannon gallery at Lake Lynn Laboratory near Fair chance, Fayette County, PA, provided a means of evaluating the relative incendivity characteristics of new and existing explosive products. Three explosives—a pumpable emulsion-ANFO blend, a packaged water gel, and an emulsion blasting agent—exhibited low-incendive qualities compared with other more highly incendive products such as ANFO and some dynamites. Based on the data collected during numerous full-scale blasts in oil shale and sulfide ore mines, the low-incendive products significantly reduced or eliminated the ignition hazards while at the same time providing effective fragmentation of the rock. Based on the positive results from the gallery and field testing, low-incendive explosives, coupled with good blasting procedures, show promise in reducing dust and/or gas ignitions associated with blasting operations in oil shale and sulfide ore mining applications.

By G. E. Rennick, F. E. Armstrong, J. Pasini, J. R. Abrams

An oil well penetrating the Pittsburgh bituminous coalbed in northern West Virginia was plugged and safely mined through 3 months later. A sensitive chemical tracer, introduced into the oil reservoir before the test, was not detected in the mine air following the plugging and during mining of the pillar and penetration of the well. Effectiveness of the plugging in preventing reservoir gas from entering the mine through the well hole was verified by continuous monitoring of the mine air for indications of sulfur hexafluoride, an inert gas detectable in amounts as minute as 112 part per billion. Expand- able cement and fly ash-gel-water slurry were utilized to seal the well above and below the coal seam. Three other wells were also plugged using various techniques.

Jul 1, 1972

By E. Morrice

Techniques developed by the Bureau of Mines for the preparation of high-purity rare-earth metals and their alloys by electrolysis of the oxides in fluoride media are summarized. Cerium, lanthanum, neodymium, praseodymium, dysprosium, gadolinium, and yttrium metals, the mixture didymium, and specific alloys of these metals and samarium with iron, nickel, chromium, and cobalt were prepared. Individual metals were electrodeposited in the liquid state on tungsten or molybdenum cathodes. Alloys were prepared by electrodepositing the rare-earth metal on a consumable cathode, at a temperature above the melting point of the eutectic formed between the rare-earth element and the cathode material. Cells were designed for electrowinning metal products in gram and pound quantities, and methods for continuous electrowinning of cerium and lanthanum were developed.

Jan 1, 1968

By Nicholas Kyriazi, John P. Shubilla

The National Institute for Occupational Safety and Health, National Personal Protective Technology Laboratory, has undertaken a study to determine how well self-contained self-rescuers (SCSRs), deployed in accordance with Federal regulations (30 CFR 75.1714), hold up in the underground environment with regard to both physical damage and aging. This report presents findings regarding laboratory-tested SCSRs in the seventh phase of testing from May 1999 to August 2000. The SCSRs were tested on human subjects and on a breathing and metabolic simulator. The results indicate that most of the apparatus, if they pass their approved inspection criteria, perform satisfactorily. The deployed CSE SR-100s, however, exhibited significantly higher inhaled carbon dioxide (CO2) levels than new units, as they did in the previous two phases. Several Draeger OXY K-Pluses that rattled when shaken were found to have potassium superoxide (KO2) particles throughout the breathing circuit, including the mouthpiece. Draeger investigated the problem and developed a shake test to detect damaged units. The durations of new Ocenco M-20s were statistically significantly longer than those of deployed units, although only by 2 min.

Jan 3, 2002

By H. B. Carroll

The Bureau of Mines investigated the adaptability of the Meteorology Research Inc.2 (MRI) nephelometer and the Sinclair-Phoenix smoke meter for use in routine, analytical, smog-chamber experiments and to compare their responses to aerosol during these experiments. Both instruments' sampling systems were modified--smaller size sample input systems were studied using the nephelometer and a secondary sample system was added to the smoke meter to allow measurement of Aitken or condensate nuclei. Both instruments were easily adapted for use with small smog chambers and both displayed good precision and sensitivity to aerosol. A correlation was shown to exist between the two instruments' responses to aerosol. This correlation makes it possible to report the Sinclair-Phoenix measurements in visibility and/or mass units if desired.

Jan 1, 1973

By Edward F. Divers

This Bureau of Mines report describes the results of a laboratory evaluation of a mechanical dust collector (scrubber) suitable for underground coal mine applications. The scrubber was developed by the Mining Research and Development Establishment (MRDE), Burton-On-Trent, England, and tested at the Federal Bureau of Mines Pittsburgh Mining and Safety Research Center (PMSRC) as part of a technical exchange program. The 2,000-to 8,000-cfm scrubber consists of an electrically driven vane-axial fan, water sprays, a 2-inch-thick, loosely knit stainless steel wire filter panel, and a water droplet eliminator. The dust-laden airstream travels axially through the water sprays, filter panel, fan, and eliminator. Slurry water drains into a sump where a belt-driven pump recycles it back to the sprays. Fractional breakdown tests showed a maximum dust collection efficiency of 96 pct of respirable-size (less than 7 µm) coal dust at 2,000 cfm. Efficiency decreased with increasing airflow; for example, to 91 pct at 6,000 cfm. Following these tests the original wire panel was replaced with a similar but smaller panel developed at PMSRC; a marked improvement in dust collection occurred at all flow rates tested.

Jan 1, 1979

By C. P. Lazzara, Y. Miron, A. C. Smith

This report presents a U.S. Bureau of Mines study to identify the causes of self-heating events beneath the floor of a deep underground coal mine. Mine samples from both heated and unheated areas were examined by various techniques, including visual, microscopic, thermal, chemical, and instrumental tests. The combined results led to the conclusion that pyrite (FeS2) oxidation was the prime cause of the beatings. However, adiabatic oven tests of selected samples did not indicate the effect of the pyrite on the self-heating process, probably because of the experimental conditions. A fast, simple procedure to assess the concentration of pyrite in the mine samples was developed, utilizing the reactivity of the sample with an aqueous solution of hydrogen peroxide (H2O2)

Jan 1, 1992

Detemine the elastic properties and structural integrity of a rock mass in situ. Approach An acoustic device that transmits and receives high-frequency seismic waves between boreholes was designed, built, and field tested. How It Works The acoustic cross-borehole apparatus operates by sending a seismic wave from a transmitter in one borehole to a receiver in a second bore? hole which may be located as far as fifty feet away, depending on the wave transmission quality of the rock. By measuring the wave's travel time and the distance between boreholes, the acoustic velocity of the rock mass can be determined. Characteristics of the seismic wave arriving at the receiver (such as the wave velocity, amplitude, and frequency content) are related to the physical properties of the geologic media, as calcu-

Jan 1, 1982

By Curtis H. Elder

In studies conducted by the Bureau of Mines, two test areas were hydraulically stimulated and exposed by mining: One in the Pittsburgh coalbed at the Vesta No. 5 mine, Washington County, Pa.; and one in the Illinois No. 6 coalbed at the Inland mine, Jefferson County, Ill. Induced fractures were contained totally within the coalbed with no adverse effect on the stability of associated rock strata. Induced fractures were vertical and were propagated normal to the direction of least residual tectonic stress. Gas production was increased fivefold to twentyfold by hydraulic stimulation.

Jan 1, 1977

By Charles L. Kimbell

In broadest overview, a substantial part of the world's mineral industry in 1990 registered small gains over its 1989 performance, but traditional statistical measures of mineral industry performance, namely global production, trade, and consumption levels, failed to mirror these gains. This was because of the sharp downturns in the mineral industry activity in the U.S.S.R. and the former centrally planned economy nations of eastern Europe. These downturns in this one geographic area had influences on almost all traditional statistical series, in some cases simply significantly reducing growth, in other cases providing for a global downturn, in almost all cases despite considerably brighter outlooks based on activities in other world areas. To be sure, the U.S.S.R. and eastern Europe were not the only places on the planet suffering problems of one type or another in 1990 that impacted on minerals industry activity, but with the acquisition of information presently available, it seemed almost assured that the difficulties of these economies in transition will be the most difficult of problems to resolve in the long run. It certainly appeared that the legacy of the half century or more of economic central planning will be a decade or more of very difficult adjustments, and a number of these will greatly affect not only the minerals industry of these transition countries, but also the rest of the globe's mineral industry as well.

Jan 1, 1993

By Douglas Pollock, John Organiscak

Water spray characteristics, including droplet size and velocity, airborne dust capture potential, and induced airflow quantity for various spray nozzle designs were evaluated to provide basic information for improving spray applications. Water droplet size and velocity characteristics were initially measured by a Phase Doppler Particle Analyzer (PDPA) for hollow cone, full cone, flat fan, and air atomized spray nozzles at similar operating parameters. Airflow inducement and dust capture experiments were also conducted under the same operating parameters to examine any salient features of the spray nozzle type, droplet characteristics, induced airflow, and airborne dust capture. Test results indicate that there are trade offs between airflow inducement and dust capture efficiency. A spray nozzle with a wider discharge angle was observed to induce more airflow, but at reduced dust capture efficiencies. Increasing spray nozzle fluid pressure(s) generally reduced water droplet sizes with concurrent increases in droplet velocity, airflow inducement, and airborne dust capture. Placing a three-sided barrier around the spray nozzles normally reduced spray air induction and increased dust capture efficiency. A direct relationship between airborne dust capture efficiency and spray input power normalized per unit of airflow induced was ob- served. This information can be utilized to improve the performance of water sprays for reducing airborne dust levels.

By Jon C. Volkwein

The canopy-air curtain was originally developed by the Bureau of Mines to surround the operator of a continuous mining machine with a zone of clean air. This report describes the application and testing of a canopy-air curtain on a gathering-arm loader, as well as some of the problems associated with providing a zone of clean air to a standing, semimobile operator. The area of air-curtain coverage and effects of air velocity are discussed. In its present form, the canopy-air curtain provides a 50 percent reduction in respirable dust to the operator.

Jan 1, 1981

To quickly and reliably assess the stability (safety) of saturated and unsaturated tailings pond embankments. Approach Determine embankment geometry and soil properties, then use that data to obtain the safety factor of the embankment directly from one of a series of factor-of-safety charts.

Jan 1, 1982

By A. Gene Collins

During recent years the interest in trace and minor constituents of oil-field water, petroleum, and their associated reservoir rocks has increased. The metals copper, nickel, lead, manganese, iron, zinc, and cadmium are not determined routinely in oilfield brine analyses. Determination of these metals and subsequent correlation of these data should yield information to aid 1n the interpretation of the origin of different waters. The methods of analyzing oilfield waters have several potential applications: (1) Aiding in the search for petroleum; (2) identifying sources of intrusive brines; (3) controlling corrosion; (4) controlling produced water; increasing knowledge of the geology of subsurface formations; (5) identifying incompatible waters in waterflooding operations; (6) increasing the knowledge of the flow of oil, gas, and water in underground formations; and (7) aiding in the identification and location of valuable mineral reserves. Some brines contain enough valuable minerals to be recovered commercially.

Jan 1, 1962

By F. P. Haver

The Bureau of Mines developed a process to extract about 90 percent of the sulfur from molybdenite flotation concentrate by compacting the concentrate with one-quarter of its weight of aluminum powder, heating it at 800° C for 30 minutes, and then allowing the product to react with water. This thermite reduction yields an impure molybdenum alloy plus aluminum sulfide. The latter readily hydrolyzes, to yield pure hydrogen sulfide which can be converted to elemental sulfur by the Claus process. At least 95 percent of the molybdenum can be subsequently recovered as 99.95-percent-pure molybdic oxide.

Jan 1, 1968

By Michael D. Fenton

Social and political movements that had been gathering momentum over several years continued in 1993 to dramatically affect and inspire uncertainty on the global mineral industry. Privatization of government-controlled mineral industries continued throughout the world, especially in Africa, Asia, Central Eurasia, Eastern Europe, Latin America, and Western Europe. The reasons for privatization varied among regions and countries, but the trend was universal and was not expected to end soon. Regional trade blocks were being developed and expanded. The European Union (EU), the North American Free Trade Area (NAFTA), the Association of Southeast Asian Nations (ASEAN) , the Asia Pacific Economic Cooperation (APEC) , and the Latin American Southern Cone Common Market (MERCOSUR) were expected to contribute to reduced internal tariffs and increased minerals trade. Minerals consumption within the politically unstable former Soviet Union (FSU) decreased significantly without a simultaneous cutback in production, while its exports flooded the world's mineral markets. These exports into Western Europe and Japan, still in economic recession, depressed minerals and metals prices worldwide, especially for aluminum, magnesium, nickel, and potash. Increasingly restrictive environmental laws and land-access limitations in Australia, Canada, Western Europe, and the United States tended to discourage mineral resource development. However, the number of undeveloped countries in Latin America and Asia that encouraged exploration and development by revising mining and tax laws and regulations increased, thereby increasing investment opportunities for foreigners.

Jan 1, 1995

By August J. Kwitowski

This Bureau of Mines report describes how the reinforcement mechanisms of untensioned, full-column resin bolts were determined during one underground study. Both axial and transverse shear loadings were identified for two instrumented resin bolts that replaced standard resin bolts in an opera-ting room-and-pillar mining section. The strain responses of resin bolt steel cores to local axial and transverse shear loadings are described. This information was obtained from laboratory testing of resin bolts installations; it was also used to analyze the data from the underground test.

Jan 1, 1980

By Joan T. May

Anhydrous methods were tested for the extraction of beryllium from low-grade source materials. The purpose of the investigations was to find new extraction processes that are applicable to domestic ores. Beryl, helvite, and phenacite materials containing from 0.1 to 2.8 percent BeO were used as starting materials for direct halogenation tests and pretreatment followed by halogenation. The results of the investigations showed that direct fluorination and carbide-chlorination are two practicable methods that can be applied to low-grade concentrates. Treatment of concentrate-carbon mixtures with anhydrous hydrogen fluoride extracted 99 percent of the beryllium in the concentrate; the soluble fluoride product, converted to an oxide, contained 70 percent BeO. Chlorination of beryllium-silicon carbide, prepared from low-grade concentrates, extracted beryllium into the volatile chloride product.

Jan 1, 1962