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Humic acids adsorb on coal and depress coal floatability in the acidic pH range. In alkaline solutions, their effect is not pronounced. In the neutral pH range, a second small addition of kerosene plus MIBC leads to a significant increase in coal yield and better selectivity. Humic acids present on oxidized coal surface were found to be responsible for the inhibited floatability of the? coal. As expected, the flotation of such oxidized coal also strongly depends on the method of pH adjustment.

Jan 1, 1988

By Carl Scholz

Discussion of the paper of Carl Scholz, published in Bi-monthly Bulletin, No. 22, July, 1908, pp. 551 to 559. HOWARD N. EAVENSON, Gary, W. Va. (communication to the Secretary*) :-For some time before the publication of Mr. Scholz's paper, I had been collecting data bearing upon its subject, and I now take pleasure in presenting my results to the Institute in the form of a discussion. It has long been a matter of common opinion among mining-men that mice-explosions are, more frequent during the colder, or winter months, than during the warmer ones, and it is a matter of common knowledge among them that the air-ways and road-ways in most mines are much drier and are more in¬clined to be dusty during the winter than during the summer. In many mines, places which are wet and sloppy in the summer are dry and sometimes dusty during the winter. These changes, of course, can only be due to atmospheric conditions, and are caused by differences in temperature and humidity. Until recently, however, very little attention has been paid to the part that atmospheric conditions may play in mine-explosions, or, rather, to the effect they may have in rendering mine-conditions peculiarly dangerous, and in spreading and rendering more disastrous the effects of what would otherwise probably have been .small explosions. To show the difference in mine-conditions during sunnier .and winter months, I have tabulated in Table I. the results of 24 observations of hygrometric conditions in several different mines at different times of the year. Mines Nos. 1, 2, and 6 are located in the Pocahontas.coal -region, in McDowell couuty, W.Va., the first one being a shaft-mine shaft mine and the others drift. Mines 1A and 2A are drift-mines located in Logan county, W. Va. All of these are mines of fair size, but none of them has been in operation more than six years,

Jun 1, 1909

By Carl Scholz

DURING November And December, 1907, Four Serious Mine-explosions Occurred In The Appalachian Coal-Field, Which Resulted In The Loss Of Nearly A Thousand Lives And Caused An Enormous . Damage To Property. These Accidents Attracted More Than The Usual Attention; Coal-Trade And Engineering Papers Contained Many Comments And Suggestions On The Cause And Prevention Of Accidents; The Daily Press In Many Instances Condemned The Coal-Operators And Charged These Accidents To Their Negligence, Or Their Anxiety To Make Money Without Adopting Precautionary Measures. Immediately After Each Accident The Respective State ..Authorities Ordered Close Investigations To Be Made, With The View Of Establishing The Cause And Suggesting Remedies To Prevent Recurrence. Representatives Of The Technologic Branch Of The U. S. Geological Survey, To Whom The Investigation Of Mine-Accidents Had Recently Been Delegated By The Secretary Of The Interior,. Visited The Mines And Co-Operated With The Local Authorities In Their Determinations. It May Be Safe To Say Here That An Investigation Of A Mine After An Explosion Has Occurred Discloses But Little, Because. The Causes Have Been Removed And Conditions Have Been Entirely Changed. On Jan. 8, 1905, The Coal-Operators Of West Virginia Organized An Association At Washington For The Purpose Of Making Extensive Investigations, And Sufficient Funds Were Pledged To Carry Out This Work. At This Organization Meeting, The Representatives Of The Geological Survey Present Had No Suggestions To Offer As To The Cause Of These Accidents. An Examination Of The Various Reports Concerning These Accidents Indicates That The Explosions Were Caused By The Ignition Of Gas Or Dust; They Show The Point Of Origin And The Direction In Which The Force Was Expended, And Give A Detailed Description Of The Damage Done. Very Little Has Been Said As To What

Jan 7, 1908

By S. Veeramasuneni, C. D. Dunbar

The rate of hydration influences many important physical properties of gypsum. Previous research examined the rate of gypsum hydration and related this to compressive strength and microstructure development using BET specific surface area analysis. The analysis of gypsum porosity in combination with BET surface area and rate of hydration remains to be done. In the present study, mesoporosity is analyzed using the numerical method of Barrett, Joyner and Halenda (BJH) to gain a greater understanding of gypsum hydration and microstructure development. The rate of hydration has a significant effect on mesoporosity of the gypsum matrix. The results reveal the effect of mesoporosity and hydration rate on some macro physical properties of gypsum.

Jan 1, 2000

By H. X. Yan, J. X. Zhang, F. S. Niu

"The analysis on influencing factors of hydraulic conditions in fine hematite flocculation, such as stirring speed, stirring time and axial distance of particle size and fractal dimension of floc was investigated. Furthermore, response surface methodology(RSM) has been applied according to the Box-Benhnken center-united experimental design principle to optimize parameters of hydraulic conditions as a response index to indicate the fractal dimension of floc. The results show that when the agitation speed is 900r/min, the axial distance is 2.0cm, and the stirring time is 3.0min, the particle size reaches the maximum value of 35.44µm and the fractal dimension is 1.6594. The interaction between the axial distance and the stirring speed is highly significant, but the interaction with the stirring time is not obvious. The experimental data and model predications match well, which indicates that the established model has high accuracy and practicability. INTRODUCTION With the exhaustion of iron ore resources that are easy to be mined and the vigorous demand for iron and steel, the exploitation and utilization of fine-grained embedded iron ore resources have drawn attention from the industry and the government [1~2]. Flocculation flotation is one of the effective methods for separation and recovery of fine granular minerals. In 1975, the method was first applied and succeeded in Tilden Concentrator, USA. Flocculation and desliming became the key technology of the Tilden to raise its annual treatment capacity from 4 million tons to 8 million tons at that time [3 ~ 4]. In 2008, the selective flocculation and desliming-reverse flotation technology was successfully used to treat 2.8 million tons of Qidong iron ore. Under the conditions of 28.36% raw iron grade and 98% grinding fineness -0.038 mm, the ideal index of 62.5% iron concentrate grade and 68% recovery was obtained [5]. Dr Kitchenner of the Royal College of Mining and the Ore Processing Research Group of Wallenstein Laboratory first proposed the use of flocculation to separate minerals. After that, many scholars conducted a great deal of theoretical and practical researches, but mostly they focused on chemical theories, mathematical models and selectivity differences in the flocculation process, while the research on the influence of the pulp flow state on the separation effect in the flocculation process started later [6~9]. The results show that the motion of the agitated flow field has a significant influence on the formation of flocs. The fluid morphology will change with the change of hydraulic conditions. The change of fluid morphology will not only affect the movement behavior of particles, but also change the action of chemical agents on the surface of mineral particles[10~12]."

Jan 1, 2018

By A. Osouli, B. Moradi Bajestani

"Increase in permeability of rock mass is vital for both petroleum and geothermal applications. Hydraulic fracturing is a common method to create and increase the permeability for production. Due to the complexity of fracture propagation in a naturally fractured medium, understanding the interaction between hydraulic fracture (HF) and natural fracture (NF) is of great importance to optimize the fracturing process. The possibility of interaction between HF and NF is partly a function of orientation. Various scenarios are predictable for hydraulic fracture regarding the intersection with NF such as being arrested by NF, crossing NF or crossing the fissure while injecting water into it. Different parameters such as geomechanical and geometrical properties of surrounding rock mass, the operational parameters such as injection rate and the angle between created hydraulic fracture and natural fracture (approach angle) can affect the result of hydraulic fracture and natural fracture intersection. In this paper, using a series of flow-coupled Distinct Fracture Network (DFN) simulations, hydraulic fractures were analyzed to investigate the influence of the aforementioned parameters on the hydraulic fracture propagating. Results show that the most significant parameters affecting the interaction of natural and hydraulic fracture are orientation of the intersection as well as injection rate. The interaction and fracture propagation in NF and HF intersections are also studied and discussed in detail.INTRODUCTIONThe hydraulic fracture technology has substantially changed the oil, gas and geothermal industries. With the help of this technology, extraction of fossil resources from tight shale reservoirs will be economical, feasible and sustainable. Due to presence of massive oil and gas trapped in these reservoirs, this technology has been the center of attention for the past 40 years (King, 2012). Hydraulic fracturing is the process in which high pressure water is pumped into shale unconventional reservoirs with low to ultralow permeabilities. With this process paths are created in these mediums for delivering oil and gas to horizontal wellbore and increase the surrounding rock medium permeability. Economical and sustainable stimulation of these tight reservoirs is highly dependable on our understanding in regard to fracture propagation in the highly complex rock medium. Hydraulic fracturing process in rock mediums with preexisting natural fractures is more complex because of the high possibility of Hydraulic Fracture (HF) being arrested or deviated by Natural Fracture (NF). Also, HF and NF intersection can influence the required pumping pressure, injection rate, the outcome of horizontal wellbore and the affected geological underground zones. Since the 1950s, numerous studies have been conducted to predict and plan fracture propagation with the help of modeling and simulation methods. Having a thorough and accurate prediction of fracturing process will not only prevent stimulation of unwanted geological zones or pollution of aquifers, but also will improve the efficiency of the fracturing process. Previously, several studies have been conducted in order to investigate and analyze the interaction of hydraulic fracture and natural fracture (Cottrell, Hosseinpour, & Dershowitz, 2013; Doe, Lacazette, Dershowitz, & Knitter, 2013; Shakib, 2013; Zhang & Jeffrey, 2006)."

Jan 1, 2015

By X. S. Yuan

With a demand for increasing energy efficiency and a need for improving bitumen recovery, a highly integrated solution for sustainable lease development of Aurora North of Syncrude has been proposed and implementation plans are underway. Flocculation and thickening technology as an important component of the integrated solution provides Syncrude an opportunity of rapid heat recovery from tailings and more flexible tailings closure and reclamation options. Flocculation of fine-particle suspensions by polymers is a non-equilibrium process whose performance is strongly influenced by physical and chemical variables. While polymeric flocculants are frequently used to establish the chemical conditions favorable for flocculation, the actual performance of a flocculation process generally depends more on the physical variables, such as the hydrodynamic conditions in mixing the flocculants and slurry. In order to study the effect of hydrodynamic conditions on flocculation of Syncrude fine tailings, a standardized laboratory test procedure called power flocculation has been developed in comparison with the conventional manual mixing methods. It is shown that the agitation speed and time in conditioning the flocculant solution and the slurry have a profound effect on the flocculation performances measured by initial settling rates, supernatant clarity and sediment density. It was found that the optimum bench test conditions for power flocculation of Aurora fine tailings with a sand-to-fine ratio (SFR) of about 1:1 are conditioning of the flocculant solution and the tailings slurry at 250 rev/min to 300 rev/min in 20 s to 40 s. The test results are inter-preted with a flocculant adsorption/redistribution kinetic model that helps understanding of the effect of hydrodynamic conditions on flocculant adsorption, floc formation and floc growth.

Jan 1, 2014

By T C. Souza Pinto, M Safari, F S. Hoseinian, D Deglon, L Leal Filhoc

In this study, the effect of hydrodynamic parameters on the iron ore reverse was investigated in a mechanical flotation cell. The work carries out using the case study of Iron ore from Vale in Brazil. The influence of hydrodynamic factors such as froth height, impeller speed, superficial gas velocity and solids percentage were evaluated on the quartz flotation. The results showed that the hydrodynamic conditions have a great effect on the flotation performance, especially on the fine and coarse quartz. The size-by-size analysis of the froth products showed that froth height, impeller speed, superficial gas velocity and solids percentage have a significant effect on true flotation quartz particles. The increase in the froth height decreased the recovery of quartz particles. The increase in the impeller speed increases the recovery of quartz particles to an optimum. The increase in the superficial gas velocity improved the flotation of coarse quartz particles. The increase in the solids percentage increases the recovery of quartz particles.

Sep 18, 2023

By S Mitra, D O’Dea, N Barrett, S, T Honey, M M. Hoque

The steel industry is currently exploring hydrogen-enriched blast furnace operations as a means to reduce the greenhouse gas emissions. However, there is a need to investigate the gas permeability behaviour of mixed burdens comprising of lump and sinter as the current knowledge regarding their behaviour is limited, particularly with regards to hydrogen enrichment. In the present study, a series of interrupted softening and melting (S&M) under load tests were carried out in a hydrogen rich gas environment (~15 per cent) in the temperature range from 1000 to 1300°C by placing different types of ferrous ore layer including Newman Blend Lump (NBLL), sinter and sinter-NBLL mixed burden in between two coke layers. X-ray computed tomography (CT) was then used to scan the interrupted test samples. Scanned images were first analysed using an image processing workflow implemented in ImageJ and the material simulator GeoDict (v2022) to segment different phases such as coke, ferrous and void based on their grey scale values. A quantitative analysis was then performed on the segmented images to estimate the phase volume fraction as well as bed permeability. Bed void fraction thus obtained agreed well with the bed contraction data obtained from the S&M test. It was further noted that both ferrous layer void fraction and bed permeability decreased linearly with increasing temperature for all ore samples. The mixed burden voidage changed in a similar fashion to the sinter, demonstrating a high temperature interaction between the two materials

Sep 18, 2023

By Corale Brierley

The effect of hydrogen peroxide (H202) on growth and respiration of Thiobacillus thiooxidans and Thiobacillus ferrooxidans, organisms involved in acid leaching of copper sulfide minerals and uarnium oxides, was examined. Oxygen uptake and growth by T. thiooxidans were totally inhibited after contact with 0.82 mM H202. Complete inhibition of oxygen uptake by T. ferrooxidans occurred at 8.75 mM H202, and growth was inhibited after 6 hr exposure to 2.06 mM H202. Higher concentration of H202 can be used without detriment to thiobacilli if it is dissipated prior to reaching the oxidation pond or dump surface.

Jan 1, 1980

By Behzad Vaziri Hassas, Firat Karakas, Mehmet Celik, Onur Guven

Since dewatering is a costly process, removal of moisture from relatively fine size lignites is an important industrial problem. As the lignite gets finer, the presence of micropores and relatively low hydrophobic nature of lignite lead to trapping of large quantities of water in the coal matrix. Lignites used in power stations need to be dried to a certain degree of humidity before it is transferred to the combustion chamber. It is generally wise to dewater coal as much as possible by physical means before it is dried. However, dewatering cost in some cases may be prohibitive. Thus, sometimes removal of even little percent moisture may be of great help in such operations. Surfactants have been used to increase the efficiency of coal dewatering. It is crucial to select appropriate type and amount of surfactants in order to get higher efficiency. Since the hydrophobic characteristic of coals increases with increasing the coal rank, dewatering of bituminous and anthracite can be accomplished using low HLB surfactants (Oily), however, these surfactants are not efficient in the case of low rank coals like lignites and brown coals. It is suggested that adsorption of low HLB surfactants on high rank coals is governed by Acid-Base interactions rather than electrostatic and van der Waals forces. Since this characteristic in lignites is not strong enough, low HLB surfactants could not be effectively adsorbed on low rank coals to make surface more hydrophobic. In this paper, a special set-up has been designed to study the effect of high HLB surfactants on dewatering of fine lignite particles. It is shown that high HLB surfactants function more efficiently on low rank coals than low HLB ones.

Jan 1, 2014

Effect of Hydrophobicity and Frother Concentration on Bubble-Particle Interactions in Turbulent Flow

Sep 13, 2010

By Paul Worsey, Yasutaka Dote

The choreography of large fireworks displays dictates electric initiation for precise timing. It has been common practice to pre-squib products before transportation for reducing set up time. A number of fatal accidents transferring pre-squibbed product during transportation suggests that there is a problem with impact sensitivity. The aim of this paper is to quantify the impact sensitivity of the various configurations of initiating materials used in display fireworks.

Jan 1, 2009

By A. Morrison, D. Mesa, P. R. Brito-Parada

"Froth flotation is the most widely used mineral separation technique. It is based on the relative hydrophobicity of valuable and gangue particles. In a flotation tank, two distinct zones can be identified: the pulp and the froth. The pulp is a turbulent region in which hydrophobic valuable particles attach to air bubbles while hydrophilic gangue particles remain in the slurry. As the particle-laden bubbles rise, a mineralised froth zone is formed that overflows as a concentrate. Although the process is more than a hundred years old, there remain many aspects that are not completely understood, particularly for the froth zone. Thus, the rules governing the design of flotation tanks tend to focus on pulp zone parameters, which are largely based on operating data. An example of this is the design and operation of impellers. These tend to be designed paying attention to hydrodynamic phenomena in the pulp zone, but their effect on the froth zone has not been completely addressed. The role of impellers in a flotation tank is to break the air bubbles in order to generate smaller ones and to provide an environment that enables the collision between those bubbles and the particles in the slurry. This usually creates turbulent regimes that can affect the pulp-froth interface, destabilising the lower regions of the froth and affecting the overall performance of the process. Different impeller designs and retrofit modifications have been proposed in the past, addressing some of those issues. However, there is no systematic study of the effect of different impeller designs on the bubble size in the pulp and its links to the stability of the froth. This work tested the impact of an impeller designs combined with the use of a stator on the performance of an 87 litres continuously operated laboratory-scale flotation tank, with a focus on bubble size in the pulp and froth stability. The results showed that the implementation of a stator system decreased bubble size and increased froth stability. That resulted in an increase of mass pull, measured as a proxy of metallurgical recovery."

Jan 1, 2018

By Karl Sundberg

ELECTRICAL investigations carried out in regions containing sedimen-tary rocks showed that sediments generally are good electrical conductors, a fact which at the present time is used for structural investigations by electrical methods. It is of fundamental importance, not only for these investigations but also for electrical prospecting in general, to know the electrical properties of various soils and rocks. It will be useful, there-fore, to discuss this question with the hope that the general points of view discussed in this paper will perhaps be, completed by further observations and determinations of material from various localities. This paper is based principally on the study of literature, and the purpose is primarily a discussion of the main factors that determine the electrical conductivity of soils and rocks. It will follow, however, that the factors discussed here also frequently decide how far a certain orebody can be regarded as a good electrical conductor compared with the sur-rounding rocks. All-rocks are more or less porous; and the pores are filled with liquids and gases. Their electrical conductivity, therefore, depends on the following factors: 1. The electrical conductivity of minerals composing the rock. 2. Electrical conductivity of the liquid filling the pores. 3. Proportion of the volume of liquid filling pores of the rocks to the solid rock material. 4. Shape of the pores. 5. Arrangement of the particles of gas and liquids. 6. Temperature. Dry minerals, with the exception of certain ore minerals, are complete nonconductors from the point of view of applied geophysics; in the present investigation we deal with rocks which have no conducting minerals, and factor 1, therefore, is not important. The same is true of soils. The liquids contained in soils and rocks in most cases are waters, some-times oil. As oil is a nonconductor of electricity, the impregnating waters will determine the electrical conductivity of soils and rocks.

Jan 1, 1932

By Marisa Di Sabatino, Michael Phan Knudson, Mari Juel, Eivind Øvrelid

"A p-type Czochralski silicon ingot doped with boron was characterized for resistivity, minority carrier lifetime, interstitial oxygen, and metallic impurities. Analyses show a peak in resistivity and a dip in lifetime both occur 5 cm from the top of the ingot crown. This peak in resistivity deviates from the expected trend based on Scheil's equation for boron distribution. High concentration of interstitial oxygen in this area suggests that other oxygen-related defects, such as thermal donors and precipitates, may also be present here, and the observed peak in resistivity and dip in lifetime could be attributed to such defects. The low lifetime of 15-30 µs at minority carrier density of 7.5 x 1014 cm-3 is likely due to copper contamination.IntroductionSolar energy resources vastly exceed all other alternative energy resources, ensuring that solar power must play a crucial role in the evolving energy market. The economic viability of solar power in competition with other energy resources depends upon finding efficient, cost-effective, reliable, and controlled methods for solar cell production. In this regard, minimizing waste (such as material with unsuitable electrical properties that hinder solar cell performance) is a vital component of making solar cell manufacturing cost-effective. Impurities affect electrical properties of solar cell silicon in different ways (i.e. [1, 2, 3, 4, 5, 6]). In this work we focus on the role of oxygen and metallic impurities. Understanding oxygen impurities in silicon is critical to solar cell development because oxygen has been attributed with influencing critical electrical properties including resistivity and minority carrier lifetime and thereby potentially hindering solar cell performance or rendering material unsuitable for solar cells.[1, 2] Furthermore, oxygen is a common impurity in the standard type of solar cell silicon, Czochralski (CZ) silicon, due to diffusion of oxygen from the silica crucible into the melt during crystallization. [7] This study investigates the effects oxygen impurities have on the electrical properties of p-type CZ silicon."

Jan 1, 2013

By John B. Goddard

Crystallization of ammonium paratungstate (APT) is frequently the last effective purification step in producing high-purity tungsten. However, crystallizer mother liquors are often several times higher in tungsten than predicted by the solubility of APT. The formation of heteropoly anions, particularly those containing phosphorus and silicon, is largely responsible. Solubility of tungsten in APT mother liquor can be linearly correlated with the concentration of these and other impurities. The problem can be overcome by direct treatment of the crystallizer feed solution with alum. By appropriate treatment, the aluminum hydroxide flocculates and is easily filtered, resulting in a purified low-aluminum crystallizer feed from which high APT yields can be attained.

Jan 1, 1984

By J. B. Goddard

Crystallization of ammonium paratungstate (APT) is frequently the last effective purification step in producing high-purity tungsten. However, crystallizer mother liquors are often several times higher in tungsten than predicted by the solubility of APT. The formation of heteropoly anions, particularly those containing phosphorus and silicon, is largely responsible. Solubility of tungsten in APT mother liquor can be linearly correlated with the concentration of these and other impurities. The problem can be overcome by direct treatment of the crystallizer feed solution with aluminum sulfate. By appropriate treatment, the aluminum hydroxide flocculates and is easily filtered, resulting in a purified low-aluminum crystallizer feed from which high APT yields can be attained.

Jan 1, 1985

By Carl F. Floe, John Chipman

A YEAR ago the authors published a paper on the solubility of sulphur dioxide in molten copper.1 The data in that paper agreed closely with that obtained by previous investigators, which, however, did not agree with the theoretical predictions for solubility of triatomic gases of this type. It has generally been assumed that the reaction of solution is: [ ] Neglecting the slight change in copper concentration and considering that the concentrations of sulphur and oxygen are both proportional to the volume of gas absorbed, it follows that this volume should be proportional to the cube root of the pressure. It was found that a plot of the volume absorbed versus the cube root of the pressure gave a straight line, but that this line did not pass through the origin. Calculations of the equilibrium constant for the reaction showed that it was fairly constant for pressures above l00 mm. but that actually it approached zero at lower pressures. The conclusion was made therefore that the solubility as determined could not be expressed by Eq. I or by any other simple equation, particularly at low pressures. Other investigators have concluded that the solubility of sulphur dioxide in copper as well as in several copper alloys is more nearly proportional to the square root of the pressure.* Such a conclusion, however, does not satisfactorily account for the results, even when rather complicated mechanisms for the solution are assumed. The highly improbable speculations of Lepp2 and of Schneider and Esch3 based upon hypothetical dissociation pressures of Cu20 and (a; 2S dissolved in copper illustrate the type of reasoning that has been used to account for the discrepancy. In the discussion of the previous paper, the authors pointed out that the discrepancy might possibly be due to impurities in the copper, although the purest form available was used. Further consideration of the problem suggested that the impurities likely to have the greatest effect on the solubility of SO2 in copper were oxygen, sulphur and carbon. Accordingly, further experiments have been made to show the effects of these elements. EXPERIMENTAL METHODS The apparatus used for measuring solubility was essentially the same as that shown in the previous paper. However, since it was desired to make measurements at low pressures, a McLeod gauge was added and 6-mm. glass tubing was substituted for the capillary. This increased the "hot volume" considerably but was necessary in order to obtain good vacuums in a reasonable length of time. A mercury diffusion pump was also installed.

Jan 1, 1942

By Yasuo Iizuka

We have had studied CO oxidation on unsupported Au powder (mean particle size, ca.100nm) manufactured by evaporating ultra high purity gold metal (>99.99%) in inert gas and reported that it showed some activity after oxidizing pretreatment in O2 at 423 K?453 K. However, recent XPS analysis of the Au powder revealed that it contains much amount of impurity metals such as Ag and In at levels which far exceed those expected from the impurity level of raw gold metal in the bulk. Several samples of Au powder containing different amount of impurity metals were prepared to examine whether the activity depends upon the existence of surface impurity or not. Activity measurements were performed at 273 K after undergoing the powder under various pretreatment conditions. Although the activity of Au powder varied to some extent according to the pretreatment condition, it is strongly correlated to the surface concentration of Ag. Such dependence was not found for In, indicating that the activity of unsupported Au powder is mainly due to the existence of Ag in the surface layer. The activity attributable to ?particle size effect? was not recognized for Au powder with a mean particle size larger than 80 nm.

Oct 1, 2003