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By Jon C. Volkwein

Dust concentrations inside and outside enclosed cabs on several types of mining machinery were measured by the Bureau of Mines. Results indicated that properly enclosed cabs can offer significant dust protection for machine operators. Recommendations for improvements in cab technologies were discussed.

Jan 1, 1979

By D. J. Bauer

Solvent extraction techniques were used to determine the extraction sequence of yttrium and the rare-earth elements in an amine solvent extraction system. Single-stage extraction with Primene 81-R resulted in separation factors of 3.8 between yttrium and dysprosium and 25 between yttrium and cerium. Yttrium was concentrated in the aqueous phase. EDTA and DTPA, as aqueous phase counterextractants, enhance separation factors in mine-rare-earth sulfate systems. Yttrium separation from heavy rare-earth elements exhibits marked sensitivity to the position of yttrium in the selectivity scale of the rare-earth elements with the sequestrants. Yttrium-ytterbium separation is more effective with EDTA, whereas yttrium-dysprosium separation is more effectively increased with DTPA.

Jan 1, 1963

By R. L. Anderson

Mechanical cleaning of bituminous coal in the United States was begun about 1875, with plants in western Pennsylvania and Illinois. The United States Geological Survey began to record the quantity of washed bituminous coal in 1906; and the series was carried forward to 1923, except that no data were collected, for 1922. This statistical work was transferred to the Bureau of Mines in 1925, and the collection of data on mechanical cleaning was resumed in 1927. Data collected before 1927 include only the coal that was washed at the mines and do not include that cleaned by pneumatic methods at the mines and that cleaned at central washeries operated by consumers.2/ The total bituminous coal washed in 1906 was less than 10 million net tons. In 1927, the first year for which complete figures are available for all types of mechanical cleaning, 28 million net tons of bituminous coal were cleaned in the United States.

Jan 1, 1951

By E. J. Kloos

The Bureau of Mines devised a new machine-test method for measuring carbon dioxide inspired by a wearer of self-contained breathing apparatus. The new method compares favorably in speed and precision with standard man-tests in which the apparatus is tested while actually worn, and is scheduled for use in future approval tests for facepiece carbon dioxide 'measurements. However, man-tests will still be used to measure the efficiency of the carbon dioxide sorbent materials in closed-circuit breathing apparatus.

Jan 1, 1966

By William R. Sharp

This Bureau of Mines report details a technique for aiding the engineer with the long-range design of an underground mine. The method is based upon the assumption that sufficient data are available to assign numeric values to some finite number of mineralized blocks; assignment of numerical values is problem dependent. By assigning appropriate weighting schemes, the algorithm developed in this report may be used to solve the optimal end-of-life underground mine layout, design least-cost electrical layout networks and efficient material handling networks, find least risk escape routes in the event of an accident, etc. The method is based upon the assumption that sufficient cost and geologic data is available to build a detailed mineral block inventory of the mineral deposit. It is further assumed that the cost assigned to any minable unit is independent of the neighboring blocks. The basic approach relies upon concepts and ideas from the theory of networks. To make the approach user oriented, a computer program is included and discussed. The computer code is written for an orthogonal, three-dimensional set of blocks. Computational costs and experience indicate that the program could be of great benefit in evaluating large complex mineral properties from the viewpoint of predesigning an underground mine layout.

Jan 1, 1974

By J. C. Nigro

Hematite-to-magnetite reduction kinetics were investigated mainly in CO-CO2 atmospheres at temperatures ranging from 500° to 1,000° C. Reduction rates were measured with a thermobalance, which recorded the weight loss as the specimen was reduced. Reduction data on both synthetic and natural hematite spheres showed good linearity of ro [1-(1-R)1/3] with time, t, up to over 85 pct conversion to magnetite; the rate coefficient (k[L], cm/min) obtained from the linear portion of the plot was used to characterize the penetration rate of the hematite-magnetite interface. Gas composition, porosity, and silica content were major factors affecting the rate. Temperature dependency of the reaction rate was small, yielding a mean activation energy of about 3 kcal/mole. Silica additions increased the reaction rate, probably through an increase in the effective surface area and diffusion; however, above 900° C, silica can react to form fayalite. Experimental data showed that the linear thickening rate of the magnetite layer, normally evidence of a chemically controlled reaction, can also be indicative of a reaction controlled by both mass transfer and diffusion. Evidence from this study indicates that the dominant rate-controlling factor in the reduction of hematite to magnetite at high temperatures is transport in the gas phase.

Jan 1, 1973

By W. A. Cole

The sulfur shortage that existed during the Korean conflict stimulated interest in coal measures as possible sources of sulfur. One of the areas brought to the attention of the Bureau of Mines was in Marion County, Iowa, where comparatively high-sulfur coals and other marcasite-bearing strata were known to occur. A Bureau of Mines engineer inspected the marcasite occurrence on December 4, 1954; this prompted further work on the Iowa coals and associated formations as a source of iron sulfides. An investigation of the Iowa high-sulfur coals was undertaken including core drilling, field reconnaissance, and compilation of data pertinent to consideration of the following: 1. Upgrading Iowa coal by mechanical cleaning and the feasibility of recovering sulfur from coal brasses. 2. Possibility of processing the high-sulfur coals by adaptation of methods employed in processing industrial gases to produce sulfur and sulfur products. 3. Possibility of finding concentrations of iron sulfides in associated rock formations in sufficient quantity for economical recovery.

Jan 1, 1957

By D. B. Dow

This report on methods employed for dehydrating oil-field emulsions, is the second of a series prepared as a result of a study of oil-field emulsions recently completed by the writer. The first paper2 dealt with the factors responsible for the formation of emulsions. A third paper will discuss the physical chemistry involved in the formation and resolution of such emulsions. In the early development of the oil fields of Pennsylvania, no emulsion troubles of any consequence were encountered, nor to any serious extent in the oil fields of other Eastern States: However, with the development of fields west of the Mississippi in Oklahoma, Kansas, Texas and California, where heavier oils of different characteristics were found, the problem of dealing with cut oil soon became of great importance.

Jan 1, 1925

By Robert H. Lambeth

The Madison RARE II study area has four prospects with identified resources. These are listed in table 1 and are described in the following text. A high potential for Sillimanite exists at the Placer Creek occurrence (fig. 1, no. 7) and potential for phosphate rack in all areas underlain by the Phosphoria Formation. Some prospects exhibit minor potential for copper, lead, zinc, silver, and gold in the southern portion and very minor potential in the northern portion. Deposits in the northern end also have low potential for rare earth, asbestiform anthophyllite, or kyanite group minerals (including sillimanite).

Jan 1, 1982

By Alla D. Mah

Thermodynamic calculations for antimony and its compounds have been hampered by the lack of adequate basic thermal data; much work rains even to fill the more important gaps. This paper supplies heat and free energy of formation values at 298.15° K, for the sesquioxide and tetroxide, based upon new measurements conducted by the Bureau of Mines. The heats of formation were obtained by combustion (bomb) calorimetry, and the free energies of formation were obtained by combination of heat and entropy data. The new values are believed to substantially improve the accuracy of thermodynsunic considerations involving these oxides.

Jan 1, 1962

By George H. Johnson

An evaluation of the diamond-bit-performance data accumulated from core-drilling cherty limestone and cherty dolomite reveals that the percentage of core recovered and the physical characteristics of the bits and diamonds used are economically significant. One of the established trends, of particular interest to those engaged in diamond drilling, is that bits set with small, low-quality, West African drill bort are the most economical. Detailed analysis of the factors that affect diamond-bit performances, such as diamond size and quality, bit size and type, percentage of core recovered, and the physical characteristics of the bit matrices are assessed in the tables, charts, and discussion.

Jan 1, 1958

By J. B. Gayle

The Bureau of Mines sole-heated oven has been used for studying coal expansion for some 20 years. During the period before 1940 emphasis was placed on studies of the mechanism of coal expansion and the effects of variations in operating conditions on the results. Since 1940 emphasis has shifted to a survey of the expansion properties of various coking coals. Because additional information concerning a number of unsolved problems in connection with the earlier studies appeared highly desirable, this investigation of the use of sole-heated ovens for studying coal expansion was undertaken. The principal findings, in order of their discussion in the text, may be summarized as follows. 1. Expansion results for binary blends of coking coals exhibit nonadditive behavior, both positive and negative deviations from additive behavior being noted, depending on the particular coals tested. Additive behavior can be achieved, however, either by charging the blend components in separate layers (which indicates that the observed phenomena are not characteristic of the particular expansion oven used) or by testing relatively coarse sizes of coal (which suggests that the effects of crushing on the expansion properties of coking coals may be even more complex than is generally recognized).

Jan 1, 1959

Large quantities of combustible materials are often found in underground metal and nonmetal mines, with support timber predominating. Wood lagging and timber, wires and cables, brattice cloth, hose, paper products, cardboard cartons, and wooden containers are additional combustible materials commonly found in underground storage areas. Shorted or overloaded electrical cables, worn sockets and plugs, spontaneous combustion, careless smoking, and welding and cutting are common fire ignition sources. Inexpensive, reliable fire detection and suppression systems are available to provide early warning and to extinguish fires that originate in underground storage areas.

Jan 1, 2011

By Oliver C. Ralston, Foster Fraas

"INTRODUCTION The predominant characteristic of powdered mica is the thin -plate shape of the particulars, and the thinner the plates, the more enhanced is this characteristic. Consequently, it is frequently desirable to grade mica according to the thickness of the plates. Concerning the various possible methods for grading mica, very little has been published. There is also no information on the relative quantities of mica per given range of plate thickness. This paper presents a graphical method that shows how these quantities are distributed and how the different methods of grading compare.CUMULATIVE BULK DENSITYBulk density, which is an indirect measure of the plate thickness, was determined in a small cylindrical cup of 3.37 cubic centimeters volume. The mica was placed in the cup under a standard procedure. The densities thus measured checked these determined in a 273 cubic centi¬meter cup with less than a 2 percent error.In calculating cumulative densities it is important to know how they are averaged. In any grading operation the bulk density of a series of fractions is determined. Starting with the lowest density fraction, the cumulative percent under-density can be calculated through the various fractions. It is possible that quantity may be measured by volume or weight and that the averaging may be done by a number of methods. However, experimentally it has been shown that the quantity must be by volume and that the averaging must be arithmetic. This is illustrated in table 1, in which the calculated and actual bulk densities are listed."

Sep 1, 1942

By F. D. Wang

The Bureau of Mines has developed a computer program for evaluating pit slope stability by the finite element stress analysis and limiting equilibrium method. The program includes the finite element method of stress analysis using triangular elements, finite-element model mesh generation, plotting of the model mesh and stress contours, calculation of a factor of safety along a circular or a plane failure surface, and location of a critical circular failure surface. Instructions for preparation of input data, an example problem, and the program listing are presented.

Jan 1, 1972

By David P. Lindroth

The heat content above 25.0° C up to 1,000° C was measured for six rock types: St. Cloud Gray Granodiorite, Holston Limestone, Sioux Quartzite, Rockville Quartz Monzonite, Salem Limestone, and the basalt at Dresser, Wis. The calorimetric data were obtained with an isothermal jacket-copper block calorimeter. The experimental heat content data for each rock type are presented, along with specific heat data obtained from the temperature derivative of the heat content. For the six rock types the maximum deviations of the specific heats at a given temperature were within 10 percent below 575° C and within 34 percent above 5750°C. The increase in the values of specific heat range from a minimum of 13 percent for the basalt at Dresser, Wis. (temperature range, 100° to 1,000° C) to a maximum of 46 percent for Holston Limestone (temperature range, 100° to 870° C).

Jan 1, 1971

By Henry M. Harris

The Bureau of Mines investigated a glass containing approximately 17 percent lithia and 83 percent silica to establish a method of devitrifying cast and rolled shapes. Glass shapes with high strength were made by melting, forming, and rapid cooling of the composition, and the shapes subsequently were converted to a crystalline condition by heat treatment. The best devitrification schedule included rapid cooling of the glass to below 300° C, followed by reheating at a rate of 50° to 400° C per hour, depending on the size of the shape, followed by a of 60 to 70 hours at 500° C and another period of 15 hours at 800° C. attempts to use faster heating rates or slow cooling to accomplish devitrification in deformation of the shapes. The crystalline shapes had flexural strengths that averaged over 33,000 psi, achieved with an annealing time of 60 to 70 hours at 500° C.

Jan 1, 1965

By Mridul Gautam, Alex Bugarski

Size Distribution and Deposition in Human Respiratory Tract: Particle Mass and Number Aleksandar Bugarski and Mridul Gautam National Research Center for Alternative Transportation Fuels, Engines and Emissions Department of Mechanical and Aerospace Engineering West Virginia University TOXICITY OF ULTRAFINES (MAUDERLY et al.) ? FINER PARTICLES PENETRATE MORE READILY INTO CELLS AND TIXROUGH TISSUE BARRIERS ? FINER PARTICLES HAVE GREATER SURFACE AREA PER UNIT MASS, AND A LARGE NUMBER OF TOXIC REACTIONS OCCUR AT THE SURFACE ? FINER PARTICLES DISSOLVE MORE READILY THAN LARGER PARTICLES THUS ENHANCING THE BIO- AVAILABILITY OF SOLUBILIZED COMPOUNDS EPIDEMIOLOGICAL STUDIES INDICATE THAT THE IMPORTANCE OF ULTRAFINES REMAINS SPECULATIVE

By Richard J. Mainiero, Marcia L. Harris, James H. Rowland

In the past several years, there have been a number of blasting-related carbon monoxide migration incidents. In each case, there have been some common factors that appear to be related to carbon monoxide migration. Geology, heavy confinement of the blast, close proximity to the affected structure, and open pathways into the affected structure are just a few. Prince William County, VA is an area undergoing a boom in suburban development. In the year 2001, more than 4,050 new homes were constructed within the county.1 In the new housing development located in Bristow,VA, trench blasting was utilized to excavate proposed sewage and utility lines. On November 8, 2002, a trench blast was conducted for the installation of utility lines. Later that evening a carbon monoxide detector alarmed in a nearby house. The gas company and fire department sampled for carbon monoxide and measured 100 ppm and more than 200 ppm on the first floor and in the basement respectively. Subsequent efforts to prevent migration of CO into the nearby homes met with mixed results. The only reliable technique for protecting neighbors from CO appears to be the placement of CO monitors in the homes. The events are presented and discussed.

By John C. Franklin

The Bureau of Mines conducted extensive laboratory and limited field tests to determine whether a polymeric material could effectively reduce the emanation rate of radon gas from uranium ore. In the laboratory 46 different single-coat materials and 14 two-coat applications were tested. The laboratory tests showed that up to 100 percent of the radon gas could be sealed into the rock. Materials tested in the laboratory were polyesters, furan resins, epoxies, latices, and totally inorganic coatings. From the laboratory work six different materials were selected for field testing. The first test was single-coat materials in five static chambers; the second test used two-coat applications in an open chamber. Both tests were conducted in the Dakota mine at Grants, N. Mex. During the second test, the amanation rate of radon gas was reduced up to 62 percent.

Jan 1, 1975