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By Jochen Petersen, Caroline Muzawazi

The technical feasibility of ammonia leaching of PGM bearing Platreef flotation concentrates was investigated as an alternative method for the recovery of base metals prior to precious metal recovery. The composition of the concentrates includes 2.02% Cu and 3.17% Ni, and the major base metal minerals are chalcopyrite and pentlandite. Optimal leaching conditions were initially established in shake flask experiments to be a solution containing 4 M NH4OH, 4 M (NH4)2CO3 and a pH range between 9 and 10. These were used as base case conditions in column and batch stirred tank reactor tests, where the effects of total ammonia concentration and operating temperature were explored further. At optimal conditions nearly 100% Cu and Ni extraction were obtained in the batch stirred tank reactor, and 95% Cu and 60% Ni extraction was obtained in columns. The activation energy for chalcopyrite and pentlandite was 36 kJ/mol and 16 kJ/mol, respectively, in both reactors, indicating different reaction pathways for the two minerals. Gas-liquid mass transfer appears to be the limiting reaction step in columns much more than in tanks, and the degree of ammonia loss to air is significant. This initial test work indicates the feasibility of using ammonia leaching for this and similar materials as an alternative route to conventional smelting and refining prior to PGM recovery, but a number of technical challenges still need to be overcome.

Jan 1, 2014

By Jan Drzymala, Przemyslaw B. Kowalczuk

Froth flotation is widely used for upgrading of ores and other materials. Efficiency of flotation depends on many parameters, including type, chemical structure and dose of flotation reagents. Selection of a proper frother in flotation depends on the material used, necessary dose of frother and its selectivity. The selectivity of flotation can be characterized by proper separation factors and indices. In this paper separation selectivity and power of frothers were evaluated basing on separation data for a given material and frother, plotted as the recovery of the useful component in the concentrate versus the recovery of the remaining components in the tailing. Such a plot is called the Fuerstenau upgrading curve. The selectivity was defined as the location of the whole upgrading curve in relation to no and ideal separation lines, expressed on the scale from 50 (no separation) to 100% (ideal separation). In turn, the flotation power was defined as the dose of frother to reach a certain upgrading level at which recoveries of the useful and unwanted components are equal. The power and selectivity of frothers were determined for the Kupferschiefer stratiform copper ore floated in the presence of a fixed amount of xanthate and varying doses of frothers using a laboratory flotation machine. Basing on the separation results for different poly(propylene glycol) (CnH2n+1O(C3H6O)mH, CnPm) and poly(ethylene glycol) (CnH2n+1O(C2H4O)mH, CnEm) alkyl ethers, it was found that the concentrate yield and recovery of copper as the useful component in the concentrate were greatly influenced by the type and dose of frother. However, the same results plotted in the form of the Fuerstenau upgrading curve clearly indicated that the selectivity of frothers was similar, while their power was different. It proves that both selectivity and power of frothers are useful parameters for characterizing flotation systems.

Jan 1, 2016

By G. O. Crowell

This paper gives the history of the celestite deposit, now being mined by Kaiser Celestite Mining Ltd., near Sydney, Nova Scotia. Mining and milling procedures are covered, and the regional and local geology of the area are described, including the origin of the celestite.

Jan 1, 1971

By C. M. Acuna, M. Sherrington

In high temperature processes thermodynamic equilibrium is assumed and therefore chemical potential of elements, among the condensed phases, have to be the same. In such situation impurities distribute accordingly and their fractional distributions are affected by the masses of the coexisting phases. It has been claimed Teniente Converters perform quite well for smelting high impurity concentrates, especially in respect to volatilization and/or slagging. Production of high matte grade near white metal composition, requiring moderate oxygen enrichment in the process air, results in a huge mass of gas and therefore a high fraction of impurities report to it. Similarly, by recycling different sources of slag, flue dust or other materials, the mass of the final slag is increased and so do the masses of impurities reporting to the slag. Nevertheless, above a certain level the recycling of smelter byproducts is no longer feasible and the cycle has to be halted, unless higher impurity mattes are accepted. Although the process might be continued during converting and refining, lengthy and expensive measures have to be taken if suitable anode copper for electrolytic refining is to be achieved. In the present study samples of high arsenic matte grade and slag were obtained on a pilot scale. The matte samples, on the order 75%Cu, were equilibrated with slag at varying ratios in magnesia crucibles under CO/C02 atmospheres at 1523 K. After 24 hours equilibrium matte and slag were rapidly solidified and analyzed by copper, sulfur, iron and arsenic. Furthermore, industrial samples of matte and slag, in the order 75%Cu at 1523 K, were obtained via a special quenching sampling device to determine the association of copper and suspension of matte and copper in slag. Based on the results, the distribution coefficient of arsenic between slag and matte was evaluated along with copper species in slag and the fractional distribution of arsenic, in the coexisting phases, was determined as a function of the ratio mass of slag to mass of matte.

Jan 1, 2007

By H. A. Pearse

Introduction This paper may be regarded as another instalment of the story of the Britannia milling operation. From time to time in the past, articles (1) have been prepared by various members of the staff, giving details of crushing, grinding, and flotation treatment for the normal Britannia ore. It is not, therefore, the purpose of the present paper further to discuss what may be termed the standard milling operation, but rather to describe a flotation practice which has been evolved directly as a result of the general depression. The normal Britannia ore mixture contains chalcopyrite and pyrite as the main sulphide minerals, together with minor gold and silver values. The standard milling practice, evolved during several years of experimentation, provided for bulk flotation of the two sulphides after primary grinding to only approximately 35-mesh, followed by regrinding of the bulk concentrate, with subsequent separation of the chalcopyrite and pyrite to make a marketable concentrate of each mineral. However, in the face of a constantly increasing surplus of copper on the world markets and a steadily falling price during 1930 and 1931, it was obviously undesirable to continue producing large quantities of this metal at a loss. On the other hand, Company officials were very reluctant to add to unemployment by closing down entirely, provided operations could be continued without excessive losses. Fortunately, the existence was known of a fair sized body of ore, quite low in copper and relatively high in zinc content, with also a very considerably higher gold value than that prevailing in other sections of the mine.

Jan 1, 1934

By J. F. Henderson

THE National Advisory Committee on Research in the Geological Sciences was established seven years ago - in 1949. In 1952, shortly after the Committee had really begun to function and had issued its first report, a paper ( l) was presented describing the objectives and organization of the Committee and the progress to that time. Another four years have gone by and the Committee feels a further progress report may be of interest. HISTORY Ten years ago, in 1946, the Geology Division of the Institute set up a Committee on Geological Research. This Committee, under the Chairmanship of Dr. J. E. Hawley, recommended that "a National Advisory Committ.ee on Research in the Geological Sciences be formed" (2). With the backing of the President and Council of the C.I.M. this recommendation went forward to the then Minister .of Mines and Resources and, with his approval, to the Committee on Scientific and Industrial Research of the Privy ?Council. As a result, the National Advisory Committee was set up in 1949.

Jan 1, 1956

By J. D. Galloway

The mining industry of British Columbia continues to grow steadily in importance. The gross value of the production in 1925, sixty-two and a half million dollars, was a record, and ali indications point to the 1926 output registering a still higher figure. In an industry such as mining, where production means the depletion of known ore reserves, the discovery and development of new 'ore-deposits is of the utmost importance. To maintain and increase production, steady development is essential. In this respect, the record of the last three years in British Columbia mining is most satisfactory, as in this period more real development has been carried on than in any similar period in the history of mining in the Province. Prospecting, or the search for new ore-bodies, has also been fairly active, but comparatively few important new discoveries have been reported in the past few years. The mineral output of British Columbia consists of Iode minerals, coat and coke, and building materials. In 1925 the value of the output of these three classes of products was, respectively, about 46, 13, and 3 million dollars. The industry as a whole embraces the mining of these materials, and the treatment and manufacturing processes involved in preparing the various products for the market.

Jan 1, 1926

By Maria Agostina Cinellu

Some aspects of the reactivity of the two different kinds of gold(III) oxo complexes [Au2(N,N)2(?-O)2][X]2 [N,N = 2,2'-bipyridine (bipy) (1), 6-alkyl-2,2'-bipyridine (bipyR) (2), R = Me a, CH2Me b, CHMe2 c, CMe3 d, CH2CMe3 e] and [Au2(C,N,N)2(?-O)][X]2 [HC,N,N = 6-benzyl-2,2'-bipyridine (bipyR') (3), R' = CHMeC6H5 a, CMe2C6H5 b] (X = BF4, PF6) have been studied. Treatment with water converts the unsubstituted bipyridine complex [Au2(bipy)2(?-O)2][PF6]2 (1) and the cyclometallated derivatives [Au2(C,N,N)2(?-O)][PF6]2 (3) into the water soluble monomeric hydroxo species [Au(bipy)(OH)2][PF6] (4) and [Au(C,N,N)(OH)][PF6] (5), respectively. These hydroxo species, likely the intermediates in the formation of the oxo complexes, are quantitatively reverted to the latter ones by reflux in anhydrous solvents. Both kinds of oxo complexes react with PPh3 to give OPPh3, the gold(I) complex [Au(PPh3)2][PF6] and the free bipyridine ligands. The reaction of the dioxo complexes [Au2(bipyR)2(?-O)2][PF6]2 (2a, 2b, 2c, 2e) with different alkenes gives the unprecedented alkene complexes [Au(bipyR)(?2-alkene)][PF6]. The styrene adduct [Au(bipyip)(?2- CH2=CHPh)][PF6] (7) (bipyip = 6-iso-propyl-2,2?-bipyridine c) has been characterized, inter alia, by X-ray diffraction analysis. Organic products arising from olefin oxidation are also found in the reaction mixture.

Oct 1, 2003

By Allan R. Punkkinen

Safe extraction of the valued ore resource in the deep levels of VALE Creighton Mine has progressed in a pillar-less fashion using vertical retreat, slot-slash and uppers retreat methods since the cessation of ?cut and fill? mining in the late 1980?s. Sequencing of the panel extraction and filling has been the key to successful exploitation of high stress orebodies at depth. In late 2010, discussions between the Operating Department and Creighton Ground Control revealed an opportunity to evaluate a trial primarysecondary sequence in the west end of the 400 Orebody at the 2340m horizon. To manage the trial primarysecondary project, a high level risk analysis and management of change was carried out to mitigate potential danger. As part of the requirements, an instrumentation project was conducted in the hanging wall and footwall bottomsills of the secondary panel and within the secondary panel itself. The extraction sequence was modeled with Map3D® software, confirming high stress levels with the advance of the primary panel. Enhanced ground support was installed based on modelling results. A key objective of the instrumentation project was to verify support system response to mining and to obtain knowledge in regards to the behavior of the stope. This paper describes the first time that this type of new innovative instrumented rockbolt technology had been used in a hard rock mining environment. Understanding of the physical deformation mechanisms of ground support in response to high stress conditions is the basis for an effective ground control strategy. The data played an important role in subsequent enhanced ground support system design at the mine and importantly, established the fact that the secondary pillar had not totally failed. Subsequent cavity monitor results helped establish that fact.

Jun 1, 2012

By A. G. Roach

IT IS generally stated that the gold ores of Nova Scotia are free-milling, and for the most part this is true. However, there is a certain proportion of the gold finely disseminated throughout the sulphides, notably arsenopyrite, and this gold is definitely not recoverable as 'free-milling' gold by amalgamation. The proportion of free-milling gold to total gold seems to vary widely in different localities in the Province and is lowest in deposits of the fissure-vein type. The problem of recovery of these relatively recalcitrant values is usually one of economics, in some plac.es a simple gravity concentrate being of such low tenor that its extraction and subsequent disposal will not bear the costs involved. In other cases, such a high percentage of values escapes from the mortars and plates that concentration is definitely indicated. The size of the mining operation is also an important factor. In the large majority of cases, however, some concentrating step is warranted, even if the resulting concentrate is stock-piled until sufficient has accumulated to justify further treatment.

Jan 1, 1940

By Roger V. Pierce

"WITHOUT mineral wealth, modern man would not exist. True, man could survive on a stone-age basis with an average life expectancy of, say, 25 to 30 years -once he got past infancy.However, no metal would tip his arrow in a hunt for protein; no steel plough would break the soil for the organized planting of seed; and no coal, nor oil, nor natural gas nor uranium fuels would pro-vide him with light or beat or safety from either beasts, or other men, or an unkind nature that threatened him and his family.Modern agriculture, fishing and forestry represent the other three wealth-producing industries. With-out metals, non-metallics and energy minerals, however, it would be impossible to fit any of these to man's modern needs."

Jan 1, 1967

By S. Ivanova

The results presented in this paper show that the gold solution dilution is a key parameter to control the dispersion of gold on ?-Al2O3 the selected support. The variation of concentration leads to changes in pH which modify the nature of gold complexes from HAuCl4 formed in the solution. These complexes are presented. Some of them (AuCl3(OH)- and AuCl2(OH)2 -) react with the surface of alumina and give interesting interaction. AuCl2(OH)2 complex has been considered as an ideal complex because of the strong anchorage of a bidentate species on the alumina. This complex is formed mainly in a solution of gold with a concentration of 10-4 M giving a pH of 3.5-4.5. The nature of the anchorage and the amount of chlorine, has an influence upon the formation of Au-Cl bridges which modify the dispersion of the gold on alumina of the final catalyst as shown by TEM.

Oct 1, 2003

By J. Béland

"Three stages, each characterized by a particular sedimentation, magmatism, mineralization and deformation, are recognized in the geological history of Gaspe. The first stage led to the formation of the Taconian orogen, the second to that of the Acadian orogen and the third stage to the accumulation of a post-orogenic cover. The Taconian orogen includes volcanic and detrital rocks of Late Precambrian or Cambrian and Lower to Middle Ordovician ages in which ultrabasic intrusions have been emplaced. Folding is severe. Mineralization is of the Cr-Ni-Cu type, related to the igneous facies.The rocks constituting the Acadian orogen include two distinctive sequences corresponding to two successive sub-stages. The second substage began in Early Devonian time with the first pulses of the Acadian orogeny. The rocks of the first substage grade southward from a nearly platformal sequence to an assemblage implying less stability and spotty volcanism. The second substage was one of synorogenic deposition of elastic rocks, first in a marine environment and later under terrestrial conditions. Granitic intrusions, surrounded by aureoles of skarn and hornfels in which Cu-Pb-Zn mineralization is found, accompanied the Acadian deformation. The second-stage"

Jan 1, 1969

By L. K. Mireku

"Abstract - The Halfmile Lake South Deep zone, Bathurst Mining Camp, New Brunswick, was discovered by Noranda Inc. (Exploration) as a result of a 3-D seismic survey in 1998 and the subsequent drilling of ten diamond-drill cores. The deposit consists of massive, breccia, and stockwork Pb-Zn-Cu sulfide minerals, and is hosted by a volcano-sedimentary sequence belonging to the overturned Ordovician Tetagouche Group. Epiclastic rocks and interbedded fine-grained felsic pyroclastic rocks dominate the stratigraphic footwall. Locally, crystal-rich felsic tuffs and subordinate epiclastic rocks comprise the immediate stratigraphic hanging wall. The entire stratigraphic sequence was intruded by quartz-feldspar porphyritic intrusions, and cut by intermediate and basic dikes. The volcanic and sedimentary rocks can be discriminated geochemically using trace element ratios such as Zr/TiO2 and Nb/TiO2, despite intensive alteration and cleavage development. These ratios indicate that four protolith volcanic compositions exist: rhyolite, dacite, andesite, and basalt. The aphyric and feldspar- and quartz-phyric volcanic rocks are dacitic and rhyolitic in composition; epiclastic rocks have trace element ratios consistent with dacitic compositions. Pearce element ratio diagrams, general element ratio diagrams, and petrographic observations demonstrate that the rhyolitic volcanic rocks exhibit evidence of albite, potassium feldspar, and quartz fractionation, dacitic volcanic rocks exhibit little evidence of any fractionation, and epiclastic sedimentary rocks exhibit evidence of quartz sorting only. Hydrothermal alteration is best represented by the presence of phengitic muscovite and daphnitic chlorite. Minor calcite occurs in the stratigraphic hanging wall, deep in the stratigraphic footwall, and in post-mineralization dikes, and thus is not interpreted to be part of the causative hydrothermal event. Element additions and losses during alteration have been used to determine net alteration reactions, and these have been used to identify alteration parameters that are independent of other forms of alteration and fractionation/sorting, and which can be used to guide exploration. These parameters include: a bulk hydrolysis measure, (2Ca+Na+K-2CO2)/Al; a muscovite alteration measure, K/Al; an albite destruction measure, Na/Al; a chlorite alteration measure, (Fe+Mg-S/2)/Al; a chlorite composition measure, (Fe-S/2)/Mg; a sulfidization measure, S/Ti; and a carbonatization measure, CO2/Ti. With the exception of the carbonatization measure, these alteration parameters define a distinct lateral and vertical zone of intense hydrothermal alteration in the stratigraphic footwall of the deposit, and demonstrate that the epiclastic rocks are predominantly chlorite altered, and the volcanic rocks are predominantly muscovite altered. Within the alteration halo, element additions of Fe and H, and element losses of Na are characteristic. Potassium was added to muscovite-altered rocks, but subsequently removed from chlorite-altered rocks. The results from this study demonstrate that metamorphism and deformation have not significantly obscured hydrothermal alteration signatures."

Jan 1, 2006

By R. V. Hopper, M. E. Wilson, L. S. Trenholme

"The Company known as Rouyn Merger Mines, Limited, was formed in 1943 to take over the ownership of claims in Rouyn and Joannes townships formerly held by East Rouyn Mines, Limited, O'Neil Thompson Mines, Limited, and the Hosking-Cockeram Prospecting Syndicate. The NorandaSenneterre branch of the Canadian National railway passes in an approximately east-west direction through almost the entire length of the property. Since 1937, sixty-three diamond drill holes have been drilled from the surface to cross faults on the contact of the Timiskaming sediments with the Abitibi ( Keewatin) volcanics, along which ore has been found to occur. Late in 1945, the sinking of a 3-compartment inclined shaft in the andesite agglomerate beneath the ore zone was commenced. On January 17th, 1947, this shaft had a depth of 944 feet; cross-cuts have been driven north-northwest from the shaft at 150-foot intervals from depths of 200 to 800 feet on the shaft (Fig. 2).GEOLOGYThe western or East Rouyn part of the Rouyn Merger property in which ore is being mined adjoins the area owned by McWatters Gold Mines, Limited, on the east and is underlain by the eastern continuation of the McWatters formations. As at the McWatters, the rocks belong structurally to three areas: (1) the territory north of the Cadillac-Bouzan Lake fault, occupied almost wholly by Abitibi ( Keewatin) volcanics; (2) the area along the south boundary of the property, underlain by Timiskaming conglomerate and greywacke; and (3) the synclinal belt of McWatters volcanics and sediments between areas 1 and 2.1Bouzan fault of Hawley."

Jan 1, 1954

"HPGRs operate in a wide array of applications in mining and minerals. These range from relatively coarse crushing of copper and gold ores at one end of the spectrum to the processing of fine iron ore pellet feed and fine industrial mineral products at the other. Traditionally these circuits involve the treatment of relatively moist materials in pre-grinding circuits; using single stage HPGRs in open circuit or as a closed circuit operation with screening or partial product recycle. More recently, HPGR is increasingly deployed in dry grinding in combination with air classification. The high throughput demonstrated by larger HPGRs has stretched the application towards coarser size reduction duties for a number of new projects. At the same time, the basic principle of inter-particle crushing for generating a product with a high fines proportion gives ground to investigate applying the technology further towards finished product duties. The advantages that HPGR brings are clear. Multi Stage grinding enables energy efficient size reduction across more of the comminution circuit. Primary HPGR serves for a coarse grinding duty, whereas a secondary HPGR is geared towards generating a fine product for downstream processing or even a finished product. This publication summarizes some of the features of staged HPGR circuits and discusses some examples of operating and projected applications.INTRODUCTION In most HPGR applications, the grinding units are used as a single process stage, either in open circuit, such as for pebble crushing [Rose 2002, Westermeyer 2000, Van der Meer 2015] or in closed circuit with classification [Van der Meer 2009, 2012] or product recycling [Van der Meer 2010]. Where a higher plant capacity is required, the HPGRs are commonly installed in multiple lines in a parallel arrangement [Parker 2005, Koski 201, Vanderbeek 2006]. HPGRs can take a wide range of feed size distributions, and grind this down to a product with a high fines content. In general view, there is a limit on the size reduction range that even an HPGR can provide. Grinding down from a very coarse ore (e.g. 70-100 mm) to a very fine product (e.g. 100 microns range) is stretching the ability of a single stage HPGR circuit. Fine grinding generally requires a classification stage that returns the classifier oversize to the head of the HPGR circuit. From one point of view, it can be demonstrated that when recycling a large proportion of fines and middlings back to the HPGR feed results in an effective feed with an overrepresentation of middlings and fines, which will eventually reduce the grinding efficiency and consequently result in an increased recirculation mass flow [Van der Meer 2014]. From another point of view the large recycling mass puts a strain or even a limit on the capacity of present-day conveyor capacity."

Jan 1, 2018

By S. Nakamura, K. Fujiwara, S. Hirosawa, S. Tsukamoto, Y. Koshino, Y. Aruga

"In this study, hardness test, differential scanning calorimetry(DSC)and transmission electron micros copy were carried out to investigate the age-hardening behavior of Al-Mg-Si alloy with a Mg+Si concentration of 1.5mass%, and a Mg/Si ratio of 1.0. Pre-aging treatment was conducted for the solution-treated and then water-quenched specimen at 100, 80, 60, 40, 20 (natural aging), 0 and -20°C for 20min or 5h, followed by artificial aging at 170°C for 20min. It was found that when pre-aging time is prolonged from 20min to 5h, the bake-hardening response is deteriorated irrespective of the pre-aging temperature. In particular, the specimens subjected to pre-aging at 20-40°C for 5 h hardly increased the hardness with the subsequent artificial aging. From the results of DSC measurement, it was suggested that as pre-aging temperature is lowered, the amount of solute clusters formed during pre-aging, i.e. Mg-Si clusters and Si-rich clusters, is decreased, but the ratio of Si-rich clusters is increased, resulting in the deteriorated bake-hardening response.INTRODUCTIONIn recent years, Al-Mg-Si alloys have been widely used forautomotive body panels due to their excellent characteristics such as high strength-to-weight ratio and good formability. Their strength is increased not only by artificial aging during paint-bake treatment; i.e. “bake-hardening”, but also when kept at room temperature(RT);i.e. “natural aging”, in association with the suppressed bake-hardening response. Such a “negative effect of two-step aging” has been a serious problem because Al-Mg-Si alloy coils are unavoidably maintained at RT in the manufacturing process of body panels; e.g. shipping and storage. However, it was reported that pre-aging above 70°C before the two-step aging can restore the bake-hardening response, and such an improvement is related to the formation of solute clusters(Sato, 2006; Abidet al., 2010; Takaki et al., 2014; Zandbergen et al., 2015). From the comprehensive analysis by three-dimensional atom probe (Aruga et al., 2014 and 2015), it is believed that Mg-Si clusters formed during pre-aging transform into the strengtheningß"" phase, whereas Si-rich clusters formed during pre-aging act as a detrimental precursor of ß""phase. In this study, it was aimed to investigate the effect of pre-aging conditions, especially pre-aging temperature and time, on the formation of solute clusters during pre-aging, in order to elucidate the mechanism of the age-hardening behavior of an Al-Mg-Si alloy."

Jan 1, 2018

By W. L. Brown

"The properties of Base Metal Mining Corporation are in Yoho Park about 2 1/2 miles northeast of Field; British Columbia; on the main line of the Canadian Pacific railway. There are actually two mines; the Monarch on mount Stephen and the Kicking Horse on mount Field; separated by the steep valley of Kicking Horse river. The outcrops of the orebodies range from 4; 900 feet to 5; 300 feet above sea-level. The concentrator is situated below the Monarch mine and is connected to the main portal by an aerial tramway. The ore from the Kicking Horse mine is conveyed by aerial tramway to a storage bin on the main highway and is then trucked to the concentrator.During the construction of the Canadian Pacific railway through Kicking Horse valley, galena float was found at the base of mount Stephen. The East Monarch outcrop was staked in 1894. The outcrop of the West Monarch ore body on the cliff face of mount Stephen was not discovered until 1916. The Kicking Horse orebodies on mount Field were discovered a few years later. In 1912, a 75-ton concentrator was erected, which operated at intervals until 1924. During this period approximately 42,000 tons were mined and milled, largely from the East Monarch orebody. In 1928, the Base Metal Mining Corporation, Limited, was formed to take over the Monarch and Kicking Horse mines. A 300-ton differential flotation concentrator was erected and production started in the autumn of 1929. In a very short time, however, the low price of metals forced the mill to shut down until August 1933. From 1929 to 1935, when the mill again ceased operation, a total of 256,500 dry tons of ore, averaging 1.59 oz. silver per ton, 9.7 per cent lead, and 12.6 per cent zinc, was mined and milled, largely from the West Monarch orebody. After a period of further underground development, the concentrator reopened in 1940 and is still in operation. From 1940 to the end of 1944, 354,363 tons of ore was milled, averaging 5.32 per cent lead and 10.47 per cent zinc."

Jan 1, 1954

By W. A. Alexander

Introduction In the course of a programme of research on beryllium in progress in these laboratories, knowledge of the recrystallization temperature became necessary. As the information is not available in the literature, the determination of this temperature for metallic beryllium was undertaken. By the reduction of grain size through working and recrystallization and the probable simultaneous induction of preferred orientation, it was hoped to improve the working properties of beryllium at lower temperatures. The recrystallization temperature is usually determined by observing the lowest temperature of annealing at which new crystals are formed in severely cold-worked metal or alloys. This temperature is profoundly influenced by the following factors: the purity of the metal, in the case of an element, or the composition of the alloy; the degree of straining or working; the temperature of straining; the original grain size; and the time held at the annealing temperature. The observed temperature is lowered by higher purity, more severe straining, lower temperature of working, smaller original grain size, and longer time of annealing. Beryllium presents special difficulties in that the percent elongation in tension is effectively zero, so that ordinary squeezing or rolling was not possible. A possible means of straining was suggested by the fact that indentation hardness tests could be made. It was known from earlier work that the metal could be worked at elevated temperatures, so that working at the lowest feasible temperature and quenching might also be a means of producing strain. The purity of the metal is also a point of some uncertainty in the case of beryllium. Losano has prepared 99.96% Be which appears to be the best reported. Distilled metal used in the present work approached this purity. However, by analogy with other metals, residual impurities may have a pronounced effect on the recrystallization. Further purification of beryllium would evidently entail considerable difficulties due to the highly reactive nature of the metal, and was not attempted.

Jan 1, 1947

By T. G. Edgeworth

Some of the historical background of the industry is reviewed, with reference to the different types of reduction cells in use for aluminum smelting. Factors to be considered in cell des1gn involve capital, power, and operating costs. The trend is apparently toward larger cells. The industry is studying new construction materials for cell linings, as well as alternate electrolyte compositions and other design changes which will improve productivity and energy efficiency. The aluminum smelting activity in other countries is briefly reviewed. TODA Y'S industrial production of aluminum is still based on the simultaneous discoveries made in 1886 by Charles Martin Hall in Ohio, and Paul Heroult in France. Up to that date, only about 50 tons of aluminum had been produced in the world, and the price at that time was about $5 per pound. Sucl1 figures must be contrasted with the present world aluminum smelting capacity of over five mil-lion tons per year, and a price of about 25 cents per pound.

Jan 1, 1962