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By Vernon R. Miller

The Bureau of Mines developed and evaluated a detector-sorting device to separate the copper-bearing portion from the barren portion of native copper ores. Small-scale sorting tests were run on minus 1-inch plus 1/2-inch size materials from the following Michigan samples: Winona, Kingston, and Centennial ores, and "poor" rock from the Champion mine dump. Results showed that 60 to 85 pct of the copper was recovered in 9 to 19 wt-pct of the sorted fraction. About 90 pct of the copper recovered was obtained in the first pass through the sorter. For the Kingston and Centennial ores, combinations of sorter concentrates and fines generated during crushing, resulted in recoveries of 93 and 94 pct, respectively, of the total copper in the samples. The combined products constituted about 66 wt-pct of the total sample and allowed the balance to be discarded with only a 6 to 7 pct copper loss.

Jan 1, 1974

By B. T. Brady

Laboratory measurements by the Bureau of Mines indicate that failure in dry rock specimens measuring approximately 13 cm in length is preceded by tilt anomalies lasting a few milliseconds. The tilt behavior is qualitatively similar to that reported to precede earthquakes. Test results suggest that the time duration of this tilt anomaly for laboratory specimens of this length is independent of rock type, in agreement with theoretical predictions and other experimental data on rock failures including earthquakes.

Jan 1, 1975

By G. A. Brady

Seven samples of Pennsylvania anthracite from the Bottom Ross bed were analyzed and tested to obtain data on cleaning characteristics, proximate and ultimate analyses, specific gravity, grindability, heating value, and ash softening temperature. Ash content of the samples varied irregularly from 9.0 to 34.4 percent, the range being narrowed to an upper limit of 14.8 percent ash by removing impurities dense enough to sink in a medium with a specific gravity of 1.90. Ash content of the sink material with specific gravity greater than 1.90 ranged from 56.4 to 80.4 percent; corresponding specific gravities were 2.095 to 2.534. Volatile matter contents were indicated to be higher for the ash-forming minerals than for the pure coal substance in the various specific gravity fractions of a given sample. Specific gravities of anthracites with compa¬rable ash contents but from different locations in the bed varied as much as 0.06. The grindability index increased significantly with increasing ash con¬tent of specific gravity fractions from all the samples.

Jan 1, 1968

By L. H. Lange, F. F. Hintze

"Mineralogical Composition of Cyanite RockIn the group of minerals used in making this study, the cyanite is associated with quartz, mica, and feldspar in the schist. The amount of quartz is variable, but it is always an abundant mineral. Both large and small crystals of quartz occur in irregular masses, rarely ever showing crystal outline. Mica is of the clear and dark varieties the larger crystals being dark as a rule, and the finer crystals of light color, The present mineralogical composition of the mica is rather variable as most of the original biotite and muscovite have suffered alteration, and much secondary mica is present as a result of alteration of the original mica and other minerals present, especially the larger cyanite crystals. A large part of the mica now found in the ore is chlorite, with varying amounts of Jefferisite and others, especially sericite. These are in the form of aggregates, or felt-like intergrowths filling the spaces between the quartz, cyanile, and feldspar.The feldspar is plagioclase probably mostly albite. It is white, possesses good cleavage, and is one of the hard brittle minerals of the rock. It alters to kaolin, and sericite, and more or less of these alteration minerals are present within the feldspar crystals but not separated from them.The cyanite is of two varieties, distinguished by their colors as blue and white cyanite. The blue color varies in intensity, being a pronounced blue in some crystals and paler in shade in others. Some crystals have been seen which possess the blue color in one-half of their mass and are pure white or clear in the other half. The purity of the cyanite is probably not affected by the color, but it is difficult to detect the white cyanite in the ore by macroscopic examination, so that great care has to be exercised in the selection of the ore in the field."

Apr 1, 1931

By F. F. Hintze

In the group of minerals used in making this study, the cyanite is associated with quartz, mica, and feldspar in the schist. The amount of quartz is variable, but it is always an abundant mineral. Both large and small crystals of quartz occur in irregular masses, rarely ever showing crystal outline. Mica is of the clear and dark varieties, the larger crystals being dark as a rule, and the finer crystals of light color. The present mineralogical composition of the mina is rather variable, as most of the original biotite and muscovite have suffered alteration, and much secondary mioa is present as a result of alteration of the original mica and other minerals present, especially the larger cyanite crystals. A large part of the mica now found in the ore is chlorite, with varying amounts of Jefferisite and others, especially sericite. These are in the form of aggregates, or felt-like intergrowths filling the spaces between the quartz, cyanite, and feldspar.

Jan 1, 1931

By Suresh K. Bhatt, Dennis R. Dolinar

The roof bolt system of a mine, if properly selected and installed, can allow for better roof control and reduce the potential for roof falls. Because of this potential to reduce roof falls and improve ground control conditions, the National Institute for Occupational Safety and Health (NIOSH) has an interest in the types of roof bolts that are used by the coal industry. Further, NIOSH has conducted research into how various support parameters can affect the number of roof falls that occur, including support type. Today, the five main types of roof bolts installed in U.S. coal mines are mechanical anchor bolts, point-anchor or resin-assisted mechanical anchor bolts, torque-tension bolts, combination bolts, and fully grouted resin rebar. This paper describes each support in detail. Because of the importance of resin in the functioning of the majority of bolts installed, resin grouts are also discussed. Further, trends in the types of roof bolts used are reviewed. Over the last 10 years, the significant trend has been the large reduction in the relative number of mechanical anchor bolts that are installed. These bolts have been replaced mainly by the resin-grouted rebar system. Data are also presented to show the impact of these changes in bolting on the number of roof falls.

Jan 10, 2000

By J. F. Barkley

As part of the work of serving as Chairman of Subcommittee 3, Health and Industrial Requirements, of the American Society of Mechanical Engineers' Committee on Air-Pollution Controls, the author assembled the following information on accepted maximum permissible concentrations of air pollutants from the standpoints of health, damage to vegetation, damage to property, and requirements of industrial processes. A search in technical literature was made followed by direct inquiry to all State governments as to their regulations. The subcommittee membership - G. D. Clayton, senior sanitary engineer, Public Health Service, United States Department of Health, Education, and Welfare, Detroit, Mich., Dr. L. Greenburg, commissioner; Department of Air Pollution Control, New York, N.Y., Dr. M. Katz, Defence Research Chemical Laboratories, Ottawa, Ontario, Canada, and Dr. H. H. Schrenk, research director, Industrial Hygiene Foundation of America, Inc., Mellon Institute, Pittsburgh, Pa. - reviewed the information and made very helpful comments and corrections.

Jan 1, 1954

By Deborah A. Kramer

As part of the Nation's growing concern with the competitiveness of U.S. firms in the world economy, especially with respect to advanced materials, the Bureau of Mines assessed the actual and potential recovery and manufacturing capabilities for gallium and gallium arsenide (Gacis). GaAs has advanced from a laboratory curiosity to a material with important "high-tech applications within only the last few years, and although protected North American gallium supplies are currently considered adequate, consumption could grow to the point that this assessment would need reevaluation.

Jan 1, 1988

By A. W. Fahrenwald, W. W. Staley

"In flotation concentration, various machines are employed for agitation and aeration of the ore pulp in the operation of frothing. The power required in the operation of these machines varies considerably with the type and make of machine used. The object of this investigation was to determine the effect of certain physical properties of the pulp particularly viscosity, density, and temperature - upon the power required by certain forms of pulp agitators.The viscosity factor is most involved because it is affected by temperature and by density. Viscosity of liquids and suspensions has been extensively studied and the physics and mathematics of the subject are much enlarged upon in books and in the literature. It is not, however, the intention of this study to become involved in the intricacies of these phases of the subject.The agitation of the various mediums in the experimental work did not last long enough to cause a measurable rise in temperature from the ""beating"" of the medium, hence no cognizance is taken of this factor.No attempt has been made to correlate the data obtained with the impeller with any information regarding centrifugal pumps. The object sought here is quite foreign to the problems of pumping. The impellers used are ""open"" and air is involved.The experiments performed and the data obtained are presented. Only that amount of discussion necessary to make the results understandable is given.Tap water was used in all experiments. A comparison of distilled water and tap water showed no measurable difference. In the experiment in which sodium chloride was needed, the commercial salt as used in fire assaying was taken. The quartz was of the ""bull quartz"" variety, thoroughly washed free of iron oxide."

Jun 1, 1930

By Murray Jacobson

The respirable dust standard in the Federal Coal Mine Health and Safety Act of 1969 is designed to prevent disability and death from coal workers' pneumoconiosis. Beginning June 30, 1970, the operators of coal mines were required to maintain the average concentration of respirable dust in the active workings at or below 3.0 milligrams of dust per cubic meter of air. The standard is reduced to 2.0 milligrams per cubic meter after Dec. 30, 1972. This paper presents the equipment and procedures used by the coal mine operators in implementing the respirable dust sampling program established by the Secretary of the Interior and the Secretary of Health, Education, and Welfare and shows the effect of the law, during the first year, on the reduction of dust levels in selected mines. The system employed by the Bureau of Mines for analyzing and processing the dust samples is also presented.

Jan 1, 1971

By Gordon E. Fletcher

This Bureau of Mines report outlines the atomic absorption analysis of oilfield brines for barium, calcium, copper, iron, lead lithium, magnesium, manganese, potassium, sodium, strontium, and zinc, using the method of additions. The advantages of using atomic absorption are discussed. The method of additions was chosen to overcome large matrix interferences usually found in brines; techniques of overcoming chemical, ionization, and background interferences are also described. The method was used to analyze several hundred oilfield brines and found to be rapid and reasonably accurate. A solvent extraction method was used to concentrate lead, copper, zinc, and iron in low-level samples.

Jan 1, 1974

By R. L. Montgomery

The heats of solution of erbium chloride in water and in hydrochloric acid and of erbium oxide in hydrochloric acid were determined. The results reveal a discrepancy of 10.5 kcal. per gram-atom between the heats of combustion and solution of erbium reported in the literature, the heat of combustion being more negative. The heat of combustion of erbium t4)4 and its heat of solution in hydrochloric acid (1, 18) have been reported in the literature. The heat of solution of erbium chloride was determined in two studies (2, 19). The present work was undertaken to check the reported heats of solution of erbium chloride and to determine the heat of solution of erbium oxide in hydrochloric acid. The latter quantity permits the heats of combustion and solution of erbium to be compared for mutual consistency. It was also desired to determine the degree of similarity between the thermochemistry of yttrium and erbium.

Jan 1, 1961

Provide reasonably priced, reliable fire protection for loading shovels. Approach An automatic fire, sensing and suppression system using both dry chemical and Halon 1301 was developed. It is more rugged than similar industrial-type fire protection systems. How It Works Temperature sensors detect heat from a fire, and trigger the system. These sensors are located inside the machinery house and under the house and shovel frame where it rotates around the crawler chassis ring gear. An alarm is sounded, and extinguishing agents are released either in the machinery house or in the ring gear area. The system can also be triggered by a manual control. If the fire Is detected in the machinery house, all power is shut down to the motor-generator sets, ventilation fan, and all electrical controls. Doors are automatically closed. After a delay to allow time for the ventilation fan to stop, Halon 1301, a gaseous fire extinguishing agent, is released inside the machinery house until it reaches a concentration of about 7 percent. This concentration is sufficient to extinguish a fire, but isn't toxic to personnel

Jan 1, 1980

To improve the reliability of the Bureau developed bore-hole gage now widely used to determine the absolute state of stress in rock. Approach Use the knowledge gained by extensive field tests to design a more rugged and reliable Instrument using lighter and stronger materials. How It Works The original gage consisted of a stainless steel cylinder 1-3/8 Inches In diameter and 10-1/2 inches long. The new gage is made from titanium. This lighter material reduces the weight of the gage by 43 percent, which enhances the gage placement and depth of overcoring in vertical up? holes. For added strength, the titanium case and placement end are now threaded to the gage body instead of using screw fasteners. Three pairs of strain gaged transducers are positioned to measure the diametral deformation of a 1-1/2 diameter borehole at 60-degree intervals around the Inner surface of the borehole. Each transducer consists of a beryllium copper cantilever with a strain gage cemented on each side. These transducers are secured Into the gage body by a tapered shank for minimal creep. The transducers opposite each other are wired together to form a 4-arm external bridge circuit. A pair of transducers is referred to as a component. Any deformation of the borehole, which occurs during overcoring, is detected by pistons which translate the motion to the components. Each

Jan 1, 1982

By John T. Aydelotte, Martin J. Gavin

" Oil shale contains little or no oil as such , but it contains an organic material from which oil may be produced by destructive distillation" . This statement , or others conveying the same meaning, appears in many popular and techni cal articles on oil shale . It is based on the belief that the ordinary solvents of petroleum have but little action on the organic substances contained in oil- yielding shales , although on distillation these same shales may yield upwards of 50 gallons of crude shale oil per ton . A 50 - gallon shale thus yields by distillation 18.73 per cent of its weight as oil ( assuming the specific gravity of the oil to be 0.900 ) , although only a relatively small part of this can be recovered by extraction with such solvents as chloroform , carbon tetrachloride , and the like . In the course of certain experiments designed to determine the solubilities of different shales after they had begun to yield oil by distillation , it was found desirable to determine the quantity dissolved from certain unheated shales by various solvents , at or near the boiling points of these solvents . The method used and results obtained are presented below. These experiments were made in connection with the oil - shale investigations being conducted by the U. S. Bureau of Mines , in cooperation with the States of Colorado and Utah .

Jan 1, 1922

By Robert D. Schmidt

This Bureau of Mines report describes the development and application of a computer model for simulating the hydrological activity associated with in situ leaching. The model is intended to provide uranium resource developers with a description of the flow behavior of leachants and ground water during the development, production, and restoration phases of a leaching operation involving an arbitrary pattern of injection and recovery wells. Different aquifer environments are modeled, using a closed-form solution to the partial differential equation that describes three-dimensional changes in piezometric head as a result of pumping from leachant injection and recovery wells. The computer program can model a maximum of, 50 arbitarily located wells. Numerical techniques involving difference quotients and Taylor expansions about time points are used to derive time, velocity, areal sweep, and fluid volume parameters associated with leaching hydraulics. These parameters are output by the program in graphic and tabular formats. Other numeric methods insure that the program running time is minimized without significantly affect-ing the accuracy of results.

Jan 1, 1980

By P. G. Clites

This study was undertaken to determine the effect of consumable-electrode vacuum arc melting on the properties of copper and to determine the applicability of the process to the production of cast shapes of copper. Ingots and castings were produced from electrolytic tough pitch copper (ASTM designation ETP), from electrolytic cathode copper (ASTM designation CATH), and from oxygen-free copper (ASTM designation OF). The products of this study were evaluated to determine the effect of the melting process on the removal of impurities from the copper and on the physical properties of the copper. The results indicate that consumable-electrode arc melting can be satisfactorily applied to the melting and casting of copper. Ingots prepared directly from electrolytic cathode copper contained slightly higher levels of impurities than are found in commercial oxygen-free copper, Excellent results were obtained with centrifugal castings of unalloyed copper, and reasonably successful static castings can be produced if proper mold and gating systems are employed.

Jan 1, 1963

By Robert F. Chaiken

A novel approach to eliminating environmental and public safety hazards that are associated with fires in abandoned coal mines and waste banks involves the use of in situ combustion technology developed by the Federal Bureau of Mines to accelerate the burning of the wasted coals in place. This technology would be used under exhaust ventilation control conditions that would allow for total management of the hot gases produced. Combustion stoichiometries would be optimized to minimize unburnt combustibles and to maximize the heat content of the gas products, which will be exhausted at one or more fan locations. When necessary, scrubber systems would be employed to remove air pollutants, such as sulfur dioxide; heat utilization systems (process heat, steam, and electricity) would also be employed to offset operational costs. Ultimately, complete burnout would solve the fire and acid water formation problems of the abandoned coal mine or waste bank. Pertinent technical data for burnout control are derived and discussed in terms of the important material and operational parameters. In general, it is believed feasible to operate a burnout system in an existing abandoned mine or waste bank fire at thermal power levels in the range of 10 to 100 Mw, and at exhaust gas temperatures of 1,000° C (1,830° F).

Jan 1, 1980

By G. W. Jones, R. E. Kennedy

"INTRODUCTION Information relative to the ignition temperatures of acetylene and acetylene-air mixtures has become of particular interest recently due to a number of explosions that have occurred in 500-pound, double-rated, medium-pressure acetylene generators in shipyards on the West coast. Various suggestions have been made as to the causes of these explosions prominent among which has been that air finds its way into the acetylene generators during abnormal operation or that air remains in the carbide hopper of the generator following the purging and charging operations.This raises the question as to how and to what extent the presence of small percentages of air in acetylene affects the ease of ignition of such mixtures at the various operating pressures of the acetylene generators. The range of operating pressures in the 500-pound, double-rated generators involved in the explosions may vary from below atmospheric to 15 pounds gage.The present report gives the results of an investigation made to determine the effects of pressure on the ignition temperature of pure acetylene and of acetylene containing varying percentages of air:EXPERIMENTAL Apparatus A preliminary investigation showed that a heated quartz surface gave lower ignition temperatures than other material tested.A ""hot-spot"" method of ignition was found desirable in the case of the acetylene mixtures since the violence of the explosions was reduced by keeping most of the test mixtures at room temperature. Explosive violence was reduced further by using an ignition tube 17 mm. or less in diameter."

Mar 1, 1945

Provide reasonably priced, reliable fire protection for AN-FO haulers. Approach An automatic fire sensing and suppression system for AN-FO haulers was developed and on-vehicle tested. How It Works The system works in two ways to protect personnel from dangerous and unpredictable AN-FO fires. First the system senses and suppresses fires on the truck before they spread to the AN-FO in the bunker. This design was chosen because AN-FO truck fires generally start when combustible liquids (such as diesel fuel, hydraulic fluid or lubricating oils) are ignited by hot surfaces mainly on three areas: the engine, the transmission or the power take-off. These fires are quickly sensed by a linear temperature sensor strung throughout these three areas. The system then warns the operator and automatically suppresses the fire by discharging 30 pounds of multipurpose dry chemical extinguishing agent through a network of fixed hoses and nozzles. Second, this system includes six spot thermal sensors mounted inside the bunker on the truck to monitor the AN-FO temperature in case a fire does spread to the bunker area. If the bunker temperature rises to 190° F, a loud siren is sounded to warn nearby per-

Jan 1, 1981