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Infacon 74 The National Institute for Metallurgy, the South African Institute of Mining and Metallurgy, and the Ferro-Alloy Producers' Association of South Africa extend a cordial invitation to participate in the International Ferro-alloys Congress to be held in Johannesburg, South Africa, in April 1974. Obituary RICHARD AUSTIN COOPER On the 31st March 1972, a once very active member of the Institute, R. A. Cooper, died at the age of 82. He had served on the Council for many years and was Vice-President in 1933/34. ALEXANDER JEREMIAH ORENSTEIN CB., CM.G., C.B.E., LLD., D.Se., M.D., M.R.C.S., F.R.CP., F.R.S.H. Dr Orenstein, who died on the 7th July 1972 at the age of 92, was so well known and so widely acclaimed during his lifetime that it is difficult to add to the tributes which have already been paid to him.

By M. Ericsson

?Rare earths ?will not be bargaining instruments?? was stated in a headline in China Daily of 29 October 2010. The Chinese government is trying to fend off the persistent accusations from Japan, the USA, and Europe that it is manipulating the supply of these so called ?critical? metals to gain political and economic advantages. The critics maintain that China has taken the rest of the world hostage by controlling 97% of the resources of rare earths. These elements are crucial in a number of high-tech applications. They are not impossible to substitute, but difficult to do so effectively. The name ?rare earth? is a misnomer, as even the least abundant is 200 times more common in the Earth?s crust than gold. They are, however, difficult to find in economic concentrations. The Chinese near-monopoly over the rare earths, together with China?s scramble for other resources in Australia, Africa, and elsewhere around the world, is seen as an example of a Chinese strategy to take control of vital metal resources. The Chinese are also accused of using unfair and sometimes illegal business practices in this fight for resources. Practices which, critics claim, put the Chinese interests above the interests of the host countries, in particular in Africa.

Jan 1, 2011

The 89th Annual General Meeting of The South African Institute of Mining and Metallurgy was held at Kelvin House, Johannesburg, on 20th August, 1986. Mr. H. E. James (President) was in the chair and declared the meeting open at 16hoo. Obituaries President: It is my sad duty to announce the deaths of the following members of this Institute: Life Fellow D.L. Carson; Retired Fellows T.K. Adams, G.E. Carlyon, N.M. Holford, D.E. Maclver, C.J. Morgan; Fellows S.K. de Kock, R.R. Porter, Dr G.J. Rees; and Associate Sir Lindesay Clark. As a mark of respect to the memory of the deceased and in sympathy with the bereaved, please rise and observe a moment of silence. Minutes President: The 88th Annual General Meeting of the Institute was held on Wednesday, 14th August, 1985, and the minutes were published in the September 1985 issue of the Journal. The minutes were confirmed.

Jan 1, 1986

The Grants register 1979-1981, edited by Roland Turner. London, MacMillan, 1980. (Available from Geonicla Publications, P.O. Box 31487, Braamfontein 2017 at R31,37; price to libraries R28,33.) Buyer's guide. Pretoria, South African Bureau of Standards, 1980. (Available free of charge from the Director General, SABS, Private Bag X191, Pretoria 0001.) SABS specification on gold alloys. World coal resources, by Bernardo F. Grossling. London, Financial Times, 1980. 160 pp. $D.S.155. Resources policy, a quarterly journal publish d in March, June, September, and December. Annua subscription: £40. Diamond jubilee 1980 The Associated Scientific and Technical Societies was established in 1920 primarily to 'promote the interests of Scientific, Professional and Technical Societies, the advancement of knowledge in Scientific and Technical subjects, and to uphold the professional status of such Societies,' and to 'represent corporately the views of Scientific, Professional and Technical Societies and the members thereof'. In this manner the strength of unity

Jan 1, 1980

By T. Groenewald

Potential applications of thiourea In the processing of gold by T. GROENEWALD, Ph.D. (Rand), D.I.C. (Imperial College) (Visitor) The aqueous chemistry of gold(l) that has found practical application is mainly the chemistry of the anionic complexes involving ligands such as cyanide. sulphite, and the halides. The one potential exception is the cationic gold(I)-thiourea ion. While many laboratory studies have been made during the past decade. the application of thiourea in the processing of gold is only now reaching the development stage. While thiourea is relatively inexpensive. recent interest has probably been spurred mainly by the novel technology that could arise out of the cationic properties of the gold-thiourea ion. This review outlines the chemistry of gold and thiourea. and discusses the possible use of thiourea in the processing of gold with respect to dissolution. solvent extraction. ion exchange, electrowinning. electroplating. electroless deposition. electro-etching, and electropolishing.

Jan 6, 1977

By D. G. Krige

Some basic considerations in the application of geostatistics to the valuation of ore in South African gold mines by D. G. KRIGE, Pr. Eng., D.Se. (Eng.) Rand (Fellow) There is much room for improvement in the statistical procedures that have been used by gold mines over the past decade in the valuation of their ore reserves. Improvement depends on the establishment of the extent to which the patterns of frequency distributions and the directional variograms for the gold values vary from area to area within each section of a mine. The application of the lognormal distribution and of the De Wijsian variogram model for routine ore-reserve valuations requires detailed study before some of the reservations still held by mathematical statisticians can be met. This paper provides some preliminary evidence of the extent to which these models can be used with confidence, as well as suggesting how they can be applied to their full potential.

Jan 4, 1976

This International Mine-Surveying Conference will take place in Budapest (Hungary) from 5 to 14 June, 1972. Detailed information can be obtained from the Mine-Surveying Working Committee of the Hungarian Mining and Metallurgical Society. Write: OMBKE Bányaméröi Munkabizottsag Budapest, V., Szabadsag ter 17, Hungary. SYMPOSIUM ON NICKEL The 'Gesellschaft Deutscher Metallhiitten-und Berglaute' is holding a Symposium on nickel on 24-25 September, 1970 at Wiesbaden, on the occasion of the G.D.M.B. Annual Meeting. Some 24 papers will be presented by metallurgists from many important companies around the world. Information may be obtained from The Secretary, G.D.M.B., Postfach 210, 03392 Clausthal-Zellerfeld, German Federal Republic. VISIT TO THE COUNCIL FOR SCIENTIFIC AND INDUSTRIAL RESEARCH On 23rd June, 1970, members of the Institute visited the C.S.I.R. in Pretoria. More members had booked for this tour but the current flu epidemic caused cancellations which was unfortunate. The visit was organised with military precision, which prevented detailed discussion of any particular subject, but provided a bird's eye view of a large number of interesting projects. The visit was packed with interest for all and those requiring further information were invited to contact the relevant divisions afterwards. Or Denkhaus welcomed the delegates and stressed the importance of integrating research efforts with industry's requirements. An excellent colour and sound film was shown which depicted the work of the Rock Mechanics division. This showed very clearly methods used for preparing rock samples and demonstrated the machines and instruments for the various tests. It made one realise the extent to which this research has been integrated with the actual mining situation. The fullscale experiments underground showed the failure of pillars under applied loads and were very interesting. This is undoubtedly a film which all mining people should see. After the film the rock mechanics laboratories were visited where the actual machines were seen and described. We then visited the metal and strength mechanics sections where the metallurgists were able to see some interesting experiments and tests. We also visited the Aeronautics Research group where a large 1 000 hp wind tunnel was inspected. We were told enough about this to realise something of the complexities involved in the design and operation of a closed circuit tunnel of this type. The tunnel is used for tests on models which are necessary for the design and modification of aircraft. After a very excellent lunch at the C.S.I.R. recreation centre, the delegates attended two lectures-one by Mr. Mandersloot of the Chemical Engineering group, who outlined the varied functions of this group and told us something of their work. Of particular interest was the research into the suitability of various South African manganese ores for dry cell batteries. Work on the thickener settlement studies interested the metallurgists. The second lecture was given by Mr Donaldson of the National Building Research Institute. This Institute has about ten divisions each of which covers a particular aspect of building research. The work of the soil mechanics division was described in detail and illustrated by coloured slides. This was particularly interesting and demonstrated clearly how building failures result from lack of attention to detail of construction where unstable soil conditions exist. Cracks in walls of compound blocks brought the subject home forcibly to the mining delegates. This division has also caried out important work on sinkholes and sUmes dams and produced some positive results. Altogether the visit was most interesting and enjoyable. It was made more worthwhile because the emphasis was on the work being carried out and not on just seeing the laboratories. The Institute is greatly indebted to the C.S.I.R. and its staff for the very excellent arrangements made.

By K. R. Vost

Variation in air temperature in a cross-section of an underground airway by K. R. VOST, B.Sc. (Glas.), M.Sc. (N.S.W.) (Visitor) Measurements of air temperatures in underground airways are normally made at only one point in a cross-section, and the air tem peratures at other points in the cross-section are assumed not to differ significantly from this. This paper discusses measurements made at a number of points in fifty crosssections in airways with different air velocities and wetness of floor. These measurements show that significant variations of air temperature can occur in a given cross-section at a given time. The effects of such variations on the accuracy of measurement of rises in air temperature as air passes along an airway are discussed. The importance of considering experimental error in the measured rises in air temperature when attempting to validate theoretical and empirical methods of predicting such rises is also discussed.

Jan 7, 1976

By L. Morin, S. Mortazavi, K. Volchek, A. Demers, A. Di Feo

The objective of this paper was to investigate the possibility of reducing process (fresh) water and increasing recycled water (thickener tank overflow water). As part of the investigation, rougher flotation tests were done with the two water types and a mixture of the two (50%/50%). The effect of recycled water on the grade-recovery response and rougher recoveries was investigated. When thickener tank overflow was used (50% and 100%), the nickel+copper grade versus nickel recovery decreased. The decrease in the grade-recovery was due to higher pyrrhotite recovery. Also, there were no effects on nickel and copper recoveries, which was confirmed using multivariate statistical analysis at the 95% significance level. Keywords: Flotation, nickel, copper, water recycling, multivariate statistical analysis, MANOVA, reverse osmosis

Jan 1, 2020

By I. du Plessis

The metallurgical response of a difficult to treat coal and an easy to treat coal orebody were investigated in terms of the coal yield and the coal quality in a basic coal recovery flowsheet. The purpose of this paper is to show trends and derive principles for the treatment of different coal types. This investigation entailed using the LIMN simulator to simulate the metallurgical response by varying the plant operational parameters. The controllable plant variables investigated were: ?Cyclone size ?Screen and hydro-cyclone cut points ?Medium cut density ?Feed particle size distribution.

Jan 1, 2010

By K. Kabezya

A study on slag dispersion in a model of bottom-blown bath smelting converter was undertaken at room temperature. The aim was to investigate the behaviour of the dispersed slag phase at various operating conditions with very high gas flow rates in low slag volume (10%) systems. For simulation purposes water, paraffin-oil, and air were used to represent the bulk steel, molten slag, and gases respectively in a one-fifth cold model of the commercial 100 t Creusot-Loire-Uddeholm (CLU) converter used in the manufacture of stainless steel in South Africa. Dimensional analysis was done to correlate mathematically the dispersed phase holdup with the operating conditions and the modified Froude number. The overall expression of the holdup revealed that the dispersed slag phase decreased with the vertical distance from the original interface between the liquid phases. The dispersed phase also decreased with the radial distance in the water plume zone toward the sidewall. The holdup was apparently much higher on the side of the reactor where there were no tuyeres. The modified Froude number ensured the correlation between the model and the prototype.

Jan 1, 2014

By J. A. Kinnaird, B. J. Youlton, K. L. Youlton

Methods for treating and processing refractory gold ores are well established. However, what is less well understood is how the formation of the gold-bearing deposits affects gold processing and extraction. In order to evaluate the effect of ore genesis on gold extraction a number of South African gold deposits were studied. These included complex Pilgrim’s Rest samples as well as refractory Fairview, Barbrook, and Consolidated Murchison samples. We found the refractory nature of gold ores is controlled by a limited number of well-understood mineralogical factors. Solid solution gold is linked to low temperature and pressure conditions in fine-grained sedimentary lithologies, while reactive pyrrhotite can form from hydrothermal fluids associated with mafic magmatic rocks. These formational controls can be used to identify and avoid complex deposits at a desktop study phase, or address and reduce complications further along the pipeline using early mineralogical studies.

Jun 1, 2021

OFS Branch Committee Meeting held in the Committee Room at the Welkom Club at 4.15 p.m. on Wednesday, 5th March, 1975. Progress in mineral dressing The National Institute for Metallurgy and the South African Institute of Mining and Metallurgy are to hold a symposium on 17th and 18th September, 1975, entitled 'Recent Progress in Mineral Dressing'. INFACON 74 This book of over 300 pages is a record of the First International Ferro-alloys Congress, which was held in Johannesburg from 22nd to 26th April, 1974, under the auspices of the Ferro Alloy Producers' Association of South Africa, the National Institute for Metallurgy, and the South African Institute of Mining and Metallurgy. NIM reports Report no. 1595 Preliminary tests on low-grade brecciated fluorspar ore from the Ottoshoop district. (5th Nov., 1973, declassified April 1975). Report no. 1612 Flotation tests on sulphide-bearing high-grade brecciated and wad ores. (20th Mar., 1974, declasl>ified April 1975). Report no. 1643 Further tests on low-grade brecciated fluorspar ore from the Ottoshoop district. (12th Jul., 1974, declassified April 1975). Report no. 1654 The determination of osmium in platiniferous media. Report no. 1689 The determination, by atomicabsorption spectrophotometry, of arsenic, selenium, tellurium, antimony, and bismuth on ion-exchange restns. Report no. 1715 Flotation tests on various types of ore from the Ottoshoop district Report no. 1730 The chromitite from the Marico occurrence, western Transvaal, its alteration, and possible reasons for its refractory nature. Report no. 233 A chemical and mineralogical study of microlite from the N oumas pegmatite. 24th Geomechanics Colloquy The above Colloquy is to be held on 2nd and 3rd October, 1975, in the Salzburg Congress Hall. Rosenhain centenary The centenary of the birth of WaIter Rosenhain (1875-1934) will be celebrated by an international conference to consider how physical metallurgy has contributed to engineering practice. Iron and steelmaking The Centre de Recherches Metallurgiques (CRM) and the Verein Deutscher Eisenhiittenleute (VDEh) are jointly to hold the International Meeting on Iron and Steelmaking 1976 in Brussels from 17th to 18th May and in Diisseldorf from 20th to 21st May, 1976. International Symposium on Mine Surveying The III I.S.M. is being held in Leoben, Austria, from 28th June to 3rd July, 1976. Book review Tenth International Mineral Processing Congress. 1973. London, The Institution of Mining and Metallurgy. 1208 pp. £20. Particles A course on particle characterization and a symposium on experience in the applications of particlesize analysis will be held during the last week of July in Pretoria and Johannesburg. A.S. & T.S. Trust The A.S. & T.S. Trust was formed on 24th March, 1972, to mark the Golden Jubilee year ofthe Associated Scientific and Technical Societies, with the object of advancing science and technology in South Africa. Second International Congress of Engineering Geology The Proceedings of the above Congress, which was held in Sao Paulo, Brazil, from 18th to 24th August, 1974, are now available.

Jan 6, 1975

By C. C. Pretorius, S. Ramjee, R. J. Mostert

The study investigates the effect of prior corrosive exposure on crack growth resistance behaviour of thin sheet (3 mm thick) aluminium alloy 2024-T3 at slow strain rates. Compact tension specimens were exposed to standard corrosive environments that simulate accelerated atmospheric corrosion attack. Two corrosive environments were considered – an exfoliation corrosion (EXCO) solution and a 3.5 wt% sodium chloride solution. The unloading compliance R-curves of the two-hour EXCO-exposed specimens revealed a significant degradation of approximately 11% in the crack growth resistance behaviour (Kc_e values) compared to the baseline (air-exposed) values. Furthermore, secondary intergranular crack formation was also revealed in the plastic zone ahead of, and adjacent to, the crack tip of these specimens; which formed during the crack growth resistance loading. It is postulated that the observed degradation of the Kc_e values of the EXCO-exposed material is due to hydrogen embrittlement since the exposure times for the EXCO evaluation were limited to ensure that uniform corrosion dominated; that is, significant penetration of corrosion damage and pitting due to localized corrosive attack did not occur. The sodium chloride-exposed specimens revealed a similar degradation (13%) after 24 hours exposure. However, slight intergranular corrosive attack and isolated pitting were observed on the exposed surfaces prior to crack growth resistance loading, resulting in notch effects that could assist in crack growth. Pitting and intergranular corrosion were, however, not observed at the pre-crack tip. The relative contributions of the notch effects and the hydrogen embrittlement during the degradation of the KR performance are, therefore, unclear.

Apr 1, 2021

By E. Spicer

X-Ray diffraction (XRD) provides useful information about the composition of an ore sample in terms of quantification of crystalline phases and amorphous content. The use of new, fast detection systems in XRD creates the opportunity to use this technique in modern process control. In the analysis of heavy mineral sands, XRD can identify the main mineral phases, such as ilmenite FeTiO3, rutile TiO2, Zircon ZrSiO4and quartz SiO2, and any other minor components present, such as anatase TiO2, magnetite Fe3O4, haematite Fe2O3or monazite (Ce, REE)PO4. Quantitative analysis is possible by various classical methods such as straight line or polynomial calibration with standards, but modern quantification analysis techniques such as Rietveld analysis (Bish and Howard, 1988) are attractive alternatives, as they do not require any standards or monitors. These methods offer impressive accuracy and speed of analysis. The Rietveld method compares calculated versus experimentally derived X-ray powder diffraction patterns for the sum of all crystalline phases. Another analysis technique offering great benefit to mining industries is cluster analysis. Enormous amounts of XRD measurement data are generated during the process control and material evaluation. New ways of handling such vast amounts of data are required to produce meaningful information for the end users. Cluster analysis greatly simplifies the analysis of a large amount of data from different processes or different raw materials, and automatically sorts closely related scans of an experiment into clusters and marks the most representative scan of each cluster as well as outlying patterns. The use of cluster analysis to evaluate the XRD data allows fast and reliable tracking of the process. It is the most economical procedure to have automatic data evaluation without involving any dedicated personnel in the process. Details of the techniques used, sample optimization methodologies, results, data precision and limitations will be discussed. The approach has potential as a relatively inexpensive, reliable tool, useful in the characterization of heavy minerals sand materials.

Jan 1, 2007

By D. J. Briggs

The use of backfill for regional and local support is receiving increasing attention in the South African mining industry. To ensure that fill materials meet the purposes for which they are intended, a test procedure to characterize the load-deformation characteristics for a particular fill was developed. The major variables identified as influencing the load-bearing proper- ties of backfill include particle size distribution, porosity, width-to-height ratio, strain rate, confinement, water content, and additives. The influence of these variables on the performance of backfill is described in relation to crushed waste, dewatered tailings and deslimed tailings. These investigations confirmed that no single test could be used to define the overall stress-strain behaviour of a selected fill. Nevertheless, resulting from this work, a preliminary standard test procedure for uncemented backfill materials, com- prising a suite of tests in unconfined and confined compression, has been formulated. This test procedure is a significant advance towards a more meaningful evaluation of fill materials. Test results will also provide numerical information for input use in computer programs for the design of mine layouts incorporating backfill.

Jan 1, 1988

By C G. Robinson, B. K. Loveday, J. C. Paynter

"A method of optimizing the design of a processing plant has been developed which minimizes capital and operating costs for average stripping ratios and ore characteristics. Models were developed to describe the operating characteristics and costs involved in various operations such as up-grading, leaching and solid-liquid separation.The options available in up-grading policy and the relation between the cut-off grade and the costs incurred subsequently in the treatment of the ore formed the basis of the optimization. To arrive at an optimum plant configuration and a set of operating parameters, the interrelation between grinding size, leaching temperature, leaching time, and various plant recycle options was investigated."

Jan 1, 2014

By C. J. Liebenberg

This paper focuses on the application of ion exchange technology for the recovery of copper from a leach solution originating from a heap bioleach in which base metals are leached from a low-grade ore that bears platinum group metals. Screening tests indicated that Dow XUS43605 has high selectivity for copper over the other metals in the solution, namely nickel, iron, cobalt, zinc, manganese, and aluminium. Batch adsorption kinetic experiments showed that copper adsorption equilibrium is attained at a fast rate. The kinetics of adsorption increased as the temperature was increased from 25°C to 60°C due to the decrease in solution viscosity and the subsequent improved intra-particle mass diffusion. Single-component Langmuir and Freundlich isotherm models were fitted to the batch copper adsorption equilibrium data, and a maximum copper capacity of 26 g/l was observed for Dow XUS43605. The effects of flow rate, temperature, pH, and initial metal concentration on the dynamic recovery of copper were investigated in fixed-bed columns, and it was determined that temperature and flow rate had the most significant impacts on the loading of copper on the resin at copper breakthrough. A 36% increase in copper loading at breakthrough was observed when the temperature was increased from 25°C to 60°C. Finally, it was determined that a split elution is possible by using different concentrations of H2S04 to first elute co-loaded nickel from the resin, followed by the elution of copper.

Jan 1, 2013

By G. Akdogan, C. Bergmann, C. J. Coetzee, Q. G. Reynolds, S. J. Baumgartner

Submerged arc furnaces (SAF) are used extensively in the production of ferrochrome, where charge material – consisting of mixtures of carbonaceous reductants, fluxes such as silica, and ore in the form of pellets – is fed through chutes into the vessel. The feed typically forms a thick bed or ‘burden’ of solid particulates above a bath of molten material below. This burden layer surrounds three electrodes, which are typically arranged in a triangular configuration in circular SAFs. A major challenge in the industry is the availability of sought-after reductants, volatile market conditions, and increasing electricity tariffs in South Africa. A good understanding of the physical properties of the raw materials in the charge is therefore of great value in order to best deal with the reductants available at any given time, and thereby maximising furnace throughput. This paper presents a study of the effects of different particle properties on particle flow behaviour relevant to SAF operations. Discrete element model (DEM) simulations were used to estimate the sensitivity of the particulate flow of beds of charge material to properties such as the coefficients of friction, particle shape and size, and others. The present study lays the groundwork for the development of full DEM models of the SAF that will greatly improve understanding of the flow of complex mixtures of solid particles in the submerged arc furnace, and how the relative physical properties of each component in the charge can influence electrical behaviour of the burden.

Sep 1, 2021

The key functions of project evaluation are to assess potential profitability and to develop an effective operational design. For mining projects, design aspects include mining methodology, ore treatment methodology and production rates. All of these characteristics impact on project economics and overall value. Resource models, which form the ultimate basis of project evaluation, typically consist of tonnes above cut-off, grade above cut-off and the spatial distribution (connectivity) of tonnes/grade above cut-off, for one or more variables. Dilution, ore loss and metallurgical recovery are all modifying factors applied to the resource model during evaluation and determination of profitability. A key issue is: how is the value determined? In addition to traditional combination of in situ tonnes/grade, the following merit serious consideration: the concentration of deleterious elements, throughput rates, mining/processing costs and - importantly - metallurgical recovery. Geometallurgy is an emerging field targeted at integrating these issues by identifying either direct measures or proxies for throughput (hardness, grindability), recovery (liberation, mineral shape/texture, etc) and concentrate quality from easily collected macro-, meso- and microscopic data. These 'geometallurgical variables' drive project costs and revenues in a fundamental way. For geometallurgical characterisation to have a real impact on business design, it must enable improved mine planning. When creating spatial estimates for such variables, it is preferable to find proxies that can be measured as close to the intact rock mass as possible. However, spatial estimation of proxies for geometallurgical properties and responses is complex and requires special consideration. Unlike grades, both proxies and absolute measures of geometallurgical variables are not necessarily linear or additive and therefore require very careful geostatistical consideration. In some cases, models must predict extreme values of geometallurgical attributes rather than averages. Incorrect characterisation of metallurgical recovery/throughput can (and has) led to misspecification of the scale of projects, and thus can be seriously value destructive. Aspects of geometallurgy have long been important in iron, bauxite, manganese and coal deposits and are increasingly on the radar for base and precious metal miners. However, as more metallurgically complex deposits are developed and mining of large-scale, low-grade deposits becomes more commonplace, the importance of characterising the metallurgical response in order to generate properly optimised projects will rapidly increase. It is possible that in many `traditional' (ie grades and tonnes) reserve models, the variables that drive the project are missing!

Jan 1, 2007