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By J. E. Tiffany

"The new permissible blasting device, Cardox, utilizes as a blasting agent liquid carbon dioxide which is discharged.as a gas from a steel container or shell. The loaded shell is placed in a borehole, stemmed, and tamped in a manner similar to that employed with explosives, and is fired by electricity.The Bureau of Mines' approval for use of the device in coal mines was granted as Approval No. 1 under date of October 3, 1928; as the result of tests made under the conditions and requirements of Schedule 20. There have been three subsequent extensions whereby minor modifications in the original design were granted.The permissibility of the device is subject to the following conditions; (1) It shall be in all respects similar to the sample submitted for tests; (2) certain thicknesses of disc and. weights of heater ingredient and of carbon dioxide, all of which are set forth in Table 2 under the provisions governing permissibility, must be used: (3) the rear cap must always be in place after the shell has been charged, to prevent accidental firing; and (4) firing must be done by means of a permissible-type blasting unit.The permissibility of Cardox was established by gallery tests similar to those used in testing explosives for permissibility. In these tests the shell was discharged into gallery 1 without causing any ignition of gas and air or of gas, dust, and air mixtures there. The conditions of charging the shell, such as weight of the ingredients of the heater element, the carbon dioxide charge, and thicknesses of the disc, were varied according to the conditions under which it would be likely to be used in blasting. The tests made in gallery 1 are here described in detail, as are also the tests which have been made for determining the propulsive strength of the device and the quantities of poisonous gases given off when a shell is discharged."

Mar 1, 1929

By A. W. Fahrenwald

Coarse sand flotation, both alone and in conjunction with gravity concentration, is a subject of research at the U. S. Bureau of Mines Field Office, Moscow, Idaho. One of the most important results of this work which is being carried out in cooperation with the University of Idaho, has been the development of a concentration process embodying flotation, classification, and tabling, in the order named. The flow sheet of the process is given in Figure 1. The type of feed desired for this process is coarser than is common in present "all flotation" practice, and is about the size of table feed.

Jan 1, 1929

By A. B. Coates

During the last three years the use of ethylene glycol dinitrate4 (E.G.D.) as at low-freeze (L.F.) agent in place of nitropolyglycerin has become common in the manufacture of explosives of the dynamite type. The usual proportion of D. G. D. in the explosive "oil" is 25 per cent; the remainder, 75 per cant, is regular nitroglycerin. These proportions were probably selected as a continuation of the practice of 25 per cent nitropolyglycerin and 75 per cent regular nitroglycerin.

Jan 1, 1929

By A. W. Fahrenwald

As an aid to studies of grinding, a batch laboratory classifier and elutriator has been developed at the U. S. Bureau of Mines Metallurgical Field Office at Moscow, Idaho, in cooperation with the University of Idaho. It is designed for use in conjunction with other batch laboratory apparatus, such as ball mills and flotation machines. It is shown in Figure 1. Description and Operation of Batch Laboratory Classifier The classifying column is a cylinder 4 feet 2 inches long, of 5 3/4-inch inside diameter, and terminates at its top in a cone or funnel 18 inches in diameter at the overflow elevation. The pressure chamber is of the same diameter as the classifying column, and has a conical bottom; it is provided with two openings, one in the cylindrical portion through which water is admitted, and the other, a small drain hole, in the apex of the conical bottom. The two compartments are bolted together and communicate with each other through the medium of a constriction plate provided with 3/16-inch holes spaced 1/2 inch apart. Constriction plates having any other percentage of opening may be substituted as the needs demand water is admitted to the compartment below the constriction plate at constant pressure. The volume of eater admitted is controlled with a valve. It should be mentioned that the classifying column at the bottom, just above the constriction plate, is glass.

Jan 1, 1929

By H. M. Lawrence

"In the land-pebble district of Florida a lively interest in the possibilities of obtaining increased recoveries of phosphate rock is evident. Research in several directions is being carried on by companies operating in the district to increase the yields obtained by the washing plants. The Bureau of Mines is cooperating with this research program to promote more efficient plant practice and to avoid unnecessary depletion of mineral resources.Washing practice, as carried on in the district at present for the recover of phosphate rock from the crude ores or matrix, is not a complicated process. Flow sheets of the several companies are similar, although the equipment varies with the preferences of the individual operators. For disintegrating the matrix log washers are favored, although revolving drums equipped with flights to break up lumps of clay are also used. Fine sand is removed by screening. Vibrating screens have become well established in the district, although stationary flat screens and trammels are also employed.The writer acknowledges with appreciation the cooperation of the phosphate companies in the land-pebble district; suggestions and criticism by Will. H. Coghill, supervising engineer, Ore Dressing Section of the Bureau of Mines; and the laboratory assistance of J. O. Davie, J. W. Pamplin, and E. Roca, cooperative fellows of the University of Alabama.Losses in the Finer SizesOf the phosphate that is not recovered by present washing methods the greater portion is in the finer sizes. In these sizes the phosphate grains are accompanied by grains of sand - largely quartz - of the same size, and recovery of these phosphate grains as a commercial product is not possible by simple washing methods. Phosphate recoveries approaching complete extraction can only be effecte by applying metallurgical processes, either mechanical or chemical. As yet, most of these processes have not advanced much beyond the laboratory or perhaps the pilot-plant stage. Such processes may have some application to the beneficiation of phosphatic ores or washer rejects, but a discussion of them is not within the scope of this paper."

Apr 1, 1929

By Chas. G. Maier

The bright annealing of copper is an industrial practice of considerable importance. In connection with this process, equilibrium concentrations of carbon monoxide and dioxide, which may exist in contact with copper and cuprous oxide at elevated temperatures, are of interest. Data obtained at the Pacific Experiment Station of the U. S. Bureau of Mines enable estimates of these equilibrium concentrations to be made in two independent ways. Although the publication of final data on one method can not take place until certain further experimental work is accomplished, repeated requests which the Bureau of Minus has had for data relative to the annealing and deoxidation of copper justify the present preliminary report. This paper deals with the calculation of gas concentrations in the reduction of cuprous oxide, using more scientific data which will be published later, and refers especially to those conditions of temperature and concentration of practical implication, and from which critical limits ensue.

Jan 1, 1929

By C. M. Bouton

Although much valuable work has been done in the study of dust explosions, the laboratory technique has not been developed to the point where the many factors involved can be properly controlled, and thus where really fundamental information can be obtained. This paper presents a brief discussion of the difficulties encountered in fundamental work on dust explosions, a description of apparatus intended, to overcome some of them, and an account of some results obtained. FACTORS INVOLVED IN DUST EXPLOSIONS The more important factors pertaining to the dust cloud itself which are known to determine the phenomena of explosions are (1) the kind of dust; (2) its fineness; (3) its concentration in the exploding cloud; and (4) the nature of the interior motions, or turbulence, of the cloud before and during the explosion. These factors are arranged in what seems to be an ascending order of complexity. The kind of dust is the factor most easily subject to control. The fineness of the dust at first sight seems to be a controllable factor, but when it is recalled [that] most explosible dusts are mixtures of particles of continuously varying sizes so small as to pass through the finest woven sieves, and therefore difficult to separate either for purposes of analysis or experiment, the fineness is seen to be a factor difficult to control accurately.

Jan 1, 1929

By H. R. Pierce

Bureau of Mines engineers end others have endeavored to deter-nine a fundamental method for gauging the capacity of gas wells to deliver gas under different pressure conditions. Their studies show that for accurate gauging two factors must be determined: (1) The actual pressures at the face of the sand in the well (usually referred to as "at the sand"), acid (2) the relation between such pressures and the rates. of flow of c as through the sand. This paper, the first of a series, describes a method of attacking the problem of determining the actual pressures at the sand by means of observations of pressures and volumes at the well head.

Jan 1, 1929

By H. R. Pierce

A gas well has a certain definite capacity to deliver gas from the gas sand through the producing string of pipe. This capacity depends upon the pressures in the sand; that is, a well will deliver gas at a rate of flow which is determined by the formation or "shut-inn pressure in the sand and the back pressure at the face of the sand in the well. The three factors, rate of flow, formation or "shut-in" pressure, and the back pressure, for a given well, can be written into a fundamental relation which is strictly applicable only to that well. This relation can be used to determine the capacity of the well to deliver gas from any formation pressure against any back pressure held at the f ace of the sand in the well. Studies have been made of the deliveries of 400 gas wells operating under different conditions of pressure, Most of the wells which have been studied are in Osage County, Okla.; however, several representative studies have been made on wells in southern Louisiana, southern Texas, the Texas Panhandle, and West Virginia.

Jan 1, 1929

By A. M. Gaudin

A study of the consumption of reagents used in flotation gives useful data as to the market which employment of the flotation process creates for the manufacturers of the necessary chemicals and oils, and furnishes a useful clue to the trends in flotation practice influencing the choice of reagents used and the' extent to which new reagents are displacing less suitable older reagents. In the present investigation an attempt has been made to cover both of these phases of the consumption of reagents in flotation. Unfortunately, however, the data collected in tie various districts have not been equally informative; some operators have reported very completely both the consumption of reagents and the metallurgical results obtained therewith, while others were apparently unable to supply these figures in sufficient detail to meet the requirements of this investigation. RESULTS OF INVESTIGATION Table 1 gives the tonnage of ore treated by flotation, as reported. This table shows that flotation has been most largely used in the concentration of copper ores, next in complex lead-zinc ores, followed by lead ores, zinc ores, miscellaneous ores, and copper-iron ores.

Jan 1, 1929

By R. E. Head

At the microscopic laboratory of the Bureau of Mines Intermountain Experiment Station, Salt Lake City, Utah, efforts are being made to devise methods of differentially coloring finely crashed minerals as a means for their identification. Staining would facilitate sight recognition of minerals under the microscope and would be of great value in the study of crushed ores, concentrates, and tailings. Since the treatment of ores for their beneficiation is primarily based on the recovery of the minerals containing the clements of value, it is extremely important that these minerals should be known and that a method for quickly determining them when in minute fragments should be available. Herein lies one of the greatest uses for color methods. In many cases it is a difficult matter for even the trained petrographer and mineralogist to identify finely crushed minerals quickly. Although ordinary petrographic methods are accurate, they are often time--consuming and are not suitable to the needs of millmen who require, especially in the examination of tailings a method for determining minerals by inspection.

Jan 1, 1929

By A. W. Fahrenwald

The purpose of screening is to separate a crushed or natural product into one or more products in which size of grain is constant, or within certain size limits. The ore dresser finds need for this operation in the laboratory, in the study of ore-dressing processes, and for various purposes in the plants. In the plant, for example, screens are employed in closed circuit with crushing devices such as rolls, and sometimes are used in closed circuit with ball mills. Screens are generally used to prepare jig feed where a sized feed is wanted. For any given sieve opening there is in any feed a certain percentage of grains that will pass through the sieve meshes only with difficulty and under favorable conditions. For example, cylindrical grains of length greater than the maximum dimension of the sieve mesh and of diameter less than the sieve opening pass the sieve only when the long axis of the grain is normal or nearly normal to the sieve. Whether such grains should actually be in the through's or the oversize of a screening operation--considered from the point of view of the subsequent treatment of the grains--can not be said. The grains that pass the sieve opening in a screening process only under-favorable conditions have been named "difficult" grains by R. K. Warner.4 In many ore-dressing flow-sheets it probably matters little whether these difficult grains show up in the screen through's or oversize. The main objection to them is that they are sieve-blinding.

Jan 1, 1929

By John D. Sullivan

The present article is one of a series which is being prepared by the Southwest Experiment Station of the United States Bureau of Mines in cooperation with the Department of Mining and Metallurgy, University of Arizona, Tucson, Ariz., of papers dealing with factors involved in the leaching of copper ores. A knowledge of the time required to dissolve the various copper minerals present in ores, as well as of the consumption of leaching reagents is very desirable, because with the decrease of the Nation's total tonnage of sulphide ores increasing attention is being given to the recovery of copper by leaching methods from low-grade disseminated ore containing both oxidized and sulphide minerals. As leaching has already been applied with success and profit, this study was undertaken to determine certain fundamental characteristics that are applicable to all ores suitable for leaching.

Jan 1, 1929

By G. St. J. Perrott

Through the development of manufacturing processes whereby ethylene glycol can be made on a large scale; ethylene glycol dinitrate is now being used in high explosives (dynamites and permissible explosives) by some manufacturers as a low-freezing ingredient of the "explosive oil" instead of such compounds as nitropolyglycerin and nitrosubstitution compounds. The amount of ethylene glycol dinitrate being used constitutes 25 to 50 per cent of the oil. The purpose of this report is to give the results of toots, to determine the effect on the safety and physical properties of permissible explosives of subsituating 25 peg cent of ethylene glycol dinitrate for an equal amount of nitroglycerin or a mixture of nitroglycerin and nitropolglycerin.

Jan 1, 1929

By F. D. DeVaney

An examination of the physical properties of manganese ores is being made at the Mississippi. Valley Station of the United States Bureau of Mines in cooperation with the Missouri School of Mines and Metallurgy, Rolla, Missouri. The object of the study is to find out how much these ores can be beneficiated by such processes as jigging, tabling, magnetic separation, and flotation. Some. of the results were given in an earlier report.4 Eighty samples obtained from various prospects and mines throughout the country have been examined; this is a very small part of those that should be examined before the work can be a definite factor in-the appraisal of manganese ores or the guide in beneficiation which the operators seek. The ore deposits are not expected to reach to great depths vertically, after the manner of copper and gold, but in lateral distribution their greater extent is notable. This applies particularly to the residual and replacement deposits of manganese.

Jan 1, 1929

By W. H. Coghill, B. W. Gandrud, F. D. DeVaney

"The self-fluxing iron ores of Alabama are the foundation of the thriving iron and steel industry of that State. In addition to these deposits of self fluxing ores there are seams containing practically the same percentages of iron but too much silica. These ores at present are valueless, but if they could be concentrated by reducing the silica content, the ore reserves of the Birmingham district would be greatly augmented. A detailed report on the iron-ore deposits of the district, describing the types of ore and their extent, has been published.In forwarding its mineral conservation policies the United States Bureau of Mines has given some attention to the siliceous ores of this district.The low cost of gravity concentration gives this process first rank in the beneficiation of iron ores. For this reason many experimenters have tried to concentrate the Alabama iron ores on tables. In the face of the early failures a new trial has been made and the results have justified the effort.In this work more attention than formerly has been given to the physical, properties of the ores. The removable siliceous gangue is in the form of oolitic grains which ""shell"" out like corn, leaving the hematite as rich high-grade ""slime"" and as clean granular grains. The ""slime concentrate"" may be recovered by well known desliming processes. The oolitic grains and granular hematite are separated on tables."

May 1, 1929

By W. W. Adams

"The results of the fourth annual safety contest, 'mown as the National Safety Competition, contacted by the United States Bureau of Mines are herein announced. A bronze trophy, ‘Sentinels of Safety’, the gift of the Explosives Engineer magazine, has been awarded to the leading mine in each of the five groups into which the mines and quarries that participated in the contest were arranged. These five groups were: anthracite mines, bituminous coal mines, metal mines, nonmetallic-mineral mines, and carries and open-pit mines. The leading plant in each group was the mine whose employee lost the smallest number of days from accidents in proportion to the total number of man hours worked. Where two or more mines operated without a lost-time accident, the winner was adjudged to be the plant which operated the largest number of man hours during the year.The contest was based upon reports of accidents and exposure sent by the competing companies to the Bureau of Mines. Records of the five leading companies in each group were made known to a Committee of Award, consisting of the following seven members: H. Poster Bain, Secretary of the American Institute of Mining and Metallurgical Engineers; James F. Callbreath, Secretary of the American Mining Congress; W. H. Cameron, Managing Director of the National Safety Council; H. L. Gandy, Secretary of the National Coal Association; A. T. Goldbeck, Director of the Engineering Bureau of the National Crushed Stone Association; William Green, President of the American Federation of Labor; and A. J. R. Curtis, Assistant to the General Manager of the Portland Cement Association. Members of the committee voted for the winning company in each group in accordance with the rules governing the contest.. A majority vote prevailed."

May 1, 1929

By S. P. Kinney

The efficient operation of a blast furnace is primarily dependent upon efficient contact between the descending stream of solid materials and the ascending stream of gas. The United States Bureau of dines is conducting a program of research dealing with the interior of the present-day furnace. The work is being carried oat by.(1) observations on commercial furnaces end (2) experiments in the laboratory. Through the courtesy of the officials of the Illinois Steel Co. it was possible to make a detailed investigation of the interior of the shaft of Number.4 furnace at the company's South Works, South Chicago, Ill. The experimental work is to be reported in a U. S. Bureau of Mines bulletin which will include the results of several thousand observations on the interior of the shaft of this furnace. Such of the data as are presented later in this paper constitute only a brief summary.

Jan 1, 1929

By A. B. Coates, J. E. Crawshaw

"The use of such methods and apparatus as the Dautriche method and the Mettegang recorder for the determination of the rate of burning of black blasting powder and other strictly burning explosives has been found to give such erratic results that no reliance can be placed on the data thus obtained. Consequently, investigators of those factors which may affect the burning rate, such as size of grain, absolute density, chemical composition, and means of ignition have had to rely mainly on observations made during practical use for determination of the part played by each. Such tests are very difficult of interpretation.The purpose of this paper is to describe a method used by the explosives division of the Bureau of Mines for the investigation of such explosives and to present the results of an investigation using that method.The investigation was concerned with the effect of grain size, initial pressure, and means of ignition on the rate of burning or rate of pressure development of black blasting powder as compared with pellet powder.The Bichel pressure gauge was used for these tests, with the slight modification to the apparatus and method described in U. S. Bureau of Mines Bulletin 15.4 These modifications consisted of reducing the speed of the revolving drum on which the time-pressure record is taken, measuring the speed of the drum by a belt-driven tachometer, and introducing an induction coil in series with the electric squib or electric detonator to mark on the time pressure record the instant at which the squib or detonator was fired."

May 1, 1929

By T. W. Johnson

The Bureau of Mines, in cooperation with the Natural Gas Department of the American Gas Association, has in progress a study or the flow of natural gas through high-pressure transmission lines. A major problem of this study is to compare the deliveries calculated from the gas pipe-line flow formulas commonly used, with the metered deliveries from pipe lines in operation. In order to obtain such comparisons a series of tests has bean made on 25 operating pipe lines in Kansas, Oklahoma, Louisiana, Arkansas, Texas, and California ACKNOWLEDGEMENTS Study of the flow of natural gas through high-pressure transmission lines was made under the general supervision of H. H. Hill, former chief petroleum engineer of the Bureau of. Mines, H. C. Fowler, acting chief petroleum engineer of the Bureau of Mines, N. A. C. Smith, superintendent of the Bureau of Mines Petroleum Experiment Station at Bartlesville, Okla., and T. Brandenthaler, chief of the oil and gas action of the Bartlesville station.

Jan 1, 1929