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By G. L. Neumann

The Andover-Sulphur Hill iron mines in Sussex County, N. J., have a production record extending over 100 years. The last production recorded was about 1880. These mines produced high-grade ore of two types: Bed ore (hematite) and blue ore (magnetite. Some sulfides (lead, zinc, and copper) were found underlying the iron deposits. Data as to size and grade of these sulfide bodies are very sketchy, Toward. J. Hewitt of Elizabeth, N. J., lessee of the Sulphur Hill mines from 194045, prospected for lead, zinc, and copper. .His Only production was several hundred tons of low-grade iron ore, which was crushed and used as heavy aggregate to make concrete blocks for ship ballast. In October and November 1942 made a magnetic survey of this area and bored six-diamond-drill holes with the dual objective of prospecting for sulfides and testing for extensions of the iron-ore deposits indicated by the magnetic survey. In 1944, an iron-mining company examined this property and diamond-drilled seven holes Between December 1949 and March 1950, the Bureau Of Mines in search of sulfide deposits, bored three additional diamond-drill holes. Two of these were on the Sulphur Hill tract and one on the adjoining Tar Hill tract.

Jan 1, 1952

By J. W. Holcomb

Many mines are opened into the coal beds by shafts; and, at some of these operations, the same cages or skips that are used for hoisting coal also are used for transporting men into and out of the mines. At some mines, separate man-and-material shafts are maintained, and the cages in these are utilized for transporting men and supplies only. In most instances, these cages are operated either singly or in pairs by a hoisting engine installed in a building near the shaft. Single ropes from the tops of the cages pass over bull wheels on the head frame to either electrically or steam-driven hoisting engines that require engineers to operate them. There are records of several instances where hoisting engineers have become incapacitated suddenly while hoisting men, and the passengers on the cages were killed or injured. Where the same cages are used for hoisting cars of coal and for lowering and hoisting men, especially where self-dumping cages or skips are used, safety pre¬cautions must be taken, such as providing steel bonnets for the cage deck, enclosed sides, adequate handholds, gates for closing the end openings, safety catches, and locking devices to prevent accidental dumping. Some of the newer hoisting installations are of the elevator type; where an operator rides in the cage in the same manner as an elevator operator in a building. These cages have single or multiple decks and are primarily for transporting men; but, in some instances, supplies also are transported. They are a great improvement over the installations where the same cages are used for hoisting cars of coal and transporting men.

Jan 1, 1952

By L. W. Kelly

The primary purpose of this paper is to show the appreciable savings that were made by roof-bolting the main west entry of the Kings mine, which was to be the permanent, main haulage road, as compared to the cost of supporting the same roof with peg timbering as first planned. Additional items that might prove valuable to other mine operators are contained in this paper and detailed below. 1. A detailed cost of the system of roof support known locally as the peg-timbering method is given. It consists fundamentally of supporting steel cross bars on pegs inserted into holes drilled in the ribs close to the roof. 2. A method of supporting the roof in caved entries is shown, where such support must endure for an extended period in haulageways and air courses.

Jan 1, 1952

By J. B. Zadra

The use of activated carbon for extracting gold and silver from pregnant cyanide solution and pulp has been investigated many times. The primary advantage of this use of activated carbon is that .the dissolved values can be recovered from slimy ore pulps or from slime portions of ore without settling and thickening or filtering. The loaded carbon is removed from the barren pulp, and the pulp can then be discarded. Activated carbon has been used recently in treating gold ores containing very little soluble silver. When the carbon was loaded with a suitable amount of gold, the silver load was negligible. The remaining problems concerned the removal of the gold from the carbon, the recovery of the gold as bullion, and the reuse of the unloaded carbon. As described in a recent report, a method that solved these problems was developed. The gold-laden carbon was leached with caustic sodium sulfide solution and the gold simultaneously recovered by electrolysis. Both the carbon and the spent solution can be reused. That process was applicable to gold-laden carbon only. It was not applicable to carbon carrying silver, because sodium sulfide does not leach silver from carbon but "fixes" it. It has been necessary, therefore, to develop a modified process for the removal or desorption of both gold and silver from loaded carbon. This modi¬fied process permits the use of activated carbon for extracting both gold and silver from gold ores carrying enough silver to have economical interest or in which silver may be the predominating value.

Jan 1, 1952

By Louis A. Panek

An improved centrifugal-testing apparatus has been designed and built in the Bureau of Mines laboratory at College Park, Md., which is unique in that it incorporates the use of resistance gages to measure directly the strains in a rotating model without testing it to failure. Owing to this feature, a more rapid testing method can be used; furthermore, model materials need not be restricted to those of the prototype. The behavior of any structure in which strains of significant magnitude are produced by its own weight may be studied in a small model subjected to simulated gravity loading. The model is rotated in a centrifuge to induce in it centrifugal forces, which, like the gravitational forces in the full-size structure, act on the volume elements and are proportional to the masses thereof. Centrifugal testing is, therefore, applicable to the design of mine openings and to the study of similar ground-control problems. It constitutes an experimental method for determining the state of strain in a structure for which analytical methods are excessively laborious or even impossible. In previous applications of centrifugal testing by other investigators, the models usually were tested to failure, and the analysis was made from-the type of break produced. The models were made of the same materials as the proto-type, and the test results were applied only to the particular prototype represented by the model. Beam deflections were measured from photographs of the rotating model, but no means was employed either to determine the actual distribution of stress in the model or to determine quantitatively the degree of restraint imposed on the ends of the loaded model beam, that is, to determine whether the loaded model behaved as a beam with rigidly fixed ends or as some other type of beam. With the apparatus described, it is possible to determine the state of strain, and thus the boundary conditions, in a rotating test model weighing up to 90 lb., which can be subjected to centrifugal forces up to about 2,600 times the force of gravity. The load-strain relationship, applicable directly to the prototype, can be determined from a Single model test. The test results can be presented as quantitative relations between the loads, strains, and dimensions and mechanical proper-ties of the structural members and can be applied to any prototype, whatever its component materials, that satisfies the similarity requirements.

Jan 1, 1952

By John B. Gayle

The Bureau of Mines has designed and constructed an experimental coke oven, using a commercial oven as a model where practicable. Because the rate of carbonization is important in determining the quality of the coke produced and may affect the "mount of pressure developed during carbonization, particular attention was given to those elements of the design that govern the heat transfer to the charge. The new oven deviates in design from most existing test ovens in that the charge is full width (17 inches), the heating walls ore constructed of 4-1/2-inch silica brick, and zoned, heat-input arrangements compensate for heat losses at the ends, top, and bottom of the charge. This report describes the oven, which was designed by H. S. Auvil and installed under his direction, at the Southern Experiment Station, Tuscaloosa, Ala., while he was supervising, engineer, Coke Section. It gives the results of a limited number of carbonizing tests. These results indicate that the main objective in designing and building this oven, that off duplicating commerical, slot-oven carbonizing conditions, has been accomplished; if coke-discharge conditions simulate commercial-oven conditions, the cokes from the experimental oven arc very similar to oven coke, in soma tests being fully as close is duplicate tests from a Angle batch of coke.

Jan 1, 1952

By D. S. Colby

The productive capacity of natural-gasoline and cycle plants in the United States as of January 1, 1952 was 811,596 barrels per day, an increase of 163,691 barrels per day since the last survey on January 1, 1950. The rate of growth during these 2 years has been 12 percent per year s only slightly below the maximum rate, recorded from 1948-50. This survey, for the first time, presents capacity data on a barrel rather than a gallon basis. Also, for the first time, a break-down of capacity by products has been obtained. The combined LP-gas producing capacity of plants and fractionators equaled 382,790 barrels per day, 47 percent of the total industry capacity tor all products. During January 1952, LP-gas and natural gasoline and other products were each produced at the rate of 76 percent of the January 1 capacity.

Jan 1, 1952

By J. D. Davis

THIS report gives results of an investigation of the carbonizing properties of the following eastern Kentucky coals: Elkhorn No. I bed, No. 28 mine, Wayland, Floyd County; Elkhorn No. 2 bed, Turner No. 5 mine, Drift, Flood County; Leatherwood (Haddix No. 5) bed, Leatherwood mine, Leatherwood. Perry County; and Harlan bed, Path Fork mine, Path Fork, Harlan County. The carbonizing properties were determined by Bureau of Mines-American Gas Association (BM-AGA) tests at 800° and 900° C. and by expansion tests in the sole-heated oven. Plastic properties were determined by tests in the Gieseler and Davis plastometers. The coals were tested singly and as blends with 20- and 30-percent low-volatile Pocahontas No. 3 coal. The dry, mineral-matter-free, fixed-carbon content of the carbonizing samples ranged from 56.7 percent for Elkhorn No. 2 to 59.7 percent for Leatherwood, and the heating values on the moist, mineral-matter-free basis ranged from 14,420 B. t. u. per pound for Elkhorn No. 2 to 14,720 for Harlan. The percentage of ash ranged from 2.9 to 6.1. The fluidity of three coals, measurer. In the Gieseler plastometer, ranged from 230 to 670 dial divisions; the fluidity of Elkhorn No. 2 could not be determined by this method. Blending lowered the fluidity of each coal; the fluidity of the blends containing 20 and 30 percent Pocahontas No. 3 ranged from 16 to 53 and from 8 to 17 dial divisions, respectively. Agglutinating values determined on silicon carbide-coal mixtures in the ratio 15:1 ranged from 3.8 to 6.3.

Jan 1, 1952

By James J. Dowd

The investigation to evaluate the reserves of coking coal in the United States suitable for the manufacture of metallurgical coke is being made by the Bureau of Mines in three parts: (1) To estimate known measured and indicated recoverable reserves of all coking coal; (2) to upgrade marginal coals through effective preparation; and (3) to study the carbonizing properties of coals and coal blends not now widely used for metallurgical coke making. This is the eighth of a series of reports giving the results of studies by counties under part (1) of the investigation. (See appendix.) This report covers Jefferson County, Pa., which comprises parts of Marienville, Hallton, Ridgway, Brookville, DuBois, Penfield, Smicksburg, and Punxsutawney quadrangles. (See fig. 1.) A short resume of the chemical and carbonizing properties of the coals is included. Data on the coal beds in the county were obtained from mining companies, land companies, individual landowners, and other sources of authentic information. A base map for each bed in each quadrangle was made to the scale 1 inch equals 1,200 feet. Maps of mines, locations of drill holes, bed and total coal thicknesses, and the outcrop of the bed were plotted on the maps. With all available data plotted, isopach lines were drawn to limit areas of known unmined reserves in beds 0 to 14 inches thick, 14 to 28 inches thick, 28 to 42 inches thick, and over 42 inches thick, These areas of coal reserves also were divided into "measured" and "indicated" categories. All areas in each thickness range and in each category, mined-out areas, areas excluded from the estimate, and areas outside of the outcrop were measured by planimeter on the base maps. Estimates of total reserves 14 inches and more thick and maps for individual beds were prepared from these data.

Jan 1, 1952

By Jr. Sayre

Results of studies of reservoir and wax-precipitation temperatures relating to wax deposition in the reservoir of the Bradford oil field are presented in this report. During 1949 and 1950 Bureau of Mines engineers made temperature measurements in 42 wells, which indicate that the Bradford Third-sand temperatures range from 59.7° F., at 1,150 feet, to 71.9° F., at 2,040 feet. Reservoir temperatures measured at the same depths in newly drilled wells and oil-producing wells differed as much as 4.5u F. Injection-well temperatures measured during water injection showed that the temperature of the water entering the sand was 11.5° F. lower than reservoir temperatures before injection. The cooling in the formation resulting froth the injection of low-temperature water was 11.5° F. in the vicinity of the injection-well bore, and a maximum of 2.1° F. 200 feet from the injection well. Sand temperature, after 5 months of water injection, was reduced 1.5° F. 90 feet from water-injection wells. The temperature at which wax begins to precipitate from solution in crude oil was determined at atmospheric pressure for 26 samples and ranged from 51° to 67° F. Oil samples from wells producing no water had wax-precipitation temperatures ranging from 51° to 58° F. and wax contents from 2.20 to 2.97 weight percent, whereas the samples from wells producing water and oil had wax precipitation temperatures ranging from 580 to 67° F. and wax contents from 2.57 to 3.42 weight percent .

Jan 1, 1952

By John A. Ruppert

1. It has been proposed that the addition of enough limestone to an open -hearth s lag to give a CaO-3P2O5 ratio of approximately 2-followed by SiO2 firing in an oxidizing atmosphere under the proper conditions of time and temperature will result in a clinker having a magnetic phase containing a preponderance of Mn, Fe, Al, and Mg as oxides and a nonmagnetic phase consisting for the most part of a phosphorus-containing dicalcium silicate. It has been postulated further that the metal oxide phase can be recovered by fine grinding and magnetic separation. These broad principles have been substantiated by numerous clinkering operations made in an electrically fired studio-type kiln, a batch rotary kiln, and a continuous rotary kiln and by magnetic separations made in a Davis -tube separator and a laboratory-size Jeffrey-Steffensen three -roll continuous separator. 2. Quenching the clinker after firing seems to improve its grindability. Microscopic examination of the ground clinker indicates .that the oxide phase grinds down at a somewhat faster rate than the silicate phase. 3. Very fine grinding is necessary to approach liberation, of the oxide phase from the silicate phase. Grinding to ininus-325-mesh, followed by magnetic separation, gave only a rougher concentrate, which had to be reground before final separation. 4. Although the manganese content of the final concentrate was higher, there was some evidence that manganese recovery was lower from a clinker made from a flush s lag than one made from a mixture of tap and flush slags. A possible explanation is that a clinker made from a mixture of slags has a higher iron content and hence is more magnetic and more easily separated.

Jan 1, 1952

By Irving Hartmann

When permissible explosives are used in coal mines according to the procedure recommended by the Bureau of Mines they are relatively safe, and no mine explosions are known to have resulted from this type of blasting. However, unsafe blasting practices - the use of nonpermissible explosives or the improper use of permissible explosives - have caused many serious disasters. In fact, such unsafe practices constitute the third most important cause (exceeded only by electricity and the use of open lights and smoking) of coal-mine explosions in the United States. During 1929-1947, inclusive, 81 explosions, resulting in 475 fatalities, were ascribed to unsafe blasting. The hazards of black powder, dynamite, and other nonpermissible explosives in coal mines have been recognized for many years, and attention has been called to this in numerous Bureau of Mines publications. Not only can these explosives ignite namable gas-air mixtures readily, but they can also ignite coal dust, as has been illustrated repeatedly in tests and at educational public demonstrations at Bruceton and elsewhere.

Jan 1, 1952

By N. E. Hanna

To be authorized for use in coal mines, explosives and blasting devices must pass certain safety tests prescribed in schedule 1F,3/ on the basis of extensive practical and theoretical research by the Explosives Testing Station of the Federal Bureau of Mines. An explosive or blasting device that passes these tests is placed on the active permissible list. As this list is constantly revised, it has been the practice of the Bureau of Mines periodically to publish the names of explosives and blasting devices that have been added to the active list, as well as those that have been transferred to the inactive list; changes in brand names also are reported. This circular covers all permissibles including additions, transfers, and changes made between December 31, 1945,4/ and December 31, 1951.

Jan 1, 1952

By R. J. Hundhausen

The Shamrock copper-nickel mine in Jackson County, Oreg., was formerly a part of the Chisholm mercury property. In 1948 new owners advanced the old workings 40 feet to reveal encouraging widths of copper-nickel sulfide, ore on the Shamrock claim. When the owner's funds became exhausted, the Bureau of Mines carried on the development in 1949-50, completing 1,650 feet of bulldozing trenching, 396 feet of drifting, and 3,419 feet of diamond drilling. The Bureau's trenching disclosed a separate surface deposit 600 feet south of the mine deposit. This and the previously known deposit subsequently were diamond-drilled. The underground deposit has a known length of 100 feet, a dip length of. 100 feet and a width varying from 1 to 25 feet. The surface deposit is 200 feet long, 200 feet deep, and 5 to 38 feet wide. Neither deposit has been entirely delimited by development to date.

Jan 1, 1952

[1.1. The provisions of this code are minimum provisions and are designed to minimize hazards to life and property in and about underground coal mines where electrical equipment and circuits installed used. They indicate the Steps necessary in the selection, installation, operation, inspection, and maintenance of electrical equipment and circuits to obtain proper safeguards in reducing electric shock, fire, explosion and other hazards. Surface as well as underground installations were considered in formulating the code and, unless otherwise stated, each provision applies equal to both underground and surface installations. This code does not apply to buildings and installations not directly connected with mining operations, nor does apply to strip-mining operations.]

Jan 1, 1952

By R. F. Stevens

A laboratory method for examining crude shale oil is described. The method uses only about 500 ml. of sample and a limited number of analytical determinations. Results provide information on the general characteristics and composition of an oil and serve as a basis for comparing different oils. However, the method does not provide for direct estimates of yields of commercial products. Analyses of 10 oils produced in the United States by different methods of retorting and of 10 shale oils from commercial-scale operations in 6 foreign countries are given. The shale-oil-analysis method presented in this paper is based on and employs the same equipment as the Bureau of Mines routine method for analyzing crude petroleum. As shale oil contains groups of compounds not generally found in petroleum, several modifications of the petroleum method that might increase its suitability for application to shale oil were investigated. The modifications included in the present method take into account the apparent poor heat stability of shale oil and the presence of large quantities of olefins and nitrogen compounds.

Jan 1, 1952

By Arnold B. Hubbard

This report describes a method of concentrating the insoluble organic material (kerogen) in a rich Colorado oil shale without any apparent alteration of its original chemical form. The method involved treating finely pulverized shale with dilute acetic acid at room temperature to remove the carbonates, which act as a cementing agent for the shale, and cause the shale particles to partly disintegrate into the organic and inorganic components. The acid-treated shale then was centrifuged in different liquid mediums ranging from 1.4 to 1.15 gravity to effect a mechanical separation. From a Colorado oil shale containing 48.0 percent ash, kerogen concentrates containing 43.3 to 8.7 percent ash were obtained. The carbon:hydrogen ratios of the kerogen in the original shale and the different concentrates were essentially the same. The oil:kerogen ratios calculated from Fischer assays of the above samples were essentially the same, regardless of the organic or inorganic contents. This was also true of the assay water:kerogen ratios of the same samples. These data indicate that no significant change occurred in the kerogen during the concentration process.

Jan 1, 1952

By Joseph J. Wallace

1. The Investigation shows that there are six coal beds of major importance in McDowell County from the standpoint of present production - Pocahontas No. 3, Pocahontas No. 4, Pocahontas No. 5, Sewall, Beckley, and Pochontas No. 6 - and five beds of minor importance - Iaeger, Douglas, Welch, Pocahontas, No. 9, and Eagle. The Pocahontas No. 3 bed contains the largest remaining, known reserves. 2. Known measured, and indicated reserves in all beds, based on a minimum thickness of 174 inches and on 1,800 tons per acre-foot of coal in place, are estimated at 2,217 Trillion short tons as of January 1, 1951. Of this total, 1,731 million short tons are in beds 28 inches and more thick. Areas in each bed were omitted from the estimate because available data relative to the bed characteristics are too meager to make an estimate that conforms with the definitions of measured and indicated coal adopted for this study. Should future drilling or development prove reserves in these area, such reserves should be added to he total estimated reserves.

Jan 1, 1952

By Peter H. Toepfer

Hydraulically emplaced, classified mill sands long have been used for stope fill. Entrained water drains rapidly from this type of fill through openings between the sand grains. Slimes are removed to facilitate drainage of the water, thereby lowering dangerous hydrostatic pressures in the fill. Use of unclassified mill tailing as practiced at the Dayrock mine is a recent development and represents a fundamentally different approach to the problems of inhibiting the development of hydrostatic pressures within the stope fill. At the. Dayrock mine, mill tailing is used to form a densely packed fill of sand and slime particles relatively impervious to additional water.

Jan 1, 1952

By Oliver Bowles

Manufacture of lime is one of the oldest industries. Plants are distributed widely and furnish an essential raw material for numerous commodities. Use of lime in hundreds of manufacturing and chemical processes, by the building trades, and in agriculture has created a demand for large production and has necessitated exhaustive research on methods of manufacture and uses. The bibliography of publications on lime is extensive; but, for the most part, each publication has dealt with individual operations. The purpose of this paper is to present a general picture of the industry as a whole. The abundant literature has been abstracted and quoted freely, and the National Lime Association has furnished valuable data for certain sections. Publications containing more-detailed information on the various branches of the industry are referred to in the footnotes and bibliography.

Jan 1, 1952