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By J. E. Hamak

This publication contains analyses and related source data for 144 natural gas samples from 19 States. Of the total samples, 139 were collected during calendar year 1990. The remainder were collected earlier, but releases granting permission to publish were not received until 1990. All samples were obtained and analyzed as part of the U.S. Bureau of Mines investigations of the occurrences of helium in natural gases of countries with free-market economies. This survey has been conducted since 1917. The analyses were made by mass spectrometer and chromatograph.

Jan 1, 1991

To separate complex mineral mixtures according to their dielectric properties. Approach Develop a laboratory-scale continuous dielectric separator to separate mineral mixtures by exploiting their difference in dielectric properties. How it Works Dielectric separation is de-fined as the separation of particles based on their dielectric properties. The uniqueness of the Bureau's continuous separator, called the ?Rotating Drum Dielectric Separator,? is that it contains a high-voltage electrode con-figuration. The drum electrode consists of a series of coaxial parallel wires mounted on the outside surface of an Insulated cylinder. The screen electrode Is a wire mesh, quarter cylinder positioned outside and coaxially with the drum electrode. The drum electrode is placed in a liquid of dielectric constant K with the liquid level just above the drum's axis. The screen electrode is completely Immersed

Jan 1, 1981

By G. D. Coe

Float-and-sink tests indicate what results are obtainable by gravity separation and rare therefore an invaluable adjunct to most coal-cleaning processes. However, it is difficult to make a direct interpretation of float-and-sink data on coal, and several systems for interpreting them have been proposed. Of these, that developed and used extensively by Bird3/, Yancey4/, and Gandrud5/ is considered by the author to be the most satisfactory. It makes use of four interrelated curves (hereafter referred to as be "washability curves"). These curves were explained by Bird in a paper6/ published in 1923, but his explanation has been regarded by some as not sufficiently

Jan 1, 1938

By V. A. Marple, K. L. Rubow

"IntroductionA particle dispersion system has been developed to aerosolize bulk powders or material deposited on surfaces such as filters. The size distribution of the aerosolized particles can then be obtained by sampling the particles with an aerosol sizing instrument such as a TSI aerodynamic particle sizer (APS) or a cascade impactor.Of particular interest is the applicability of using this technique to obtain the size distribution of particles collected on filters. This system has been used to determine the size distribution of coal dust particle collected on membrane filters. The use of this device in this application is quite intriguing in that, if this technique can be shown to accurately determine the size distribution of airborne particles, one can easily collect particle samples using either personal or area particle samplers, determine the mass concentration of the collected material through gravimetric techniques and then use the particle dispersion system coupled with the APS to determine the particle size distribution. With this technique one can determine the particle size of dust in environments, such as underground mines, where it would be inconvenient or impossible to use a particle sizing instrument.Particle Dispersion SystemA prototype particle dispersion system has been developed for aerosolizing particles. A schematic diagram of the system is shown in Figure 1. The system consists of mechanism for advancing the particle sample beneath a dust pickup tube, a venturi for deagglomerating the particles, and a instrument for analyzing the aerosolized particulate matter.The procedure to analyze a particle sample is as follows. The particles to be aerosolized are placed on a sample plate from where the particles are picked up by an air stream flowing upward in a small capillary tube (dust pickup tube). This tube operates as a small vacuum cleaner passing over the sample plate. The air is drawn up the capillary tube at a rate of 2 L/m by a venturi aspirator. This is accomplished by placing the outlet of the capillary tube near the throat of the venturi. The accelerated velocity of the air creates a low pressure in this region which draws flow up the capillary tube. From the outlet of the capillary tube particles are transported to the inlet of the APS where a small fraction are sampled and the aerodynamic diameter of the particles determined. The particles which are not measured by the APS are passed into a HEPA filter."

Mar 1, 1989

By David C. Oyler, Paul B. Stubbs

The Bureau of Mines and United States Steel Corp. are conducting a joint project to monitor formation pressures at a large (23-well) coal- bed gas drainage field near Oak Grove, AL. Three monitor holes were drilled in late 1981, and pressure monitoring began in December 1981. The Bureau of Mines direct method was used to obtain gas content data from cores taken in the monitor holes. Comparison of the 1981 gas con- tent data from the monitor holes with initial gas content values obtain- ed from the production wells in 1977 indicates a 50-pct reduction in ad- sorbed gas content inside the pattern and a 29-pct reduction at one point 500 ft outside the pattern. The combination of pressure and gas content data has also allowed an in situ isotherm curve, relating the formation pressure to adsorbed gas content, to be developed for the area of the production wells. From the current rate of pressure decline (1 lbf/inz per month), the observed changes in gas content, and the isotherm curve, it appears that most of the early gas production came from within the pattern, but since 1981 (and possibly earlier) most of the gas produced has been migrating to the wells from outside the pattern area.

Jan 1, 1985

Until man was able to produce light, his working day was pretty much limited to daylight hours. Underground miners have a special problem because in a mine it is just as dark during daytime as it is at night. The first devices used for mine lighting were torches and open flame 011 lamps. Torches made from twisted grass and dipped in tallow or pine pitch would burn for a while, but they made a lot of smoke and probably went out when they were needed most. During the 15001s, miners lamps consisted of a small metal dish with a hook attached to hang it up. The saucer-shaped dish was filled with animal or fish oil and a wick made of twisted fibers was laid In the 011 and hung over one edge where it would burn. This lamp would burn longer than a torch, but the amount of light cast by the pale, flickering flame was probably only a little better than no light at all.

Jan 1, 1976

By Charles W. Huggins

DEVELOPMENT of the electron microscope has permitted man to examine many small objects that could not be resolved by the light micro-scope. Diffraction, spherical aberration, and chromatic aberration are the main factors that limit resolution to about two-tenths micron with the light microscope. No matter how perfectly a light microscope is constructed and operated, it cannot possibly resolve points separated by less than two-tenths micron. Rapid development following World War II has produced many electron microscopes capable of 20 A resolution. Fibrous inorganic minerals are well suited for electron microscopic study. Many micrographs of chrysotile have been published, but electron microscopic study of the amphiboles has been somewhat neglected. New techniques in sample preparation have simplified the study of fibrous material. Ultrasonic energy has been very helpful in sample dispersion. This publication contains a representative group of electron micrographs of natural inorganic fibers that have industrial value. These fibers commonly are referred to as the asbestiform minerals. The Bureau hopes that the knowledge gained through electron microscopy and other scientific study of the natural inorganic crystalline fibers eventually will lead to the production of synthetic fibers that will satisfy the requirements of industry.

Jan 1, 1959

By W. A. Haley

This is the second of a series of publications that describes the progress of mechanical longwall coal mining in the United States in which a German coal planer was employed.3/ Details of the equipment, a description of its operation, and the results obtained in mining the experimental panel were published in the preceding report. Experimental mining with the planer in the first panel showed an improvement in performance over conventional mining methods at the coal company's Stotesbury 11 mine. The work, which was begun on an experimental basis, soon proved successful, and the coal company purchased the equipment for continued use. Two panels, adjacent to the first, were developed and mined with the planer. Each of these panels was shorter than the preceding one because water seepage from a surface creek limited development. On completion of mining in the third panel, the planer equipment was moved by the cooperating company to a nearby mine operated in the same coal bed where a large area of coal suitable for planer mining is available.

Jan 1, 1954

By Benjamin W. Haynes

As part of the first-order assessment of potential manganese nodule processing reject waste materials, the Bureau of Mines estimated the physical and chemical characteristics of reject waste materials that would be generated from each of five potential process flowsheets. These processes were chosen because of their economic and technical feasibility for first-generation nodule processing. A brief description of the five processes is given to show process inputs and outputs, The physical characteristics are predicted based on land-based laterite processing where applicable, and where no land-based analog exists, on the basis of process chemistry. The probable chemical characteristics such as element content and compound form are tabulated for each process for 16 elements: As, Ba, Be, Cd, Go, Cr, Cu, Fe, Mn, Mo, Ni, Pb, Sb, Se, TI, and Zn. These elements were chosen based on their presence on the toxic substance list of priority pollutants, EP toxicity criteria, and major and minor elements of economic importance (Co, Fe, Mn, and Mo). Physical and chemical analyses as well as results of the EP toxicity test of one industrially supplied pilot plant reject waste material are presented.

Jan 1, 1982

By J. Koster

During the past several years, alunite from the Marysvale (Utah) region has been the subject of investigation by the Electrometallurgical Section of the Bureau of Mines. The nature and occurrence of this mineral, with considerable data on the Utah deposits, together with a number of results of preliminary experiments, have been given in a previous report.6/ The geology of the Marysvale region has been reviewed recently.7/ The present paper reports the results obtained by a method involving the sintering of alunite with boric acid and subsequent treatment of the sinter to produce alumina and potassium sulphate.

Jan 1, 1939

By H. G. Skavlem

This paper is prepared the United States Bureau of Mines and is descriptive of methods, practice, and costs at the McIntyre Porcupine Mines, Ltd., Schumacher, Ontario. The property is located in the Pearl Lake section of the Porcupine mining district. It is reached by a branch line of the Temiskaming & Northern Ontario Railway from Porquois Junction. There is also a good motor road into the district. The Hollinger Consolidated Gold Mines and the Coniaurum Mines, Ltd., are adjacent properties. Power for both the mining and the pulp and paper industries in the district is supplied by an extensive development of the water-power resources. Weather conditions are favorable for mining operations.

Jan 1, 1933

By F. E. Griffith, C. H. SEELING

Cardox blasting is used widely in coal mines in the United States . A model of a Cardox blasting device was approved by the Bureau of Mines subject to certain conditions and limitations , and the approval was extended to other models from time to time . Certain special hazards are entailed in the use of Cardox as with explosives . One of these is flying shells . In some blasts , the Cardox shell is violently ejected from the borehole and flies like a projectile , frequently ricocheting off solid objects and striking points considerably off the line of its initial flight . Flying shells have been known to pierce the webs of structural - steel beams , to pass through both sides of allsteel mine cars , to be driven through stout hardwood timbers , to knock out timber sets , to damage loading equipment , and to break or short - circuit power lines . A considerable number of shot - firers and other workers have been struck by flying shells and killed or injured . Accidents from this cause , although not as frequent as other types of mine accidents , are usually serious , closely approximating accidents caused by blasting with ordinary explosives . The increasing number of such accidents prompted a Bureau of Mines field investigation of possible methods of preventing dangerously violent ejections of Cardox devices . This report contains pertinent data collected during the investigation and describes methods tested and discarded as well as the development and proof of an apparently satisfactory method .

Jun 1, 1943

By E. B. Swanson

Atlantic seaboard refining and marketing companies , dependent largely upon other producing and refining areas for the crude and refined petroleum needed to meet the demand for petroleum products within the Atlantic Coast States , reported an increase in 1929 receipts of 2,542,000 barrels of crude petroleum and 13,479,000 barrels of gasoline over the quantities received during the preceding year . The relatively large expansion in gasoline receipts undoubtedly resulted from the unexpected increase in gasoline consumption which characterized the petroleum industry during 1929. Gasoline receipts from California increased 6,354,000 barrels and shipments from foreign countries were 5,381,000 barrels in excess of the 1928 figures , while receipts from Gulf Coast ports , the major source of outside supply, declined 811,000 barrels . Shipments of domestic crude oil by tanker from Gulf Coast ports during 1929 continued the average annual increase of approximately 7,000,000 barrels which has been recorded during the five years of this annual survey . These shipments have increased from 72,556,000 barrels during 1925 to 99,828,000 barrels during 1929. Shioments of Mid- Continent crude by pipe- line to Atlantic Coast refineries have , on the other hand , dropped from 11,903,000 barrels in 1925 to 1,409,000 barrels during 1929. Receipts of foreign crude oil declined 1,461,000 barrels from the preceding year . : Gasoline demand within the Atlantic Coast area reached a total of 123,345,000 barrels , an increase of 15.7 per cent over 1928. Gasoline production increased 4,157,000 barrels , while tanker receipts were nearly 11,000,000 barrels larger than in 1928. Indicated shioments from Appalachian refineries were somewhat larger than in the preceding year . Gasoline production showed an average of 33.5 per cent of the crude throughout , as compared with 31.5 per cent in 1928 and 32.7 per cent in 1927. Cracking operations accounted for 44.6 per cent of the gasoline produced , as compared with 40.6 per cent in 1928 and 35.3 per cent in 1927. Gas oil and fuel oil production averaged 52.8 per cent of the crude throughput , as compared with 55.1 per cent in 1928 and 49.5 per cent in 1927 , the decline reflecting the smaller quantities of foreign crude refined during the year .

Nov 1, 1930

By V. A. Marple, K. L. Rubow

"4.1 IntroductionIn previous chapters impactors have been described as useful instruments for classifying particles by their aerodynamic diameters and for measuring particle size distributions. These impactors can be used most reliably if the user has some understanding as to how the impactor classifies particles and what parameters are important in this classification process. This understanding can best be obtained by a theoretical inspection of inertial principles.This chapter reviews the most recent theoretical impactor work and the latest theoretical efficiency curves. Procedures are then given for using these efficiency curves in the design and evaluation of cascade impactors. Finally, several examples are given comparing theoretical and experimental efficiency curves, pointing out when the theory can be used with great confidence and when the theory should be used only as a guideline.Due to the rather simple principle of operation of an inertial impactor (i.e., the impingement of a jet of particle-laden air on a flat plate) the impactor readily lends itself to theoretical analysis. Three notable works in the early 1950,s were those of Davies and Aylward (1951), Davies et al. (1951), and Ranz and Wong (1952).Davies and Aylward (1951) used a method of conformal mapping to obtain an analytical solution to Euler's equation for the flow of a frictionless fluid through a rectangular impactor. Numerical calculations were then carried out whereby the equations of motion of the particles were solved in a stepwise manner, leading to a determination of the efficiency curves. Since this theory assumed potential flow, the effect of Reynolds numbers on the characteristics of the impactor could not be determined.Ranz and Wong (1952) used an approximate flow field to calculate the efficiency of both round and rectangular nozzle impactors. In the vicinity of the stagnation point, the flow field was assumed to be that of frictionless stagnation flow. Here, the resulting equation of motion for the particles was found to be in a form similar to equations for free vibration with viscous damping. Therefore, the known solutions of the vibration equations were applied directly to the problem and the efficiency curves calculated. This solution technique, however, could not take into account the various geometric variations such as the jet-to-plate distance in the determination of the efficiency curves.The work of Ranz and Wong (1952) was later modified by Mercer and Chow (1968) and Mercer and Stafford (1969) so that the rather simple flow fields of Ranz and Wong (1952) could be used to account for various jet-to-plate distances. The same techniques, however, were used to determine the impactor collection efficiency curves."

Jan 1, 1986

Develop a reliable, portable device for non-destructively testing the support integrity of a friction rock support (commonly referred to as a Split Set ). Approach The friction rock support, used to support mine roof and ribs, is a slotted tube driven into a drilled hole of smaller diameter. Upon installation, the tube is compressed radially. The amount of compression is a function of the hole diameter, the strength of the host rock, and the properties of the split set itself. A simple lightweight self-contained device was developed to determine the pull-out resistance of the friction rock supports in-situ, based on measurements of the tube's deformation. The tester measures the com-pressed internal volume of the slotted tube, which has been found to provide an estimate of the support's resistance to pull out. How It Works The tester consists of a pump and expander sections. The expander sections are made from an elastomer membrane which is stretched over two cores, each one inch in diameter and twelve inches long. The expanders are connected by a flexible coupler so that they can fit any alignment of the support.

Jan 1, 1984

By B. S. Covino

The Bureau of Mines has conducted a laboratory and field corrosion test¬ing program to determine materials of construction for the leaching and gas-sparging crystallization environments of the clay-HC1 process in order to more fully utilize the alumina from domestically available kaolinitic clays. Laboratory tests were used to determine the corrosion rates of 22 metals and alloys by weight-loss measurements in these two environments of the process. The results of this laboratory study were used both to suggest metals and alloys for field testing and to determine the effect of the individual solution components on the corrosion behavior of the metals and alloys. Results from the field tests were used to recommend Ta, Ta-2.5W, and Ta-10W for con¬struction of the agitators for the leaching process. The metals and alloys recommended for construction of the gas-sparging crystallizer heat exchangers were Ta, Ta-2.5W, Ta-10W, Nb, Nb-1Zr, Nb-3Zr, Nb-28Ta-10W-1Zr, Nb-10Hf-1Ti, and Zr for the first stage and Ta, Ta-2.5W, Ta-10W, Nb-28Ta-10W-1Zr, Nb, Nb-10Hf-1Ti, and Zr for the second stage.

Jan 1, 1981

By Margaret M. Ragin

In a cooperative effort between the U.S. Bureau of Mines and the Florida Institute of Phosphate Research, with input from the phosphate industry, the conversion of phosphogypsum to sulfur has been investigated. The first step in the conversion scheme involves reduction of phosphogypsum to calcium sulfide. Effects of temperature, catalyst, reaction time, and type of reductant (carbon monoxide and coal) are discussed. It was determined that phosphogypsum could be reduced to calcium sulfide at 850° to 1,000° C using either coal or carbon monoxide as the reductant. The required temperature was lowered to 750° C using ferric oxide or magnetite as a catalyst for the reduction reaction. Results indicate that as the volatiles content of the coal is increased, reaction temperature may be decreased to obtain a given conversion, or if the reaction temperature is maintained constant, the conversion can be increased. Best results were 95- to 100-pct conversion using a high-volatile coal at 800° to 850° C. Addition of a catalyst increased calcium sulfide yield when low- or medium-volatile coals were used as reductants, but had little effect when high-volatile coals were used.

Jan 1, 1990

By Maria I. De Rosa

For all coal mining categories, data on coal mine fires during 1990-1999 have been reported as actual numbers and calculated values. 1. For each mining category, actual numbers include the total number of fires, fire injuries, employees' working hours, lost workdays, and coal production (for underground and surface mines only) for a 1 0-year period (1 990- 1999) and for five successive 2-year periods with the 10-year period. These numbers have also been reported by state ( 10-year period). The actual number of fire fatalities has been reported by time period. Furthermore, actual numbers of fires for the five 2-year periods have been reported by ignition source, method of detection and suppression, equipment involved, location, and burning material. Actual numbers of fire injuries per number of fires causing injuries and total fires have been reported by year, ignition source, equipment involved, and location. 2. For each mining category, the calculated values include the fire and injury risk rates during the 10-year period and the five 2-year periods. The fire risk rate (Frr) values were calculated according to the USBM formula [Pornroy and Carigiet 19951. The injury risk rate (Irr) values were calculated according to the MSHA formula [MSHA 1991a, 1992, 1993, 1994a, 1995a, 1996, 1997, 1998b, 1999c, 20001. Also, risk rate values for individual states (10-year period) were calculated according to the above-mentioned formulas. Of note is that only the risk rate values for the 10-year and five 2-year periods and risk rate values for individual states with the highest number of fires and fue injuries were considered for comparison purposes. The fatality risk rate values were not calculated because of the extremely small number of fire fatalities during the 1 0-year period. 3. Calculations of risk rate values are as follows: a. Fire risk rate (Frr) value: Number of fires per million tons of coal produced [Pornroy and Carigiet 19951. b. Injury risk rate (Irr) value: Number of fire injuries multiplied by 200,000 working hours per total employees' working hours [MSHA 1991a, l992,1993,1994a, 1995a, 1996, 1997, 1998b, 1999c, 20001. The Irr value is the average risk rate value for the number of fire injuries per 200,000 working hours for a given time period.

Jan 1, 2004

By R. C. Buehl

Pilot-plant tests have been in progress at the Bureau of Mines, Pittsburgh, Pa., on the recovery of manganese from open-hearth slag.3/4/5/ In the process, 1 the slag is first reduced in a blast furnace to make a high-phosphorus spiegeleisen containing 12 to 22 percent manganese. A slag containing 55 to 60 percent manganese is made from this spiegel by oxidation in a basic-lined converter. The metal from this blowing operation contains about 3 percent phosphorus, 1 percent manganese, and less than 1 percent carbon. Economic efficiency in the manganese-recovery process requires that this metal be converted into steel. Because of its high phosphorus content the metal is suitable for blowing in a basic-lined converter. In most of the tests described in this report, metal of this composition was used as the starting material in a 1-ton, side-blown, basic-lined converter. Although basic-lined converters are not used for steel production in the United states, in Europe a considerable portion of the steel is made in them. Open hearths largely have replaced converters for steelmaking in the United States; mainly because open-hearth steels have better physical properties than converter steels because of lower nitrogen and phosphorus contents. However, by improving converter design and operating technique during the past 15 years, metallurgists have found that low-nitrogen steels with physical properties equal to open-hearth steels can be produced in converters.6/ Tests at Jones & Laughlin steel Corp. with side-blown, acid-lined converters of 3 and 22 tons capacity showed that steel with a low nitrogen content comparable to that of open hearths operating on scrap charges could be made by surface blowing.7/

Jan 1, 1955

By Len Blackman

The Absaroka-Beartooth Study Area is a tract of approximately 1.4 million acres of National forest land in southern Montana, part of the Greater Yellowstone Area. This study evaluated the mineral potential of four mineral terranes containing undiscovered resources in the area. The geological data is probabilistic, with estimates of the possible number: of deposits and their grades and tonnages. Possible future development scenarios range from no development to many mines, including some very large. As two thirds of the study area is within the Absaroka-Beartooth Wilderness, the future development scenarios reflect the area's mineral potential, not what we expect to see in the foreseeable future. Based on the analysis performed on these four terranes, the most likely future scenario for the study area would include the potential for two medium sized, (predominately) gold, mines, each employing a few hundred workers. There is a small chance, less than 5%, that a large Porphyry Copper or Superior Iron deposit would be discovered and be economically feasible to develop.

Jan 1, 1994