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By G. F. Comstock

H. M. BOYLSTON, Cambridge, Mass.-It might be asked, since this test is so simple, why it was not discovered before. It seems to me the explanation is that when we have used the sodium picrate solution, it has .generally been on a very, high-carbon or hypereutectoid steel; to detect . the presence of free cementite, and when we have looked for sulphides, it

Jan 4, 1917

By George Comstock

IT seems a common opinion among metallographists that all light-gray inclusions seen with the microscope in polished sections of steel are manganese sulphide. Examples of this belief are continually appearing, as for instance in the paper by Dr. Henry Fay on manganese sulphide as a source of danger in steel rails,1 and in Lieutenant-Commander Cook's paper on Metallography of Steel for U S. Naval Ordnance.2 Slate FIG. 1-TRANSVERSE VIEW OF THE EDGE OF A SMALL HOT-ROLLED STEEL ROD. ETCHED WITH PICRIC ACID. X 200. colored inclusions are considered to be silicates, and dove-gray inclusions, manganese sulphide. To show the danger in the latter unqualified assumption, it should be sufficient to examine the edge of any piece of steel that is covered with a fairly thick scale, and that has been polished in such a way as to prevent the scale from breaking away entirely below the polished surface. This can be done by protecting the scaled edge of

Jan 12, 1916

By Mills KW

Coal mine pillar design formulae available to mine planners are typically based on relationships determined for specific site conditions. Application of these methods is difficult when other factors, relating to mining or geological conditions, not specifically addressed in these relationships are encountered. A review of pillar design methods, coal strength properties and relevant field monitoring of pillar behaviour has shown pillar strength and deformational characteristics are extremely sensitive to in situ behaviour of the rock and other material components that make up the coal pillar system. A method has been developed that has been found to provide excellent correlation between existing field data using the strength and deformational characteristics of materials determined in selected laboratory tests. This method is based on definition of the loading conditions, accurate modelling of the strength, confining conditions and deformation occuring in the roof, floor and coal seam and definition of the in situ strength of coal based on underground monitoring of appropriately sized coal pillar. The design method is considered to provide an accurate and rigorous pillar design method that will give mine planners a more rational mine design capability which is based on the mine geometry and geological setting of the operation. It is envisaged that availability of such a method will allow significant optimisation of pillar layouts and more closely define the geological and mining issues that relate to pillar design optimisation.

Jan 1, 1992

By Winton J. Gale

Coal mine pillar design formulae available to mine planners are typically based on relationships determined for specific site conditions. Application of these methods is difficult when other factors, relating to mining or geological conditions, not specifically addressed in these relationships are encountered. A review of pillar design methods, coal strength properties and relevant field monitoring of pillar behaviour has shown pillar strength and deformational characteristics are extremely sensitive to in situ behaviour of the rock and other material components that make up the coal pillar system. A method has been developed that has been found to provide excellent correlation between existing field data using the strength and deformational characteristics of materials determined in selected laboratory tests. This method is based on definition of the leading conditions, accurate modelling of the strength, confining conditions and deformation occuring in the roof, floor and coal seam and definition of the in situ strength of coal based on underground monitoring of appropriately sized coal pillar. The design method is considered to provide an accurate and rigorous pillar design method that will give mine planners a more rational mine design capability which is based on the mine geometry and geological setting of the operation. It is envisaged that availability of such a method will allow significant optimisation of pillar layouts and more closely define the geological and mining issues that relate to pillar design optimisation.

Jan 1, 1992

By Raymond Wilson

GRINDING costs are an important item in cement manufacture, and the cost of power is one of the large items in grinding costs. Even where power is of secondary importance, cost items dependent on mill capacity are influenced by the efficiency with which the mill uses power. Tube mills typify the grinding mills most generally used in cement plants, though other types are in use. Tube mills have been widely criticized as being extremely inefficient, and this feeling regarding them has led to many attempts to design more efficient grinding equipment. Other types may be an improvement over tube mills, but the improvement has certainly not been revolutionary, at least as applied to clinker grinding. The very fact that there is doubt regarding the relative efficacy of various types of mills is an indication that an adequate basis for an analysis of performance is lacking. The development of methods of analyzing mill performance has been hampered by the lack of a suitable method for measuring the work actu-ally done in pulverizing. There has been no acceptable standard to which mill performance might be compared. As a consequence, it was not known whether the margin of possible improvement in pulverizing operations was large or small. Even direct comparison of different types of mills was seldom possible because most plants had only one type of mill for each type of service. Comparisons between plants were difficult because of differences in the grinding characteristics of various clinkers. Some recent developments complete a chain of circumstances that place the cement, industry in a particularly fortunate position for the study of its clinker-pulverizing operations. Modern investigators of grinding phenomena have generally agreed that the best measure of mill performance is the production of new surface. For most materials this measure of performance is largely theoretical and has a rather remote connection with the practical aims of the grinding operation. In clinker grinding, on the other hand, surface area is intimately connected with the properties conferred on the cement by grinding. Moreover, the determination of surface area is rapidly coming into routine use as a test

Jan 1, 1937

By Raymond Wilson

GRINDING costs are an important item in cement manufacture, and the cost of power is one of the large items in grinding costs. Even where power is of secondary importance, cost items dependent on mill capacity are influenced by the efficiency with which the mill uses power. Tube mills typify the grinding mills most generally used in cement plants, though other types are in use. Tube mills have been widely criticized as being extremely inefficient, and this feeling regarding them has led to many attempts to design more efficient grinding equipment. Other types may be an improvement over tube mills, but the improvement has certainly not been revolutionary, at least as applied to clinker grinding. The very fact that there is doubt regarding the relative efficacy of various types of mills is an indication that an adequate basis for an analysis of performance is lacking. The development of methods of analyzing mill performance has been hampered by the lack of a suitable method for measuring the work actually done in pulverizing. There has been no acceptable standard to which mill performance might be compared. As a consequence, it was not known whether the margin of possible improvement in pulverizing operations was large or small. Even direct comparison of different types of mills was seldom possible because most plants had only one type of mill for each type of service. Comparisons between plants were difficult because of differences in the grinding characteristics of various clinkers. Some recent developments complete a chain of circumstances that place the cement industry in a particularly fortunate position for the study of its clinker-pulverizing operations. Modern investigators of grinding phenomena have generally agreed that the best measure of mill performance is the production of new surface. For most materials this measure of performance is largely theoretical and has a rather remote connection with the practical aims of the grinding operation. In clinker grinding, on the other hand, surface area is intimately connected with the properties conferred on the cement by grinding. Moreover, the determination of surface area is rapidly coming into routine use as at test

Jan 1, 1937

By R. Phillips

The low concentration of diamond in workable deposits requires very large samples for grade estimation, and results, even then, may be erratic and difficult to interpret. Although the Poisson probability distribution cannot accurately describe the occurrence of diamond, it is suggested that it gives a better estimate of grade than conventional methods, even from single samples. Examples illustrate the simple calculation required.

Dec 1, 1971

By K. Y. Haramy

This report describes the development of an equation for predicting the crushing strength of 2-inch (5.08-cm) cubes of coal from point load tests made on irregular lumps. The equation was developed from point load and cube crushing strength tests performed on coal samples from six Western U.S. coal seams. For the six coals tested, the means of the point loads [(P)] in kg at failure were approximately proportional to the deans it the distances [(V)], in cm between the platen points for lumps in the 2 to 10-cm size ramie. This finding is at variance with results of tests on other rock types reported in the literature, which tend to show that P is proportional to D2 , as is normally assumed (in theoretical grounds. [The average crushing strength of a 2-inch (5.08 cu) cane for each type of coal was plotted against the log 10 of the slope of the P vs D plots, AP/AID . A straight line was fitted to these plots. The equation of the fitted line is cr = 1.72 x 10 4 10gK -2.10 x 10 4, where Cr is re estimated 2-inch (5. 08-cu,) cube crushing strength of the coal in psi and K is the scope of the straight line fitted to a plat of P v D for the same coal.]

Jan 1, 1982

As technology evolves, accidents may occur because human-system interactions were not considered adequately in the process. A systematic methodology can be used to evaluate the causes of mishaps and to develop recommendations that will enhance safety. A recent trend observed in underground coal mining is used to illustrate this principle because an underground mine is a dynamic work environment. Mining is characterized not only by frequent geologic changes but by technological evolution that can seriously degrade human performance and compromise worker health and safety The case exemplified in this paper involves implementation of remotely controlled equipment for extended cut mining. Extended cut mining technology evolved with minimal ergonomic consideration even though the change from on¬board to remote machine operation dramatically modified the role of the human component. In response to concern that system interactions should be examined more closely. a methodology was developed to identify hazards.

Jan 1, 1998

By Gottlieb P, Sutherland DN

The paper describes a method of making quantitative mineralogical measurements on many of the major lead/zinc orebodies in Australia. The work was done using QEM*SEM. It was found that a relationship betwen phase-specific surface area and particle size, when plotted in a suitable way, gave a straight line with slope related to the grain size of the mineral in question. The method provides an excellent way of differen- tiating between minerals in existing orebodies and, consequently, an easy way to establish a comparison between a new prospect or orezone and current operations.

Jan 1, 1988

By Z. Smieszek, Z. Szota, P. Gajowski

"A new method for measuring the total quantity of suspensions contained in the electrolyte during copper electrorefining has been developed by the Institute of Non-Ferrous Metals, Gliwice. Electrolyte purity, and the suspensions content in particular, is of essential importance for the quality of electrolytic copper produced during the process. Suspensions contribute to the increase of slime impurities in electrolytic copper and increase losses in noble metals. Up to now, the laboratory method has been used for the· process control which provides analytical results with considerable time delay. Therefore, it is useless for the process control.The measuring method developed enables continuous measurements of a suspensions content directly within the stream of the flowing electrolyte. The principle of measurement is based on changes in optic properties of the electrolyte with varying suspensions content.1. IntroductionIn copper electrorefining, it is essential that the final product quality be maintained. If suspensions are present in electrolyte, the content of slime impurities in electrolytic copper, (such as Pb, Ag, Bi, Sn, Sb, and As), increases which can result in the occurrence of the so-called slime dendrites on cathodes, thus debasing the quality of the product. As a normal suspension content in electrolyte, the contents in the order of several mg/l are considered, usually not more than 5-6 mg/l, while contents exceeding 20 mg/l are referred to as an alarm state. Suspensions present in an electrolyte are usually a light fraction of anodic slime whose main components are metallic silver, lead sulphate, complexes of antimony and arsenic, and sometimes even calcium sulphate; they are mainly composed of very small particles of lead sulphate and antimony complexes. Sometimes - - in case of alarm states - - the so-called ""wandering slims"" can be observed, which are composed mainly of arsenic and antimony complexes. These ""wandering slims"" make a serious technological disturbance. In normal operating conditions of the electrorefining plant, an increase of suspension content can result from such reasons as crack of filter cloth in a slime filter, turbulent flow of the electrolyte, anodic passivation, aeration of the electrolyte, and improper servicing of an electrolytic tank. It is necessary to continuously control the suspensions content in electrolyte for proper electrorefining."

Jan 1, 1989

By J. K. Whyatt

Assuring ground control safety in many mining and tunneling projects depends, at least in part, on an understanding of in situ stress conditions that will be encountered. Yet it is rarely practical to conduct more than a very limited number of stress measurements. Stresses along the route of a proposed excavation are typically interpolated from available measurements, often assuming a linear variation of stress with depth (or elevation). However, projects where multiple stress measurements are conducted often report more complex variations of in situ stress, usually in apparent relationship to geologic structures. These structures often include lithologies of contrasting elastic properties. A method is proposed for estimating stresses in these cases by first back-calculating regional loads from available stress measurements and then modeling the distribution of stress throughout the rock mass. The method has been successfully applied to a set of in situ stress measurements from the Coeur d’Alene Mining District of northern Idaho, USA. Results provided new insights into district stress conditions and the distribution of rockburst hazards along mine drifts and between various mines. This success should transfer readily to suitable deep tunneling projects.

By John A. Herbst, Kuang Y. Lee

Coarse particle size measurement is essential for the automatic control of a size reduction process like crushing or SAG milling in order to achieve optimal process performance. However, the on-line size measurement of coarse material is not easily obtained due to the problems of material handling and sample statistics. A technique based on advanced image analysis and quantitative stereology has been successfully developed and tested in a pilot scale setting. The chord length distribution of coarse particles on a moving conveyor was measured with an image analyzer and then transformed to the mesh size distribution with a stereological model and a special numerical method. Some test results as well as the technique's industrial suitability and limitations of this method are also discussed.

Jan 1, 1992

By Wang Huichang

A tentative mathod for predicting load-settlement relationship and bearing capacity of single piles based directly on the results measured by cone penetrometer with local friction sleeve is presented. It is possible that the load-settlement curves can be constructed by means of CPT and the problem of both the bearing capacity and the settlement behaviour of single piles can be considered jointly. The proposed load-transfer functions are continuous, positive monotonic and nonlinear. a concept of weight mean point resistance 2D above and 4D underneath the pile base to determine the unit ultimate base resistance of piles is presented. The predicted results of seven jacked piles in loess are in good agreement with the load test data.

Jan 1, 1991

By Jerzy Iskra, Wlodzimierz Sikora

INTRODUCTION The effect of stress concentration in coal seams leads to a sudden release in the form of rock bursts. This effect is controlled along many lines, but the most efficient methods consist in preventing the accumulation of energy in the seam or in the roof. The over- burden weight resulting from mining is the main cause of excessive stresses in a seam. An additional weighting of roof takes place due to formation of abutment loads. The accumulation of energy in the roof takes place where thick sandstone beds occur in overburden strata. An essential problem is to watch, with appropriate measurements, the stress of coal and roof rocks, and to conclude, on this basis, the degree of rock burst hazard. The methods for determining the stresses in a coal seam are quite well developed at present. Let me mention here the seismoacoustic methods, or borehole overcoring measurement methods. On the other hand, an examination of the state of stress in the roof rocks is almost impossible at the actual stage of development of the measuring technique. Hence, the model of stresses in roof was analyzed and determined theoretically. Based on this model, a technology for roof fracturing was developed which aims at destressing rock masses in a planned way. The essentials of the fracturing method consist of a controlled breaking of sandstone roof beds in order to: - prevent the excessive weight on the pillar - prevent a spontaneous breaking of roof beds at a limiting state followed by sudden energy release. High pressure fluid infusion is used to release buildup of stresses. THEORETICAL AND RESEARCH BASES According to the tests carried out by A. Kidybinski by the method of finite elements, isobars of stresses occurring in the roof over the working face are shown in [Fig. 1]. The results indicate: - the highest values of compressive stresses occur in the roof directly over the seam, at a distance of about 5 m ahead of the working face - at a distance of about 22 m above the seam there is a line of transition of compressive stresses into tensile - within the tested roof area, the highest tensile stresses occur at a vertical distance of 35 m, and at a horizontal distance of 20 m from the line of the working face. H. Gil (1) determined the pres- sure initiating the fracture of roof rocks by the formula: [ ] On the basis of results of analysis of isobars, and of the initiation of failure stress formula (1), isobars may be designed for a given roof class. Assuming for sandstones the Poisson ratio equal 0.3, a field of failure stresses presented in [Fig. 2] is obtained. In this figure it can be seen in which areas the effects of sandstone breakage may be obtained with the operation of a determined hydraulic pressure. To use formula (I), the knowledge of Rr is still necessary. This value may be determined in two ways: - taking a sample and testing it in the laboratory, if there is access to roof rocks in the existing openings, - drilling boreholes in the roof from surface and examination of the rock mass by using hydraulic breaking, if there is no access to roof rocks.

Jan 1, 1982

By Syd Peng

In designing a proper roof support system, one must know the features of roof geology in advance of mining. The drilling parameters obtained during normal roof bolt installation cycle can provide a large amount of information on the roof geology when properly interpreted. It is also an economic way for identifying the geological features of the roof. This research develops a method for predicting the roof geology based on the drilling parameters obtained during roof bolting operation. From the results of a series of laboratory and underground tests, feed pressure is found to be a good indicator for identifying the voids/fractures and estimating the roof rock strength. This paper describes the method for determining quantitatively the location and the size of void/fracture and estimating the roof rock strength from the drilling parameters of roof bolter.

Jan 1, 2005

By C. D. Mishra

The recycling potential for any gainful utilisation of the waste products is dictated by their quality, especially the chemical characterisation. The methods commonly used for the analysis of fly ash e.g. wet chemical, AAS, ICP-AES etc are time consuming. The paper describes a rapid XRF-based method for routine analysis of fly ash which involves preparation of local standards, optimisation of sample preparation technique and use of a simple PC-based software to account for interelement effects. The matrix corrected values are found to agree well with the wet chemical data.

Jan 1, 1992

By V. A. Marple, K. L. Rubow

"Filter samplers are one of the simplest methods and, in some instances, one of the only methods that can be use to obtain samples of particulate matter suspended in a gaseous medium. Once collected, particles are normally analyzed directly on the filter by gravimetric, chemical or microscopic techniques. However, it is sometimes desirable to resuspend the particles in an airstream for analysis. This would be the case if the size distribution of the particles were to be measured using one of many particle sizing techniques such as inertial classifiers, optical particle counters or the TSI Aerodynamic Particle Sizer CAPS).A ·technique has been recently developed whereby one can resuspend particles from filter samples in an airstream. The technique has been used for the resuspension of coal dust from filters. The resuspended particles were then introduced into the APS. This development was necessary since an APS can not be taken directly into an underground coal mine. For this application, particle samples are collected on membrane filters in the underground mines. The mass concentration of the particles determined through gravimetric analysis. The particle size distribution was tl1en determined by resuspending the particles and passing them through a TSI Aerodynamic Particle Sizer (APS). Excellent agreement has been obtained between the size distribution directly measured underground with a cascade impactor and that measured from the resuspended particles. For this experiment, an open-faced filter sampler was placed adjacent to the cascade impactor in the n1ine. The particles collected on the filter were resuspended in the laboratory and Measured with the APS.A venturi aspirator is used in the apparatus developed for resuspending the particles. The venturi has a small diameter capillary tube placed in the venturi throat. High velocity air flow is passed through the venturi, thereby, creating a low pressure region at the exit of the capillary tube. The low pressure draws air through the tube. The filter with deposited particles is located at the inlet to the capillary tube where the air flow into the capillary resuspend the particles. Once airborne, the particles are deagglomerated as they pass through the high velocity air flow in the venturi throat."

Jan 1, 1989

By A. Kalogeropoulos, T. Michalakopoulos

The DEM has been used in several studies to numerically simulate the response of rocks to the cutting action with drag tools. In this research, the aim is to realistically simulate the rock material and the cutting process by controlling the grain interlocking of the numerical assembly and streamlining the calibration process while focusing on the cutting force and the failure mechanism.

Apr 1, 2023

By Andrew P. Ritter, James W. Reil, Douglas A. Anderson, Stephen R. Winzer

We have developed a method for predicting and controlling ground vibration from blasting using a rigorous scientific approach. The method is based upon the superposition of seismic waveforms generated by a single-hole free-face shot, recorded at seismographs deployed in an array that includes environmentally sensitlve locations. Waveforms generated by single-hole shots are shown to be reproducible. The waveforms for each of the sites are used to construct synthetic seismograms for delayed shots based upon linear superposition. A computer code systematically constructs the seismograms for the delayed shots, with incremental delays between holes of 1, 2, or 3 milliseconds (ms). A Fourier amplitude specs-rum is calculated for each synthetic seismogram and the spectra are plotted on a map in delay-frequency space, i.e., each row of the map represents the Fourier spectrum for a blast with a particular delay interval. For single-row shots, the delay between holes in a row is used; for multiple-row shots, the delay between holes In a row is kept constant and the delay between rows is incremented. Predicted vibration varies strongly as a function of delay and h

Jan 1, 1985