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By Gabriel Burlandy Mota de Melo

Manchas de óleo em um meio aquoso foram removidas utilizando compósitos de parafina com nanopartículas de ferritas de cobalto (CoFe2O4), níquel (NiFe2O4) e níquel-zinco (Ni0,7Zn0,3Fe2O4), nas proporções de 13,0% e 28,5% em peso. Para avaliar a eficiência da remoção, foi determinada a velocidade dos compósitos ao serem acoplados a uma mancha de óleo na superfície da água e submetidos ao campo magnético de um imã permanente. O melhor desempenho foi obtido com o compósito de parafina contendo 13,0% em peso de ferrita de níquel-zinco.

Aug 16, 2017

By Anselmo Monteiro Ilkiu

No presente trabalho será apresentado um modelo matemático para a análise da instabilidade plástica de um cilindro de parede fina sujeita a pressão interna, considerando o material com anisotropia normal R no estado plano de tensões. As equações foram obtidas, com base nas teorias elásticas e plásticas, considerando o critério de escoamento de von Mises no estado plano de tensões em termos da anisotropia normal, e de acordo com os trabalhos realizados por Johnson & Mellor [1], Chakrabarty [2] e Al-Qureshi [3].

Aug 16, 2017

By Érika Aline dos Santos

Este trabalho tem como objetivo a síntese de materiais híbridos nanoestruturados à partir da funcionalização do argilomineral haloisita com (3-aminopropil)trietoxissilano (APTES) para aplicação em processos de adsorção. A rota de modificação baseou-se na acidificação e posterior reação química entre as hidroxilas superficiais da haloisita e os grupos hidrolisáveis de APTES na presença de tolueno sob refluxo. Haloisita em sua forma natural e modificada foi caracterizada por análise termogravimétrica (TG), área superficial específica (BET), espectroscopia de infravermelho (FTIR) e difração de raios X (DRX). A quantidade de APTES enxertado, calculado através da análise termogravimétrica foi de 7,32% para a amostra funcionalizada previamente acidificada e 6,50% para a amostra funcionalizada sem pré tratamento ácido. A área superficial das amostras diminuiu com a funcionalização. As amostras funcionalizadas exibiram novas bandas características de grupos de APTES no espectro obtido por FTIR confirmando a ocorrência da funcionalização do organosilano na haloisita. A análise de DRX indicou que a estrutura original não foi alterada após a funcionalização.

Aug 16, 2017

By Diego Ruben Martin

Este trabalho objetivou comparar, por meio de experimentos desenvolvidos em uma fundição, através da adição de três inoculantes diferentes (IM-22 com FeSi-Ba/Zr, G 20 com FeSi-Ba) e IMSR 75 com FeSi-Sr), para observar as características da vida util de ferramentas na usinabilidade das peças, microestrutura e propriedade mecânica. A metodologia da pesquisa se baseou em analisar principalmente pelo processo de fresamento o ferro fundido cinzento GG-25 inoculado diferentemente, denominado de acordo com a Norma DIN EN 1561. As formas de avaliação dos resultados terão como base uma análise quanto ao desgaste da ferramenta, acabamento superficial, análise microestrutural, composição química e propriedades mecânicas do material da peça. Os resultados mostraram que dentre os inoculantes aplicados o com Sulfeto de Estrôncio (SrS) apresentou-se mais estável termodinamicamente que as amostras inoculadas com os outros dois inoculantes, pois ele levou a uma variação da energia livre de Gibbs mais negativa e portanto mais favorável a formação de núcleos com raio crítico (rc) maiores, o que permitirá uma solidificação com nucleação heterogênea. Todavia o respectivo inoculante também foi mais eficiente na formação de uma microestrutura mais estável, com maiores quantidades de células eutéticas e vida útil do inserto mais longa quando usinado.

Aug 16, 2017

By Alessandra Savazzini dos Reis

A indústria de cerâmica vermelha brasileira consome 10,3 bilhões de toneladas de argila ao mês para produção de telhas e blocos. Uma alternativa para tornar o setor mais sustentável ambientalmente é a incorporação de resíduos na massa argilosa. Na própria olaria são gerados resíduos, tal como, o resíduo de massa cerâmica crua originado na etapa de conformação das peças. Este trabalho visa caracterizar o resíduo de massa cerâmica crua para incorporação na massa argilosa usada em cerâmica vermelha. O resíduo de massa cerâmica crua foi caracterizado através de ensaios de FRX, DRX, calorimetria exploratória diferencial e termogravimetria, limites de Atterberg e distribuição de tamanho de partículas. Corpos de prova foram conformados, secos à 110ºC e queimados à 900ºC em forno industrial e foram submetidos a ensaios de absorção de água, porosidade aparente, massa específica aparente e resistência à flexão. Os resultados evidenciam que as propriedades cerâmicas avaliadas nos corpos de prova atendem aos valores das argilas-padrão brasileiras para uso em cerâmica vermelha.

Aug 16, 2017

By Claudio Luiz Schneider

Não existe na literatura formal uma descrição dos ensaios de caracterização necessários para a correta determinação de parâmetros de balanço populacional para escalonamento pelo método de Austin. As rotinas envolvidas são normalmente aprendidas em Universidades e Centros de Pesquisa que contam com engenheiros e/ou pesquisadores especificamente treinados para estes experimentos. Isso faz com que estes sistemas modernos sejam pouco utilizados na engenharia e restringe sua aplicação. Este artigo tem por objetivo estabelecer os procedimentos envolvidos na caracterização de processos de moagem e fomentar a utilização de técnicas modernas de escalonamento de moinhos de bolas nas empresas.

Aug 16, 2017

By Maria Anita de Paula Negreti

Neste trabalho, foram obtidos compósitos poliméricos de Óxido de Grafite (GO) incorporado em Poli(metaclilato de metila) (PMMA). A obtenção do Óxido de Grafite foi realizada pelo método de Hummers modificado. Em seguida foi ainda adicionada uma etapa secundária de tratamento térmico à 1000ºC no GO obtido a fim de expandir as lamelas de grafite e remover os grupos funcionais aderidos durante o ataque ácido do grafite. As cargas obtidas foram caracterizadas com o auxílio das técnicas de Difração de Raios-X (DRX), constatando a expansão das folhas após o tratamento térmico. O estudo comparativo dos compósitos de matriz polimérica com 3 % de concentração de GO antes e após o tratamento térmico foi realizado com o objetivo de entender a contribuição nas propriedades reológicas do polímero com a adição da carga de GO. Os resultados reológicos apresentaram um aumento da viscosidade complexa tanto no ensaio de Varredura de Tempo, quanto no Cisalhamento Oscilatório de Pequenas Amplitudes (COPA).

Aug 16, 2017

By Daniel Augusto Godinho de Carvalho

Since the beginning of BOF process, slag formation has been subjected to extensive development. During the initial stages of the blow, fast slag formation is primordial for the process performance. This is mainly to allow oxidizing reactions, and also to protect the refractory. A modeling of BOF process for the purpose of process optimization requires precise knowledge concerning the dissolution of CaO and MgO based materials. Using this knowledge, the optimal process conditions can be ensured by a controlling of the slag formation during the converter steelmaking process. Taking into account an application of large amount of different raw materials, as well as location-specific process conditions, the characterization of the dissolution behavior of different additives is an important key to improve the technological process. Thereby, in the frames of this project, an appropriate model for slag formation is established and compared to operational results for a 330t BOF, operating at ThyssenKrupp CSA, Santa Cruz, Brazil.

Aug 16, 2017

By Filipe Sathler

Mediante efeitos de sazonalidades do mercado Siderúrgico, períodos de crise, aliados às necessidades de reparos de equipamentos, os Altos Fornos são, eventualmente, submetidos ao desligamento. O procedimento específico mais utilizado é o Blowdown, com o abaixamento de carga até nível de ventaneiras, facilitando posterior limpeza e reparo. Para sucesso deste procedimento, é essencial um planejamento adequado das atividades. Informações técnicas e experiências operacionais permitiram o embasamento teórico e a execução do Blowdown do Alto Forno 03 da ArcelorMittal FCSA (Tubarão). Como preparação, foi efetuado o aumento do fluxo periférico (remoção de cascão) e o aumento da permeabilidade do Cadinho (maior circulação de líquidos, limpeza e drenagem). Realizou-se também a preparação de equipamentos específicos e controle dos parâmetros operacionais. O abaixamento de carga foi devidamente realizado conforme planejado, até o nível de ventaneiras e permitindo paredes internas livres de cascões.

Aug 16, 2017

By S Hapugoda, A Poliakov, E Donskoi, L Lu

A significant amount of metallic iron in the world is produced in blast furnaces from iron ore pellets. To control the quality of pellets and to optimise pellet production, characterisation of both green and fired pellets is required. Optical image analysis (OIA) allows identification of different minerals, binder, remaining fluxes and porosity within pellets.For proper identification of the mineralogy, porosity and texture in pellets a high magnification is required, therefore each individual image covers only a very small portion of the pellet. At the same time the characterisation of pellets requires that the whole pellet is represented as a single object, so the size of the resulting overall image at high magnification can make it difficult to handle. A solution to this problem has been implemented within the CSIRO OIA package Mineral4 by combining images at different levels. Namely, to average out local irregularities, individual frames can be stitched during imaging into larger MosaiX images. Mineral4 further combines these MosaiX images into a single panorama image of the whole pellet.The proposed procedures allow the calculation of mineral and porosity spatial distributions, local gradients and abundance graphs based on the distance from the centre of the pellet. The ‘Pellets’ module of CSIRO OIA software also allows for characterisation of large irregularly shaped particles of lump ore and sinter.CITATION:Poliakov, A, Donskoi, E, Hapugoda, S and Lu, L, 2017. Optical image analysis of iron ore pellets and lumps using CSIRO software Mineral/Recognition, in Proceedings Iron Ore 2017, pp 583–592 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Jul 24, 2017

By B B. Du, Y N. Lu, L X. Wang, S L. Wu

The cohesive zone in the blast furnace is largely affected by the softening and melting behaviour of ferrous burden because of its vital role in the blast furnace process. The Visual High Temperature Methodology (VHTM) has been given to study the softening and melting behaviour of sinter, two kinds of lump ores and acid pellet intuitively. Before softening, both two kinds of lump ore swelled and more serious for lump ore B because of its denser structure than lump ore A. The softening and melting temperature intervals are different from one another and this phenomenon contributed to the gas permeability of ore layer in the cohesive zone since the ‘ore window’ has formed. Besides, the softening and melting behaviour of mixed burdens have been studied, where it has been found that the softening and melting characteristics of mixed burden A (consisting of sinter and lump ore A) is better than mixed burden B (consisting of sinter and lump ore B) and mixed burden C (consisting of sinter and acid pellet) despite the poorest characteristics of lump ore A. The reason is that the high temperature interactivity between lump ore A and sinter is much better than lump ore B and acid pellet. The high temperature interactivity is mainly influenced by the chemical compositions, porosity and contact condition. This paper provides a new research method for the softening and melting behaviour of iron ore and an important technical basis for the optimisation of blast furnace burden.CITATION:Wang, L X, Wu, S L, Lu, Y N and Du, B B, 2017. The softening and melting behaviour of single and mixed iron ore burdens, in Proceedings Iron Ore 2017, pp 605–610 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Jul 24, 2017

By B Hiebl, J Martens, L Petzold

A research team at the Iron and Steelmaking department at Primetals Technologies has established new upgrading measures for improving the efficiency of the beneficiation process in ironmaking plants, relying largely on pre-existing equipment. After the upgrade, the iron content in the final iron ore concentrate was shown to be significantly higher. Remarkably, the costs for employing the respective measures are surprisingly low.This case study is based on a Kazakh iron and steel producer, whose beneficiation process is currently generating a magnetite concentrate with a final iron content of 65.65 per cent. The study shows that the implementation of Primetals Technologies’ intelligent modification measures to the current beneficiation process, the realisation of more effective dewatering, and the utilisation of an innovative binder lead to an increased iron content in the resulting pellets, reaching a concentration of 69.17 per cent (iron ore concentrate) and 66.5 per cent (pellets).The current operation consists of three closed circuit grinding stages, four stages of low intensity magnetic separation, vacuum disc filters and straight-grate pelletising. By dividing the slurry after the second stage of grinding and the third stage of low intensity magnetic separation, it is possible to divert the more iron-rich fines before they would enter the third grinding stage and the fourth stage of magnetic separation. This then reduces the load on the existing third stage ball mill. Afterwards, the ground material is treated in an additional low intensity magnetic separator and mixed with the previously diverted fraction of the fines. An improved filtration procedure, combined with the application of a highly sophisticated binder, further reduces the amount of additives needed, so that a genuine direct reduced (DR)-grade iron concentrate is produced as a result.All laboratory, pilot and pelletising test work was executed at Primetals Technologies’ laboratories in Austria.CITATION:Martens, J, Petzold, L and Hiebl, B, 2017. Enabling iron ore concentrate for the production of direct reduced iron with pre-existing beneficiation lines, in Proceedings Iron Ore 2017, pp 227–232 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Jul 24, 2017

By T Sylow, A Correa De Araujo, M Gotelip Barbosa

ArcelorMittal is among the largest world’s producers of iron ore. With a geographically diversified portfolio of iron ore and coal assets, it is strategically positioned to serve the network of steel plants, as well as supply the external global market. ArcelorMittal Mining has a global portfolio of 14 iron ore operating units across Brazil, Bosnia, Canada, Kazakhstan, Liberia, Mexico, Ukraine and the United States. Iron ore products include concentrate for sintering and pelletising, pellets, directly shipped fines and lump ore. This paper presents an overview of ArcelorMittal iron ore mines including iron ore typologies and the annual production of each unit. It will also briefly discuss the processing required in order to obtain marketable products.CITATION:Gotelip Barbosa, M, Correa De Araujo, A and Sylow, T, 2017. Overview of ArcelorMittal mining operations and research and development, in Proceedings Iron Ore 2017, pp 161–116 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Jul 24, 2017

By I Sherrell, R Jain, P Jansson

With the depleting iron reserves and difficult market conditions, precision in separation efficiency is of utmost importance. Classical local control options are predominant in the industry, but their inability to adjust to resolve application problems of interest has furthered the need of developing and implementing continuous control methodologies.This paper highlights the recent development in control of Outotec SLon® vertically pulsating high gradient magnetic separator (VPHGMS) including programmable logic controllers (PLC) coupled with distributed control system (DCS), on-site human–machine interface (HMI) control panel, advanced process control, continuous online sampling using Courier® 8 and additional modernisation packages including level control and cooling monitoring. These modern control options result in improved efficiencies, promote safer operation and at the same time reduce operational manpower needs.CITATION:Jain, R, Sherrell, I and Jansson, P, 2017. Automation for efficient separation with the Outotec SLon® vertically pulsating high gradient magnetic separator, in Proceedings Iron Ore 2017, pp 211–214 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Jul 24, 2017

By R Zhou, B J. Monaghan, S J Chew, R J. Longbottom, D J. Pinson, H Li, P Zulli, G Zhang, L Lu

Steelmakers are increasingly motivated to use iron ore resources with a wider range of grades and mineral types that were previously considered unsuitable or uneconomical for sintering. In this respect, specific issues, which now require further investigation and understanding, include the sintering of ore types with:- overall higher gangue content- elements that cause problems in the steel manufacturing operations- distinctive sintering performance compared with traditional hematite-rich iron ores. Laboratory-based investigations of the sintering performance and the behaviour of gangue impurities during sintering is an important step towards the successful utilisation of these resources in steelmaking.In terms of laboratory-based sintering investigations, there are two generally accepted experimental scales utilised prior to undertaking industrial-scale trials, which include: bench-scale tablet (compact) testing and pilot-scale pot testing. The former has the advantages of flexibility and more precise control of sintering conditions; but it is difficult to simulate the heterogeneity of a sinter bed. The latter, which is carried out in pots with diameters between 150–500 mm, simulate the commercial sintering process and conditions quite well, but is time-consuming and labour-intensive due to operational complexity. It is therefore desirable to establish a smaller scale pot testing facility that avoids the disadvantages of the normal sintering pot but can provide comparable information.To explore the feasibility of small-scale pot testing, a ‘millipot’ facility was established to examine the sintering performance of iron ores and other non-traditional ferrous materials. The millipot has a diameter of 53 mm and height of 400 mm. The facility has the capability to monitor the sintering temperature at a number of locations (axial, radial) within the sinter bed and to adjust the suction (‘windbox’) pressure. This paper describes the development of the millipot facility and operational procedures, together with initial tests undertaken in order to match its performance with industrial sintering performance.CITATION:Li, H, Zhou, R, Pinson, D J, Zulli, P, Lu, L, Longbottom, R J, Chew, S J, Monaghan, B J and Zhang, G, 2017. A millipot set-up for sintering investigation of iron ores, in Proceedings Iron Ore 2017, pp 85–90 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Jul 24, 2017

By R Stefansen

Stockyard operations are governed by the interaction between the different disciplines required to successfully schedule and control the supply chain of raw material through the stockyard in combination with the effectivity of the operation of the stockyard equipment. The system demonstrates a proven technology for implementing a centralised operation of full unmanned stockyard equipment, using a high precision absolute positioning system based on a Real-Time Kinematic (RTK) Global Navigation Satellite System (GNSS) receivers in combination with 3D rangefinders. The system implementation maps the surface profile of the stockyard inventory and allows in combination with proprietary algorithms for full operation of the stockyard machines without on-board operators. The operational impact of delayering the process by moving to a centralised operation is examined, together with the combined effect on the overall safety in the stockyard as a result of a change in reliance on operator skill dependencies. Average performance gains range from 10–20 per cent. The performance of the automation system is related to a consistency and reliability of uniform operation, which has an impact on the life expectancy and the effectiveness of the equipment. The effects of having instantaneous and correct information about the stockyard inventory volume measurement are investigated in relation towards spot price trading in current fast reacting markets.CITATION:Stefansen, R, 2017. Advanced automation for centralised stockyard operations, in Proceedings Iron Ore 2017, pp 105–110 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Jul 24, 2017

By L Matthews, D O’Dea, P C Hayes, J Manuel, B Monaghan, T Honeyands, D Pinson, J Leedham

Many different approaches have been used in the past to characterise iron ore sinter mineralogy to predict sinter quality and elucidate the impacts of iron ore characteristics and process variables on the mechanisms of sintering. Characterisation techniques include optical image analysis and point counting, X-ray diffraction and scanning electron microscopy. Each technique has its advantages and disadvantages depending on the objectives of the measurement. It is generally acknowledged that silicoferrite of calcium and aluminium (SFCA) is very important to the quality of the sinter produced; however, strict definitions of the phases and textures of SFCA are not generally agreed. This paper summarises the state-of-the-art in sinter characterisation applied in Australia by both academics and industrial researchers. The results from various techniques are compared and the relationships between the measurement results are discussed.CITATION:Honeyands, T, Manuel, J, Matthews, L, O’Dea, D, Pinson, D, Leedham, J, Monaghan, B, Li, H, Chen, J, Hayes, P C, Donskoi, E and Pownceby, M I, 2017. Characterising the mineralogy of iron ore sinters – state-of-the-art in Australia, in Proceedings Iron Ore 2017, pp 49–60 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Jul 24, 2017

By T A. J Hopper, B J. Birt, K K. Trofimczyk

Nuclear magnetic resonance (NMR) has been utilised in the oil and gas industry for over 60 years. The technology was recently identified as having potential value in iron ore, where latent bound moisture may affect ore handling even after dewatering and extraction. The first step in introducing this technology to iron ore involved laboratory tests on drill core samples. These results established the parameters for a downhole borehole magnetic resonance (BMR) tool for iron-rich environments, which was subsequently developed. A major challenge involved shrinking what is a very large tool in the oil industry to a slimhole, lightweight, 1-man deployable mining tool.Of primary concern was the ability to measure the very fast transverse relaxation times (T2s) seen in the lab results on iron ore samples. Iron creates local field gradients that significantly decrease the T2 times. As a result, the BMR tool had to be able to measure T2s in the range of hundreds of microseconds, a level not required in clastic sedimentary formations. The choice of T2 cut-offs in iron ore is critical to successfully separating the free and bound fluids. The industry has typically focused on T2 cut-offs in clastics and carbonates, but not in systems with high iron content. Using core analysis results (poro-perm and NMR) we were able to verify the BMR response. The T2 cut-offs were determined from NMR core analysis and then applied to the logs so as to provide a continuous, calibrated permeability log.Field results that highlight the challenge involved in logging in iron-rich environments are presented, as well as some minimum requirements for a successful BMR log. Examples from boreholes in an active iron ore mine in the Pilbara iron ore province in Western Australia are presented, as well as explanations for how NMR data can be combined with bulk density logs to provide a continuous dry weight density log based on the original density-porosity equation from Alger et al (1963).CITATION:Hopper, T A J, Trofimczyk, K K and Birt, B J, 2017. Development of a slimhole downhole nuclear magnetic resonance tool for iron ore – some applications and limitations, in Proceedings Iron Ore 2017, pp 473–480 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Jul 24, 2017

By M Shaffer, D C. Grant, D J. Goudie, P Sylvester, C Voisey

Scanning electron microscope–Mineral Liberation Analyser SEM-MLA can be used to discriminate between hematite/magnetite in iron ores, but achieving backscattered electron (BSE) segmentation between the two minerals is difficult for particles =75 µm using typical preparation and analysis methods for the MLA based on a tungsten filament SEM (Quanta 400) with 25 kV high voltage. Preparing iron ore sample mounts using a slow-speed polishing method, and conducting the experiment on a field emission gun SEM-MLA (Quanta 650) with the high voltage (HV) setting lowered to 15 kV reduces instrument noise and results in very clean BSE images and segmentation. This method requires new X-ray standards to be acquired for each mineral identity at 15 kV because of major changes in the spectra at lower kV. However, once these X-rays are added to the mineral reference list, effective segmentation can be achieved and a proper analysis obtained.CITATION:Grant, D C, Goudie, D J, Voisey, C, Shaffer, M and Sylvester, P, 2017. Discriminating hematite/magnetite via scanning electron microscope–mineral liberation analyser in the - mesh size fraction of iron ores, in Proceedings Iron Ore 2017, pp 541–548 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Jul 24, 2017

By A T. Job, P R. McAree

There is significant value at stake in the mining industry from the implementation of new technologies that support the enhanced profitability and sustainability of mines. However, in order to realise this value, new technology must be implemented in a way that is both effective and sustainable. The industry has a mixed history for technology implementation that provides fertile ground for understanding what is necessary for innovation to deliver value. This paper describes early stage research investigating why this is so, with the aim of improving how to deliver value. Several case studies are provided covering both successful and unsuccessful technology interventions. The paper identifies the common factors that emerge from the case studies, and offers a path forward for further research in this area.CITATION:Job, A T and McAree, P R, 2017. Three case studies on the implementation of new technology in the mining industry, in Proceedings Iron Ore 2017, pp 407–414 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Jul 24, 2017