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By Behram H. Wadia, Robert S. Lehto

A new metallurgical treatment for capturing as much of the values as possible from zinc refinery feed has been devised by personnel in Cerro de Pasco's Peruvian operation at La Oroya. Results from a pilot test illustrate that 50 metric tons of throughput can be maintained whereby substantially all the silver and copper report in the sponge iron while zinc and lead with indium and cadmium volatilize in the fume. This new technique named the Zileret (zinc leach residue treatment) process complements the electrolytic system used in the refinery so that all values in a zinc concentrate are economically recovered. In the system, dried zinc leach residue is pelletized with soluble zinc sulfate which already exists in the leach residue and a finely divided reducing agent such as anthracite coal. Upon heat addition, the loose anthracite in the charge maintains a reducing atmosphere while the free space above the charge has an oxidizing nature. When the charge reaches the reaction zone at about 1100°C, metals such as zinc, lead, cadmium and indium volatilize from the pellets, are oxidized in the upper kiln atmosphere, and are then carried in suspension as an oxide fume to the cooler and baghouse. The copper and silver content in their reduced forms, along with the iron, discharge from the kiln as a calcined product which is then cooled to below 130°C before being exposed to the air.

Jan 9, 1969

By B. C. Mariacher, I. Hoffman

In 1952, beneficiated phosphate ore first began to move from the Oron plant of Negev Phosphates Ltd. in the Negev Desert to the super-phosphate plant at Haifa, Israel. Since that time this company has continually sought to overcome its natural handicaps affecting the operating efficiency and quality of the product in an effort to bolster the agricultural program of Israel and the development of an exportable commodity. The most serious deterrent to the development of a beneficiation process was the total absence of water. The Oron plant lies approximately 30 miles south of the irrigated regions of Israel with the nearest producing water well located about 10 miles to the northwest. The urgency of early phosphate production made it necessary to consider only dry processes in the initial operation. Fortunately, the ore was amenable to a dry process which yielded a usable concentrate assaying about 28.5 pct P2O5; but phosphate recovery was low. A description of the characteristics of the Negev ore should help to clarify the principles upon which the dry concentration is based.

Jan 5, 1961

By E. D. Williamson

DURING the wartime rush to prepare the glass necessary for the needs of our army and navy, the problem of the temperature control of the annealing kilns became most serious. The narrow limits of strain allowable (all the specifications called for less internal strain than the average of the previously used German glass) made necessary a very exact procedure and the methods had to be used on a much larger scale than theretofore. At the Charleroi plant of the Pittsburgh Plate Glass Co., the members of the staff of the Geophysical Laboratory, which was cooperating with the company, had occasion to study the methods available, and reached a number of conclusions (many of them by no means new except in their application) that may interest and assist those who have to meet similar problems in other fields. The following is a short account of the essential features of the system of temperature control evolved, along with a rather abridged statement of the reasons that led to the adoption or rejection of various schemes.

Jan 8, 1919

By M. B. Standing, D. L. Katz

Density data are reported on 15 saturated hydrocarbon liquids in the range of 35° to 250°F. and 1000 to 8220 lb. per sq. in. The apparent liquid densities of methane and ethane are shown to vary with the density of the system in which they are present. A method is proposed whereby the densities of liquid hydro- carbon mixtures containing both methane and ethane in solution may be computed at elevated temperature and pressures within the accuracy of usual engineering computations. A method of computing the shrinkage of crude oils based upon the gas-oil ratio, gas analysis, and crude gravity is outlined. Introduction The densities of naturally occurring liquid hydrocarbon mixtures are important in many petroleum engineering computations. Calculation of the shrinkage of a subsurface sample of crude oil as the natural gas is evolved is one example of the use of liquid-density data. Sage, Hicks, and Lacey5 have presented a method of computing the density of hydrocarbon liquid mixtures based on partial molal volumes. Katzl has indicated a method based on the principle of additive

Jan 1, 1942

By L. R. Velho, N. A. D. Parlee, J. Gani

THE unsteady-state type of gas-liquid metal diffusion cell1 has found considerable application.2"4 Cells of this general design can function as steady-state cells if allowed to operate long enough to reach steady state. This report tells of some success in the adaption of this type of cell for steady-state work, using the 0-Ag system in which the mass transfer of the gas "species" is basically controlled by diffusion in the liquid. The gas, e.g-., O2, is maintained in the cell tube'-3 at 1 atm pressure, Fig. 1, by buret and sensitive oil manometer. The gas, after diffusing through the stagnant metal, escapes at the annular metal surface around the tube at a lower constant partial pressure, in this case that of O2 in slowly flowing air, 1 atm.

Jan 1, 1970

By Werner Langguth

SINCE the introduction of the improved method of precipitating gold from chlorine solution by SO2 and H2S at the Golden Reward chlorination-works, Deadwood, S. D.,* this modern method has been further adopted in the chlorination-works of the Portland Consolidated Company at Deadwood, and in those of the Black Hills Milling and Smelting Company at Rapid City, S. D. It has proved practically most successful in the handling of large quantities of gold solution, and constitutes up to date, with Mr. John E. Rothwell's most important improvement, namely, barrel-leaching under hydraulic pressure, the principal progress made in gold chlorination. The method of refining the gold sulphides which result from this method of precipitation, was introduced by me in 1890 at the Golden Reward works, and in 1892 at those of the Black Hills Company. It has not suffered any changes during the last three years, and is substantially as described below:

Jan 1, 1895

By H. H. Wade, N. F. Schulz

The large quantities of iron-bearing materials, including taconite, semi-taconite," and other low-grade ferruginous materials occurring in Minnesota and elsewhere, constitute an important potential source of iron. Satisfactory grade and recovery of iron ore concentrate cannot ordinarily be obtained from these ferruginous materials by simple methods of beneficiation. Iron is distinctive in that the free metal and two of its oxides [magnetite (Fe,O,) and maghemite (gamma-Fe,O,) ] are strongly ferromagnetic. The successful magnetic separation of natural magnetite from taconite has already been established on a commercial scale. The iron in semi-taconite, how- ever, occurs largely as goethite (Fe,Os.H,O) and hematite (Fe90,) which do not respond to ordinary magnetic separation methods. Magnetic roasting converts these iron oxides to magnetite, which can, after liberation, be magnetically concentrated.

Jan 11, 1960

By John Gillie

Prior to the year 1902 electricity was used in the Butte district only for lighting, for the tramming of ores on the surface, and for the electrolytic refining of copper. In that year the Canyon Ferry hydro-electric plant on the Missouri river, with a transmission line to Butte and Anaconda, was completed, and enabled the mining operators to purchase electric current in large quantities at reasonable rates, and its application and use in the various mining operations and reduction works proceeded rapidly. The principal applications. of electric current in metal mining may be listed as follows: Compressing air for hoisting. Compressing air for rock drills and pneumatic tools. Pumping. Ventilating. Lighting. Tramming. Compressing air for blast furnaces and converters Running shop and miscellaneous motors.

Jan 9, 1913

By J. Wayne Erickson

One of the major problems facing today's mining industry is how to manage people and control costs in the underground mine. It is a problem with a solution. Because of the concerted effort to find and mine minerals near the surface, open-pit mine opportunities for certain minerals are becoming more limited; the mining industry will eventually be forced to produce more and more from underground mines in order to obtain those resources necessary to sustain our civilization. Although much technical progress has been made towards solving problems associated with the underground mine, such as - mine design, ventilation, rock support, equipment, and blasting techniques, little has been written on managing mining personnel. Much of what is being taught and practiced today about human relations, motivation, incentives, etc., applies to the underground miner, but the uniqueness of his group dictates a different treatment from that associated with the typical construction worker or factory employee. The difference lies with the kind of man attracted to underground mining and his working environment. Anyone who has had the responsibility of managing an underground mine would agree it is a unique problem.

Jan 9, 1976

By Frank Clowes

This lamp has been devised to burn oil from a flat wick in the usual way for lighting-purposes ; and also to burn a hydrogen-flame of standard size instead of the oil-flame, when delicate and accurate gas-testing is to be carried out. The change from the oil-flame to the hydrogen-flame, and vice versa, can be made with great rapidity, and without opening the lamp or running any risk in the presence of gas. The oil-flame serves for illumination; and when the wick is drawn down by the " pricker," so as to abolish the light, the pale blue reduced oil-flame serves to detect fire-damp or "gas," in any propor

Jan 1, 1894

By B. C. Craft

The outstanding event of the year 1932 in this area was the intensive drilling activity in the Zwolle field of Sabine Parish, Louisiana. More new development work was undertaken and completed than during the previous year. This was due in part to the increased price of oil and in a Includes 19 parishes: Beauregard, Bienville, Bossier, Caddo, Caldwell, Catn-houla, Claiborne, Concordia, DeSoto, Grant, Lincoln, Morehouse, Natchitoches, Ouachita, Red River, Richland, Sabine, Union, Webster. B H. K. Shearer: Oil and Gas Development in South Arkansas, North Louisiana and Mississippi in 1931. Trans. A. I. M. E. (1932) 98, 159. a Includes 14 counties: Ashley, Columbia, Dallas, Drew, Hot Springs, Lincoln, LnFayette, Little River, Miller, Ouachita, Pike, Sevier, Scott and Union. * H. K. Shearer: Oil and Gas Development in South Arkansas, North Louisiana and Mississippi in 1931. Trans. A. I. M. E. (1932) 98, 159. part to the fact that production is below local market demands. Exploration during 1932 resulted in the discovery of a new oil field and a new gas

Jan 1, 1933

By D. W. Frommer

Processing nonmagnetic taconites by selective flocculation-desliming and flotation requires large volumes of water. If impounded without treatment the effluents from these processes require excessively large areas for containment. Experiments conducted in the Bureau of Mines 900-lb-per hr pilot plant at the Twin Cities Metallurgy Research Center indicates that approximately 85% of the water needed to process Michigan nonmagnetic taconite could be reclaimed from the process itself. Water was reclaimed by the controlled addition of lime, sodium carbonate, and synthetic flocculant. As a result, turbidities were reduced to ?1000 ppm equivalent SiO2, while a Ca ion content of ?16 ppm was maintained in the finished effluent. Good-quality flotation concentrates were obtained with reclaimed water and, by means of some indirect comparisons, it can be concluded that the reuse of the water permits a savings of almost 2.0 lb per ton of NaOH, and probably as much as 0.25 lb per ton of fatty acid for total savings of 7.8-10.3 cents per ton of feed. These savings are nearly offset by an estimated chemical cost of 9.3[c] per ton for water treatment.

Jan 1, 1970

By Fortunato Pereira Gamba

The Department of Narino (formerly included in the Department of Cauca) is a narrow band about 170 km. (100 miles) wide in the southern part of the Republic of Colombia, near the boundary of Ecuador, as showu in the sketch-map, Fig. 1. Its capital is Pasto, a small city of 25,000 inhabitants; the pri~icipal towns are T?querres, Cumbal, Ypiales, Barbacoas, and Tumaco. The port on the Pacific ocean is Tumaco, and traffic in the interior is carried partly on the Patia river (steam navigation to the fluvial port of Barbacoas), and afterwards overland over poor roads by human bearers or on mule-back.

Jan 1, 1913

By Roger G. Rowe

In late 1980, Exxon Minerals Company performed rock mechanics testing on oriented 150 mm drill core from their 75Fi tonne massive sulfide deposit near Crandon, Wisconsin. Instrumented samples from depths of 300 meters indicate premining horizontal stresses in a north-south direction (parallel to pillar faces) to average 12,300 kPa, with the perpendicular plane yielding an average stress of 14,630 kPa. Rock strength versus sample size was compared using uniaxial compressive strengths from 47 mm, 95 mm and 150 mm core. Massive sulfide averaged 153,300 kPa, 139,845 kPa and 75,330 kPa respectively, while the hanging wall and foot- wall averaged 92,000 kPa, 76,560 kPa and 57,960 kPa respectively. Point load compressive strengths were calculated using formula suggested by both Hassani et al., 1980 and Broch et al., 1972. Values calculated using the Hassani formula closely resembled pre- existing point load and uniaxial compressive strengths, while values calculated using the Broch formula were 50 percent low.

Jan 1, 1982

By William M. Kester

INTRODUCTION The Coal Research Bureau of the School of Mines at West Virginia University is presently conducting laboratory-scale tests to determine the technical feasibility of beneficiating pulverized coal and coal fines with high-intensity electromagnetic fields. Interest in magnetic processes for cleaning fine coals was stimulated by results obtained by Yurovsky, et a1 in 1958.1 This work, while not new in concept,2,3 indicated that pulverized coal which had been thermally treated in a rotary drum in the presence of superheated steam and air underwent thermo- chemical reactions. Films of the ferromagnetic minerals magnetite (Fe2O3), hematite (Fe3O4), and pyrrhotite (FeS[3]) were reported to be formed on the surfaces of the pyrite grains associated with fine coal during the foregoing treatment at temperatures ranging from 120 to 360°C. After thermal treatment the coal was magnetically separated in an experimental magnetic device having a field strength of 10,000 oersteds.

Jan 5, 1965

By Arthur E. Granger

IN the early days of the science, and until the recent past, geologists worked as individuals or in small groups. Prior to 1930 perhaps the largest single group under one administrative head was the Geologic Branch (now Division) of the U. S. Geological Survey, which employed at that time (including temporary help) 100 to 150 geologists. Today that same unit employs some 1500. In industry some companies employ as many as 100 geologists in a single department. These numbers obviously pose a need for administration. The basic qualifications for good administration are the same for any group of human beings, but the administration of geologists presents some special problems. Choosing Administrative Personnel: There are two kinds of personnel needs: 1) technical, which requires professional geologists who have proved their capabilities in the field, and 2) clerical and fiscal, which provide the necessary supporting or housekeeping functions. This discussion will be concerned only with the first category, except to point out the need for competent and understanding help from clerical and fiscal people and close relationship between top administration, technical or professional personnel, and the clerical and fiscal groups.

Jan 7, 1957

By D. M. Hausen

This study identifies and describes various crystalline phases of the V205-Na20 system, and relates their properties to metallurgical aspects of vanadium production. Phase equilibria and stability ranges of sodium vanadate phases of varying molar ratios of Na20/V205 were investigated in a variety of plant products, ranging from fused "black cakes" (V20 melts) to "salt roast" calcines. Crystalline compounds, Including vanadium pentoxide, V205; sodium vanadyl vanadate, 6 phase, Na2O.V2O5.5V2O5; sodium vanadyl vanadate, y phase, 5Na20.V204.12V205; sodium metavanadate, Na20 .V 05; sodium pyrovanadate , 2Na20 .V205; and sodium orthovanadate, 4Na20.~2~5, have been characterized with the aid of X-ray diffraction patterns, infrared spectra, and optical properties in addition to chemical analyses, as a guide to mineralogical "troubleshooting" of plant problems and processes in vanadium pyro- and hydrometallurgy.

Jan 1, 1984

By William McCullouch

The method of determining moisture percentages in coal has been defined as purely empirical. The procedure, as defined, has been published in the U.S. Bureau of Lanes technical papers and approved by the American Society of Testing Materials but deviations from this established procedure are common in most commercial and private laboratories. It is not within the scope of this paper to discuss the deviations in common practice but rather to give a detailed account of the method in use in the laboratories of the United Electric Coal Companies. In general, moisture values are presented as surface moisture and, for lack of a better term, inherent moisture. The formula for adding them together to give total moisture is common knowledge. In practice, on high-moisture bituminous coal, it has been found that the line of demarcation between surface and inherent moisture is very indefinite, the inherent moisture being so loosely held that it is released far beyond its natural limits when the prescribed method of the A.S.T.M. for determination of surface moisture is followed. This is shown in Table 1 for two typical washed coals from Illinois.

Jan 1, 1938

[ ] (14) SCREENS: Description of Allis-Chalmers' complete line of vibrating screens for the mining industry is contained in a new 8-page bulletin. Primary scalping, secondary scalping, and conventional screens for wet or dry sizing and screens for heavy media separation are included. Also given is a typical fiowsheet showing how horizontally operated Low-Head screens are used in the sink and float process. (15) MILLS: Forty-six years of experience and 4000 installations throughout the world lie behind the seven basic types of mills illustrated in a recent bulletin from the Hardinge Co. Fields of application and materials handled in various installations are listed. (16) BLOWERS & COMPRESSORS: A brochure describing the manufacturing facilities and the axial and centrifugal blowers and compressors made by the Sawyer Bailey Corp. is now available. (17) LINATEX: The first catalog of the Linatex Corp. of America has been issued, outlining the advantages claimed for this special form of natural rubber, when used in corrosion, abrasion, and vibration resisting applications. (18) WIRE ROPE: Twenty-four pages packed with concentrated wire rope data is the way E. H. Edwards Co. describes a booklet which they are now making available. It was condensed from the Edwards general catalog to provide users with a concise guide to every important phase of wire rope production, maintenance, and use.

Jan 1, 1952

By D. E. Moore

The strength of a natural serpentinite gouge was measured at 400°C and an effective pressure of 100 MPa. The strength of the gouge decreased with increasing pore pressure to 50 MPa and then was nearly constant between 50 and 125 MPa. The samples at 50-125 MPa pore pressure slid stably, whereas those at 3-25 MPa pore pressure showed stick-slip behavior. Lengthening the pre-heating time to 72,000 s of samples at 100 MPa pore pressure led to increases in both the strength and the likelihood of sliding unstably. With still longer pre-heating times, the strengths decreased again and sliding once more became stable. The strength of the gouge at 3 MPa pore pressure was unaffected by changes in pre-heating time. A possible explanation for the results is that excess pore pressures are being generated in the gouge, causing the true effective pressure to be lower than the apparent value.

Jan 1, 1984