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By Richard S. Olsen

Prior work by the Bureau of Mines demonstrated a feed preparation method that eliminates the formation of slime during leaching of calcined kaolinitic clay and makes leached residues fast settling and easy to filter. Nitric acid leaching rates determined for calcined kaolinitic clay prepared by this method were found to correspond to a zero-order reaction model for both batch and continuous, stirred-tank leach-ing. A rate constant of 0.136 min-1 was determined. Separation of solid residues from the reacted slurry was examined, and filtration rates were determined. Permeabilities of the flocculated, leached residues were around 51 darcys, or 5.0 x 10-7 cm2 for laminar flow through 4-ft-deep beds.

Jan 1, 1983

By H. S. Caldwell

A magnesium-base incendiary alloy, containing about 20 percent cadmium, 4 percent aluminum, and 0.5 percent zinc, was investigated in a series of vacuum-distillation experiments to determine the feasibility of recovering magnesium and cadmium as refined metals. Alloys prepared in the laboratory and actual bomb-casing alloy were studied at temperatures of 550° to 750° C. and pressures of 100 to 150 microns. Simple distillation and fractional distillation methods were only partly effective in separating the cadmium and magnesium. They were separated satisfactorily, however, with a special vapor baffle designed to condense the metals selectively. Magnesium and cadmium products were 99 percent pure and together comprised 82 percent of the total condensate. About 17 percent of the condensate was intermediate-grade alloy that could be recycled with new charge and contained about 70 percent magnesium and 30 percent cadmium.

Jan 1, 1959

By F. P. Haver

Because State and Federal agencies have limited the amount of sulfur oxides that can be discharged to the atmosphere, most copper smelters plan to convert the S02 in offgases to sulfuric acid. In some cases, however, it might be preferable to use a nonsmelting method to fix the sulfur in the form of a discardable product. Research by the Federal Bureau of Mines has shown that sulfur in copper concentrate can be converted into insoluble anhydrite (CaS04) by roasting the concentrate with lime (CaO). After leaching the calcine to recover metal values, the residue may be discarded without harm to the environment. The process can use a rougher flotation product, thus reducing separation costs and saving valuable minerals (for example, molybdenite) that are now lost in making cleaner concentrate. In tests, rougher concentrate was pelletized with the theoretical amount of lime and roasted for 1 hour in a 6-1/2-inch-ID by 11-foot-long rotary kiln at 700° C. Sulfur retention was about 97 percent. Leaching the calcine with 20 percent RCI extracted approximately 99 percent of the copper, 73 percent of the iron, and 91 percent of the molybdenum. After the molybdenum was removed from the leach solution by adsorption on activated carbon, copper with a purity in excess of 99 percent was obtained by cementation on sponge iron. The strip solution then could be spray-roasted at 500° C to recover the RCI for recycle and obtain F2O3 as a byproduct.

Jan 1, 1975

By James Paone

Land utilized by the mining industry from 1930 through 1971 amounted to 3.65 million acres, or 0.16 percent of the land mass in the United States. Land reclaimed during the same period was 1.46 million acres, or 40 percent of the land utilized. This report includes data on land use for wastes from underground and surface mining, for wastes from mill operations, and on subsidence. Data on land use and reclamation were obtained from operating companies, mining organizations, appropriate State agencies, and others concerned with such activities. The 10 leading States in land used for mining in 1971 were, in decreasing order, Kentucky, Pennsylvania, Arizona, Ohio, California, Florida, West Virginia, Illinois, Minnesota, and Indiana. Mineral commodities accounting for a major portion of land use are, in decreasing order, bituminous coal, sand and gravel, stone, copper, phosphate rock, iron ore, and clay; for coal, these commodities are produced principally by surface mining operations. Reclamation over the 42-year period was largely on lands utilized for surface mining of bituminous coal. New surface mining methods, particularly for coal, incorporate some form of land restoration.

Jan 1, 1974

By T. F. Anstett

The Bureau of Mines evaluated the potential availability of chrysotile, amosite, and crocidolite asbestos from 42 properties in market economy countries. This resulted in the development of tonnage-cost relationships indicating the quantity of grades 3 through 7 asbestos at various average total costs of production at 0% and 15% rates of return on invested capital. The availability of grades 2 and 8 was also evaluated, but since each is produced at only one property, no analytical results were given. Total demonstrated recoverable chrysotile fiber potentially available of grades 3 through 7 from the 42 properties evaluated follow: 1.59 million t, 21.00 million t, 16.74 million t, 15.54 million t, and 19.27 million t, respectively. The total amount of crocidolite is 1.69 million t. Owing to the good potential for discovery and development of new deposits, long- term availability of fiber of all three types is not in jeopardy. However, many of the crocidolite properties evaluated in the northern Cape crocidolite field of South Africa have relatively small demonstrated resources, and new deposits will have to be exploited by the late 1990's to sustain projected levels of production.

Jan 1, 1985

By Charles Prasky

The Bureau of Mines investigated the conversion of nonmagnetic iron minerals to magnetic form through reduction Toasting operations. The primary objective was to obtain a concentrate that could be used as a direct shipping material for blast furnace consumption. Crude iron materials from the Steep Rock Lakes, Ontario, area were prepared into a blend of 8 parts siliceous ore, 3 parts pyritic ore, and 1 part tailings. Experimental work included laboratory reduction roasting tests, two continuous 10-day campaigns, and one 12-hour test all in a 34-inch by 36¬-foot rotary kiln. The objective of the project was achieved in producing an iron concentrate containing about 66 percent iron with over 90 percent iron recovery. Desirable operating conditions were developed in the kiln but optimum process variables were not completely established.

Jan 1, 1969

By B. I. Ferber

Toxic and explosive atmospheres are discussed, along with some of the instruments commercially available for their detection. No attempt has been made to evaluate the accuracy of anyone device. This circular has been prepared primarily to aid mine inspectors in selecting suitable instruments for underground gas detection.

Jan 1, 1972

Exposure to airborne respirable crystalline silica dust can lead to silicosis, a debilitating lung disease. On surface coal mining and construction sites, blast hole drills are notorious sources of airborne respirable dust that may contain significant amounts of silica. The drill operator and drill helper usually receive the greatest silica exposure compared with other occupations. As a result, many drilling operations have been, and still are, on more stringent dust standards. Drilling through various rock formations naturally presents a strong potential for silica dust generation for several reasons. First, drilling is a pulverizing process that generates large amounts of very small dust particles. Second, the bailing air used to flush cuttings from the hole leaves the hole at a very high velocity and can be difficult to contain. Third, many fixed shrouds used to enclose the area beneath the drill deck have a significant amount of leakage due to 1) gaps between the shroud and ground created by raising/leveling the drill, 2) gaps in the corner seams, and 3) tom deck shrouds. CONTROLS A dry dust collection system is typically connected to the drill deck to collect dust as the bailing airflow transports the cuttings (and significant amounts of airborne respirable dust) out of the drill hole. Deck shrouds are installed in an attempt to enclose the volume around the drill steel and prevent dust escaping. However, most deck shrouds are rectangular and constructed of four separate pieces of rubber belting attached to the deck. Because of this design, there is usually a significant amount of dust escaping from the open seams as well as the open area between the shroud and the ground. This dust can be a significant source of silica exposure to drill operators as well as other personnel downwind of the drill.

By Earl T. Hayes

For several years the Northwest Electrodevelopment Laboratory of the Bureau of Mines, in cooperation with the Air Materiel Command, U. S. Air Force, has been studying zirconium alloys. A preliminary survey of these alloys has been completed and reported as a Bureau of Mines Report of Investigations. 4/ Originally the purpose was to determine the suitability of zirconium alloys in medium-temperature applications. However, data also were obtained on other properties of these alloys, and later the scope was broadened to include amore detailed investigation of a selected group. The zirconium-titanium system was one of those chosen. The Bureau of Mines has been instrumental in the commercial development of both of these metals and has constructed pilot plants for the production of titanium at Boulder City, Nev., and for zirconium at Albany, Oreg. Both elements are in subgroup A, fourth series of the periodic table, and therefore have many properties in common. Since both have similar atomic structures and lattice dimensions the possibility of extended mutual solubility seemed likely. Inc transition-point diagram of Fast indicated that the two metals are completely miscible in all proportions in both the alpha and beta forms.

Jan 1, 1951

By A. Visnapuu

The Bureau of Mines, as a part of its goal to minimize occupational hazards associated with mining and mineral processing operations, has developed and field tested a compact exhaust air muffler for mechanized, jumbo-mounted pneumatic rock drills. The muffler is constructed of 1/8-inch sheet steel and has nominal dimensions of 1-3/4 by 9 by 13 inches. A directed air passage, flexible neoprene baffles, and an expandable slit-type outlet are incorporated to reduce drill exhaust air noise and eliminate muffler icing. Field tests in actual mining operations showed a l5-dbA reduction in exhaust noise and an 8-to 12-dbA reduction in overall drilling noise with no icing problems or decrease in drill performance. Data are presented on muffler construction, laboratory, and field test results.

Jan 1, 1979

By David P. Conover

The U.S. Bureau of Mines (USBM) has developed a computer-assisted Ground Control Management System (GCMS) for near realtime evaluation of underground coal mine ground conditions. The GCMS combines existing mine-monitoring system and sensor technology with automated computer analysis techniques to enhance the acquisition, analysis, and display of geostructural data. The GCMS, which combines mine structure data with other information, such as geologic conditions and mine layout, has provided information on mining-induced stress transfer and pressure buildup associated with several ground control events. The GCMS collects and analyzes shield-leg pressure, ground pressure, and strata movement data to evaluate the structural behavior of an active Western U.S. Iongwall coal mine. Field data are transmitted over a dedicated phone line to the USBM Denver Research Center (DRC) mine monitoring laboratory, 240 km (150 miles) from the mine site. Real-time collection, processing, and analysis of mine structure and shield pressure information has proved to be an effective method for near-face ground conditions while mining progresses. The GCMS provides the mine operator with information to rapidly identify and manage potentially hazardous ground conditions while mining is in progress.

Jan 1, 1994

By Harry W. Campbell

In 1984 and 1985, at the request of the U.S. Bureau of Land Management, the U.S. Bureau of Mines studied part of the Meadow Valley Range Wilderness Study Area (NV-050-156) in order to evaluate its identified mineral resources. The study area is located in Clark and Lincoln Counties, NV, about 50 miles northeast of Las Vegas, NV. The Johnston and Fitchett prospect, in the northern part of the study area, has more than 3 million tons of marginal perlite reserves suitable for many commercial uses. A preliminary mining feasibility estimate suggests perlite could be profitably mined from the study area; however, it is unlikely these perlite deposits will be developed in the foreseeable future because of unfavorable market conditions. Zeolite minerals occur in alteration zones adjacent to perlite deposits at the Johnston and Fitchett prospect, but high quality material is closer to potential markets. A metalliferous black shale unit containing 800,000 tons of subeconomic resources may extend into the study area at the Bradshaw vanadium prospect on the northwest boundary. Limestone, stone, sand, and gravel occurrences are wide-spread, but other suitable deposits in the region are more accessible to potential markets. Seven prospects in and near the study area were examined. The entire study area is leased for oil and gas exploration. A group of perlite placer claims covering more than 480 acres was located in the 1940's in the northern part of the study area. A small group of lode claims was located in the mid 1950's in the southwest part of the study area. No mining claims are currently (1985) held inside the study area. No mineral production is known from within the study area.

Jan 1, 1987

By A. W. Fahrenwald

"About two years ago the Bureau of Mines, Department of the Interior, and the University of Idaho undertook an investigation of classification in its relation to table concentration of Idaho ores. The cooperation of the management of the Bunker Hill & Sullivan Co. in placing at our disposal their West Mill and facilities as desired, offered an unusual opportunity for studying the field of hindered classification in its practical and economic relation to table concentration.It has been shorn theoretically, and demonstrated experimentally, that ore products are more easily and economically concentrated on tables if the natural feed, consisting of various minerals and of all sizes of particles of each mineral, be classified or grouped into a series of products in which the mineral particles of greatest density are small in diameter relative to the diameter of the mineral particles of lesser density. Products in which the maximum difference in diameter of light and heavy minerals occurs are to be obtained only by true hindered settling classification. To our knowledge there has never been a really good hindered settling classifier used in practice and the present tendency seems to be to by-pass any attempt at such classification.After a careful study of the nature of hindered classification and of the requirements for hindered settling in practice, a classifier has been developed that takes fullest practical advantage of the widely known, but generally only meagerly understood, condition of hindered settling so well analyzed a number of years ago by Dr. Richards.The present paper presents briefly some of the more important practical results accruing through the investigation."

Jun 1, 1924

By M. B. Bransford

A calculation procedure was evolved by the Bureau of Mines for determining the heat-transfer characteristics of dilute gas-solid mixtures in an externally heated tube. The procedure accounts for differences in gas and particle velocities and covers a range of particle sizes. Heat transfer coefficients obtained by the calculation procedure are compared with values reported in the literature.

Jan 1, 1970

By Manuel Gomez

Primary, low-temperature tars are generally known to alter with time. The effect is believed to occur, in some instances, without the external influence of air, light, or heat. Since one of the processes occurring during extended storage is oxidation, the action of mild oxidation induced by air and heat, in addition to the effect of storage, was studied. The principal effect in aging and oxidation is formation of pitch at the expense of the distillate fraction. The fraction boiling above 270° C. is mainly involved in pitch formation due to storage, whereas all fractions are affected to some degree when tar is heated at 125° C. in the presence of air. If the effects of air are considered, the aromatic and tar-acid fractions seem to be important in pitch formation.

Jan 1, 1956

By T. F. Mitchell, J. A. McAllister, S. J. Hussey

"INTRODUCTION During the Bureau's extensive program of investigating possible domestic sources of manganese, an are-dressing study was conducted in its laboratories at Salt Lake City, Utah, on a sample of oxide manganese ore representative of vein material from the Ophir Hill mine at Ophir, Tooele County, Utah. The sample (obtained by blasting down and mixing a portion of the vein) was submitted by the Ophir Development Co. of Ophir, Utah. As the ore was too law in grade to be acceptable for direct production of ferromanganese, it was tested to determine its amenability to concentration by ore-dressing methods.At the beginning of the investigation of manganese-ore beneficiation in December 1940, the only product marketable to Metals Reserve Company was ferrograde manganese, grade B, the requirements for which follow: Mn, min., 48 percent; Fe, max., 7 percent; Si02, max., 10 percent; P, max., 0.18 percent; A1203, max., 6 percent; Zn, max., 1 percent.Later, the specifications were modified gradually. As of May 15, 1943, manganese products were acceptable if they contained over 35 percent manganese and less than 3 percent zinc and 1 percent phosphorus. Prices were based upon material containing 48 percent manganese, 6.0 percent iron, and 11 percent silica plus alumina. Premium were paid for manganese content in excess of, 48 percent and iron content below 6 percent, penalties being imposed upon products containing less than 48 percent manganese or more than 6 percent iron or more than 11 percent silica plus alumina. The specifications for commercial manganese further required that maximum particle size be 12 inches and that 75 percent of the product be coarser than 20-mesh. Therefore, fine material, such as table and flotation concentrates, had to be nodulized or sintered. In addition, carbonate manganese ores were not acceptable unless calcined."

Oct 1, 1947

By R. F. Tenney

The performances of four anthracite-burning stokers have been observed under identical 74-hp. steam boilers. Fifty runs of 12 and 24 hours' duration were made in accordance with the test code of the American Society of Mechanical Engineers (ASME). The capacity of each stoker for burning anthracite has been determined, the heat efficiency at each fuel rate has been computed, and the various significant items of hear loss have been estimated. The operating data and results from each run are tabulated in this report in the form used in the test code. The heat efficiencies and most significant operating data for each run are also presented graphically for each stoker to establish the trends with increasing boiler outputs, The tests show that rice anthracite can be burned on stokers adapted to its use at heat-conversion efficiencies of 82 percent or more under continuous firing. These high efficiencies are maintained with fuel inputs 30 percent higher and lower than the peak efficiency rate. Moreover, a heat efficiency of 70 percent or more is obtained at 50 percent of the optimum fuel rate, even though the excess air into the furnace cannot be held below 150 percent.

Jan 1, 1960

The purpose of this study is to develop designs to facilitate and accelerate auger rotation stoppage (and auger rotation start up so as to promote auger disengagement during auger miner repositioning) and to provide a time delay and warning signal prior to auger start up to permit any miner s near the augers to get away from the augers before they start rotating. In the underground coal mines in the U.S., there are four auger miners that are currently in use. They are the Jeffrey 100L (see Figure 1-1) and 100M (see Figure 1-2), and the Wilcox WCM and the MK20A (see Figure 1-3).

Jan 1, 1974

By Walter G. Dupree

When the original version of this study was published in 1972 it was evident that a problem was developing on the energy scene. The ability of the United States to find the energy supplies it needed within its own boundaries--at least in the forms desired--was declining. Production of crude oil in the United States had peaked in 1970 and was declining slowly; environmental restrictions had begun to hamper the production and consumption of high sulfur coal; natural gas reserves were beginning to dwindle; and the development of nuclear power was proceeding more slowly than originally planned. Shortfalls in energy supply were being met through the importation of increasingly larger quantities of petroleum, but supplies were adequate and the price of the imports was below that of domestic production. The energy problem was more prospective than current. In October of 1973 the prospective problem became the "Energy Crisis' when the Arab petroleum exporting countries reduced crude oil production, imposed an embargo on the shipment of crude oil to the United States, and then raised the price of crude oil in a series of large steps. This crisis was a clear demonstration of the dangers of the dependence of the United States on imported petroleum, and of the Nation's vulnerability to the actions of the oil exporting countries. After the embargo was lifted, attention shifted to the immediate hardships resulting from the higher prices for gasoline, fuel, and electricity,

Jan 1, 1975

By F. E. Block, Robert R. Brown, A. W. Henderson

The chlorination of Cr₂ 03 (chromic oxide ) in the presence of carbon with CC14 (carbon tetrachloride ) and COCl2 (phosgene ) chlorinating agents was investigated by employing the radioactive tracer carbon By tagging carbon mixed with Cr₂ 0з , the chlorination reaction was evaluated in terms of the competitive reaction of the elemental carbon and the carbon contained by the chlorinating agent . A unique gas - analysis train was used to separate the chlorination product gases ; CO , CO₂ , and COC12 . The C¹ activity of the gases was determined and used to calculate the reactivity of each source of carbon . Reactivities were determined for the temperature range from 600 ° to 900 ° C. The results of the investigation show that each source of carbon reacts significantly with the Cr2 03 and that the reactivity of each form of carbon depends on the reaction temperature , and each form is independent of the other . Radioisotope and gas - analysis techniques are discussed and a description of the experimental apparatus is given .

Jan 1, 1964