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By C. H. Herty Jr, C. H.

FEW subjects have attracted the attention of metallurgists more than oxygen in steel. From the days of Mushet and Ledebui interest in this subject has been increasing, and as additional knowledge has become available, the problem has naturally grown more complex. Instead of using the simple term "oxygen" we now distinguish between iron oxide, silicates of various kinds, oxysulfides, oxygen as gas and oxygen in solid solution in steel. There are five general methods for determining oxides in steel: hydrogen reduction; vacuum fusion; various wet-extraction methods, including electrolytic methods; methods depending on volatilization of the iron away from the oxides; and metallographic methods. For oxygen in solid steel each of these methods has both advantages and disadvantages. The hydrogen-reduction method is of no use on steels above about 0.20 per cent. carbon; 1 furthermore, it gives only FeO and possibly some MnO. The vacuum-fusion method2 is expensive and gives total oxygen, with the exception of some A1203, and does not differentiate between the various oxides in which the oxygen exists. Most of the wet-extraction methods3 give only the more insoluble oxides SiO2 and A1203, though the iodine method gives MnO to an uncertain degree (information that may be more misleading then no information

Jan 1, 1957

By A. Tosun

Muckpile fragmentation formed by blasting depends on the specific charge factor, the discontinuities in the rock mass, and the rock strength. Determination of the discontinuity characteristics and rock strength is a long and difficult process. These two parameters are directly associated with the rock drilling speed. Therefore, it is the drilling speed of the machine used for the blast-hole, rather than the blasthole discontinuity characteristics and rock strength parameters, that is used in the prediction of muckpile fragmentation before blasting. Primarily, it has been suggested that the muckpile fragmentation values can be correctly determined by establishing correlations between the efficiency of the loader and muck pile fragmentation, since fragmentation is directly correlated with the former parameter. Subsequently, a correlation predicting the drilling speed of the drill machine was developed according to the discontinuity characteristics of the blasting surface and the rock strength. Finally, a correlation was developed predicting muckpile fragmentation according to the specific charge factor and the drilling speed of the drill machine The data was obtained by conducting blasting tests in two different limestone quarries.

Nov 30, 2022

By C. C. Hawes

SILICA is the main impurity in iron ore. It is intimately associated with the iron oxide, sometimes free but more often in the combined state, as a mineral silicate. Its separation and purification sometimes present difficult problems to the analyst. In the absence of any definite knowledge to the contrary, orthosilicic acid. H4SiO4, is supposed to be the only silicic acid made, all other forms, such as metasilicic acid, H2SiO3, representing different degrees of its dehydration. These acids are exceedingly weak but form the most stable compounds found in nature. They are known as the silicate minerals and are formed by the combination of the different metallic oxides

Jan 1, 1936

Energy benchmarking is widely applied across industries to determine the potential to improve energy performance. Unlike the many technologies for which energy benchmarks and efficiency rating systems are already in maturity, benchmarking of mining processes is still in its infancy. Benchmarking energy usage in mining operations, where energy costs are high and represent a significant portion of overall operating expenses, is challenging due to the uniqueness of each mining operation. Mines vary in terms of geology, geographic setting, ore body geometry, mineralogy which impact the mining method, material handling, processing and waste management. In order to gauge the opportunity for reducing the energy intensity of individual operations and also to compare the energy performance of operations on a global scale, the deployment of new benchmarking methodologies, models and frameworks is necessary. As a step towards the establishment of an accurate framework for benchmarking the energy consumption of mining operations, comminution, one of the more energy intensive mining sub-processes, was selected as the focus of a new energy benchmarking method. The methodologies and processes used to onset fragmentation in a rock mass to the crushing or grinding of rock to a size that is suitable for economic extraction are predominantly dependent on the ore properties. For this reason, site specific factors, such as the size reduction requirements and ore hardness were included in an energy benchmark model so that the energy performance of comminution processes at different operations could be normalized and compared on a global scale. Single particle compression breakage has been identified by several prominent researchers in the field of comminution as the upper limit of energy utilization in size reduction processes. For this reason single particle compression breakage was proposed as the basis of a work index for ores to be used as an input for the benchmark model. Overall, the new method showed that the energy benchmark for mineral comminution can be normalized and subsequently compared for a range of mining operations once the ore hardness has been appropriately characterized.

Aug 1, 2013

By Liu Y, Campbell K. R

The paper shows how breakage parameters may he extracted from laboratory batch grinding results and how they may used with reference full-scale hall mill circuit data to estimate the likely size distributions of values and gangue in a full-sca

Jan 1, 1997

By Jin Dai, Xianwen Geng, Hao Liu, Pu Wang

To investigate how deformation failure occurs in roadways surrounding rock, the relationship between cohesion and plastic shear strain of the strain softening model and the equation for calculating the shear strain of a rock mass in the ultimate elastic state are derived. On this basis, the equality relationship between the built-in maximum shear strain increment and cohesion of FLAC 3D was established to give a more intuitive picture of how the cohesion of the roadway surrounding rock changes. The cohesion attenuation and deformation of the surrounding rock are analysed. The results show that significant deformation in the roadway surrounding rock was caused primarily by the development of large areas of highly softened plastic rock masses towards residual strength. Taking the floor overhead-mining roadway under different rock pillar thicknesses (RPTs) in the Xinglongzhuang Coal Mine as an example, the results demonstrate that investigating the cohesion distribution inside the roadway during mining operation can provide a more intuitive, more accurate description of the degree of failure of the surrounding rock at any point of the roadway, as well as the overall failure range of the surrounding rock. The simulation agrees well with the field monitoring result and seems to be more practically useful than simply analysing the coverage of shear plastic zones. Based on the failure range and degree of roadway surrounding rock with different RPTs, three support schemes are designed. Classified support was implemented for roadways under different RPTs, which realizes the effective control of roadway surrounding rock.

Jan 16, 2022

By D. Asefi

A new method to detect microstructural features such as recovery and recrystallization as well as cold rolling reduction in low carbon steels was developed based on magnetic hysteresis loop measurement. To this aim, a hysteresis loop measuring apparatus, specifically designed and assembled for plate samples was employed. It is shown that maximum field (Hmax) of hysteresis loop, measured at constant maximum flux density (Bmax) of 0.5T, is an adequatemagnetic property to monitor different stages of changing microstructures during annealing.

Oct 1, 2011

By P. Tsang

In order to deal with ground control problems such as roof falls, floor heaves and pillar failures in underground coal mines, a new pillar design method based on the "yield pillar" concept is proposed. Using the finite element model simulation, the functions and mechanisms of the "yield pillar" are studied. The important variables that affect the stability of longwall entry-pillar system are identified. To simplify the geological and mining conditions, a new pillar design method classifies the in-situ roof and floor conditions into four categories: 1) strong roof and strong floor, 2) strong roof and weak floor, 3) weak roof and strong floor, and 4) weak roof and weak floor conditions. The design formulae are derived based on the finite element model simulation, stability study and nonlinear regression analysis. The finite element models used consider the plastic failure properties and time-dependent behaviors of rock. To better organize the finite element model simulation, the orthogonal experiment design is used to arrange the finite element models and proved to be very effective. An application example is used to illustrate the basic design procedures involved in the new pillar design method.

Jan 1, 1993

By Frederick C. Hull

THE grain size of a metal or alloy is one of the most important factors determining its properties. In steels, for example, grain size affects hardenability, toughness and machinability; in brasses, grain size is related to hardness and deep-drawing quality. In the field of heat-resistant alloys, grain size has a marked effect on ductility, creep and endurance strength. In order to determine these effects, as well as to control the properties of materials, many accurate and rapid measurements of grain size must be made. This paper presents a new and improved method for the estimation of grain size. USUAL METHODS of EVALUATING GRAIN SIZE A frequently used method of estimating grain size is that of comparing the image of a polished and etched specimen on the ground-glass screen of a metallographic microscope with standard grain-size charts. Several types of standards are available for use with different classes of microstructures. Geometric Grids.-The Metals Handbook1 has a series of hexagonal grids ranging in size from ASTM No. I to 8. Idealized Grain Networks.-Idealized grain-boundary networks for ASTM grain sizes I to 8 are included in the American Society for Testing Materials Tentative Standard E19-39T. Standard Micrographs.- The Metals Handbook and ASTM Tentative Standard EI9-39T contain micrographs of hypoeutectoid and hypereutectoid steels ranging in grain size from No. I to 8. The grain size of annealed brass (diam¬eter of the average grain in millimeters) is obtained by comparison with 10 micrographs of varying grain size in ASTM Tentative Standard Es-39T. A handicap to accurate evaluation of grain size by this method is the fact that it is difficult to compare photographs in a dimly lighted room with the image on the ground-glass screen, or, if the general illumination is increased so that the printed standards may be clearly seen, the contrast of the image of the unknown is decreased. It is easier to estimate grain size by comparing a micrograph of the unknown with the grain-size standards. However, photographing every specimen on which the grain size is desired is too costly in time and materials to be practicable. For hardened steels, the Shepherd or Jernkontoret fracture grain-size standards are very accurate and useful, but this method obviously cannot be applied to ductile alloys such as brass, stainless steels and austenitic heat-resistant alloys. Jeffries' method for grain-size measurements consists of counting the number

Jan 1, 1947

By H. W. Hitzrot, R. A. Limons, L. V. Fegan

The authors have developed and tested a new method for measuring pellet-bed temperatures in the traveling-grate or the shaft furnace. This method-using silver-palladium alloy wires as indicators-is less costly and less time-consuming than existing methods. Silver palladium wires, having specific melting points in the 2000° to 2500°F range, are enclosed in ceramic capsules. Each capsule is placed in a nichrome wire basket filled with a sample of green pellets, the baskets being the means for recovering the capsule after firing. After the encapsulated wires have been exposed to the firing cycle, the alloy wires are examined to determine the maximum temperatures attained by the pellet sample. This gives accurate, rapid determinations of maximum temperatures attained during pellet induration in either the traveling-grate or shaft furnace.

Jan 6, 1965

By Jorma Miettunen, Reijo Kalapudas, Pertti Koivistoinen

A new method for measuring the mill filling was developed by Outokumpu’s Pyhäsalmi concentrator during 1989-90. The method utilizes the power draw oscillation which is caused by the mill lifters. Each lifter bar causes a peak in the power draw and thus a continuous oscillation results. In a fixed time scale, the oscillation peaks will shift as the lifter bare hit the mill charge sooner or later depending on the volumetric filling of the mill. Thus the measuring method is based on the phase shift of the power oscillation. So far the measurement is utilized for maximizing throughput of the primary mills at Pyhäsalmi and Enonkoski concentrators and at Harjavalta slag concentrator. The paper describes the new method and the results achieved.

Jan 1, 1992

By Dominique François-Bongarçon

A new method for open-pit design has been devised by G. MATHERON and the writers: it replaces the search for an optimum contour by the determination of a parametrizing function. The isovalue curves of this function give the optimum pit design corresponding to varying economic parameters; The method is described and indications are given about the corresponding program. Simulated data have been processed by the program and by a standard program using LERCES-GROSSMAN graphical method: the comparative results are described.

Jan 1, 1977

By Z. Zak Fang, P. Fan, S. Middlemas

"Titanium dioxide (T1O2) has been widely used as pigment in paints, paper and cosmetic products, as well as high-tech applications such as PV Cells, semiconductors, biomedical devices and air purification. T1O2 pigment is primarily produced by the high temperature chloride process, resulting in considerable CO2 emissions. A novel hydrometallurgical process for making T1O2 pigment without direct CO2 emission is investigated. The new method promises to eliminate direct CO2 emissions, consume significantly less energy, and produce minimal environmental waste. The novel process involves molten salt roasting of titania slag, with subsequent washing, leaching, solution purification, hydrolysis, calcination and post-treatment stages, resulting in high-purity anatase or rutile pigments while realizing significantly reduced environmental impacts. Pigment whiteness is critically sensitive to trace amounts of discoloring impurities such as iron and chromium. Several methods for reducing the levels of these impurities are investigated. Energy consumption and emission models are also developed.IntroductionTitanium dioxide (T1O2) is one of the most commonly used minerals in the chemical manufacturing industry. It has been commercially processed since the early 1900's, and has a wide variety of applications. Pigment is used in paints [1], plastics and paper [2], sunscreen [3], cosmetics and even as a food additive [4]. T1O2 has also been used in photovoltaic cells [5], biomedical devices [6], and in air purification [7]. T1O2 pigment has a refractive index of 2.7, which imparts a high level of opacity (and hence whiteness) to whatever material it is added [8]."

Jan 1, 2012

By R Markoski, P Grealish

The requirement for rapid vertical development for underground ventilation is often a factor when dealing with dynamic mine plans, with short vertical developments being used to optimise ventilation systems. In an effort to increase the safety and efficiency of the constructions, a simple and effective sinking methodology is required that is both adaptable and repeatable. A modified shaft construction methodology is proposed that attempts to minimise risk to the personnel as well as be cost-effective. Readily available equipment is used to ensure adaptability to the various environments and shaft parameters.One of the greatest risks of shaft sinking is having personnel working suspended over open cavities or underneath suspended loads. Removing this risk, by ensuring all construction is done from solid ground, allows for safer sinking operations. As the process is repeatable, familiarity and confidence in its construction sequence will increase with each successive sink.A trial sink is performed with a 3.6 m diameter, 20 m deep shaft. The shaft was excavated using a conventional strip-and-line philosophy, with the shaft then being lined from the collar via the use of large diameter corrugated steel culverts. The annulus between the steel culverts and shaft excavation is then filled with a concrete mixture to secure it in position.The new process was successful, with no personnel at any time during the process being suspended above an open excavation. The installation had relatively low capital and operational costs and was completed faster than an equivalent, conventional concrete-lined shaft construction. Therefore when compared to conventional shaft-sinking methods, this process can be considered safer, more efficient and relatively cost-effective.Further research is required to determine whether this method can be expanded to larger vertical developments.CITATION:Markoski, R and Grealish, P, 2014. A new method for rapid vertical development of underground ventilation shafts, in Proceedings 15th Australasian Tunnelling Conference 2014 , pp 603–606 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Sep 17, 2014

By Laihua Wang, Peter Hayes, Hae-Geon Lee

"This paper introduces a new process for the efficient removal of dissolved gases and inclusions from liquid metals. This process involves the creation and dispersion of fine bubbles in molten metals by introducing inert or reactive gas into a region of turbulent flow. The highly turbulent metal flow splits the gas into fine bubbles and results in good mixing between the gas and molten metal phases. These conditions are ideal for contacting inclusions in the metal with the bubbles and subsequent flotation of the inclusions to the metal-slag interface where the inclusions are then absorbed by the covering slag layer. Dissolved gases, such as [H], [0], [N] in the metals are also transferred to the gas bubbles and removed from solution.The process concept has been previously demonstrated using a full-scale air/water model to simulate the ladle-to-tundish system of continuous casting of steel. The present cold modelling work has further demonstrated the ability of the process to remove gas solutes. The results indicate that the efficiency of new process is several hundred times greater than that of conventional high speed rotating injectors which are currently applied in the treatment of liquid light metals.IntroductionDuring metal smelting, refining and alloying processes, unwanted gas and second phase liquid or solid impurities are incorporated into liquid metals. In the case of steelmaking, the gas-forming impurities include [0], [H] and [N], and the solid impurities as a result of deoxidation include Ah03, Si02 inclusions. Common impurities in liquid aluminium are dissolved hydrogen and solid Ah03. To avoid subsequent problems during processing and to improve the physical properties of the metal products it is necessary to significantly reduce the level of impurities."

Jan 1, 1996

By E. Bonsall, J. J. Brummer, A. R. Graham

"A method and device are described for sampling diamond-drill core by cutting a continuous fillet of constant cross section from the cylindrical surface of the core throughout appropriate sample lengths. The apparatus employs a tapered, abrasive-set, cutting wheel, the conical cutting surface of which projects slightly into a rectangular core-guiding trough set parallel to the axis of rotation. The depth of fillet and thus the amount of sample per unit length can be regulated by adjusting the core guides. The freshly cut fillet itself, by engaging in a guide beyond the cutting wheel, acts to prevent rotation of the core during operation of the device.The cuttings which form the sample are normally collected in a tray below the cutting-wheel and appear at about 80 per cent -100 mesh. They require little or no further treatment or comminution before analysis. Speed, economy and convenience of sampling are thus greatly increased as compared with conventional sampling by im-1>act breaking or sawing, followed by crushing, grinding and sub division for assayAssays from fillets (about 1/20 the cross-sectional area of the core) and from 180-degree segments, from the same ninety-three core-samples, representing 431 feet of nickel-copper mineralization, gave the following results:"

Jan 1, 1968

By B W. Atkinson

Full-stream mechanised sampling apparatus, that collect a full cross-sectional increment from the complete screen discharge, will always be the preferred option for sampling screen overflows. However, the reality is that provisions for automated sampling are rarely, if ever, provided at the discharges of individual screens within beneficiation plants.Sampling from the discharge of high capacity vibrating screens, especially multi-slope screens, is subject to sampling bias, due to the stratification of the ore that occurs on the vibrating screen deck. The stratification in the vibrating bed translates to a stratified falling stream at the discharge end of the screen, typically with smaller particles at the back of the falling stream and large particles at the front of the falling stream (Figure 1).The chemical and physical characteristics of heterogeneous ore (mineral or coal) particles vary significantly with particle size. If samples do not correctly reflect the source material size distribution, they will be biased and the resulting analytical/assay data will not reflect the actual physical nor chemical characteristics of the source material.Prior published data for coal preparation research (Australian Coal Association Research Program) has demonstrated that a bias appears to exist for samples collected from high capacity multi-slope screens.A new form of sampling scoop has been developed with the aim of overcoming this issue.Bias was evaluated at a coal preparation plant by comparing the desliming screen overflow size distribution to that for æreferenceÆ coal preparation plant feed samples collected using the recognised stopped-belt technique. The study procured 20 sets of comparison samples in order to ensure statistical relevance.Two forms of sampling device were employed for the multislope screen discharge.A conventional square aperture scoop was demonstrated to exhibit a significant coarse bias, in that the resulting samples exhibited a significantly coarser size distribution compared to the reference samples. In other words it was evident that the conventional scoop æfavouredÆ material from the front of the falling stream.A new æcollapsibleÆ sample scoop was evaluated in parallel, and its samples were found to exhibit no relevant bias.CITATION:Atkinson, B W and Swanson, A R, 2012. A new method for sampling from high capacity screens, in Proceedings Sampling 2012 , pp 89-94 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 21, 2012

By I. G. Ediz, D. W. Dixon, W. M. Fidler

In this paper a new method for the arresting of tunnel explosions is presented. In the proposed technique, the on coming explosion is detected by a pressure sensitive device by a pre-determined rise in static pressure. The sensor then triggers a mechanism which causes the explosion door to be closed in a specially constructed concrete barrier zone. The doors are of a special construction and consist of perforated steel plates that allow part of the blast wave to be transmitted but do not allow the passage of the flame. A number of design parameters have been identified, including: the likely amplitudes of the transmitted/reflected pressure waves that would govern the explosion door pressure loading; thickness of the perforated steel packages; perforation dimensions; heat transfer across the door and other factors.

Jan 1, 1995

By A. L. Bleloch, A. M. Starfield

This paper is concerned with heat flow in the plane of a typical cross-section of a deep underground airway. A new algorithm, called the quasi-steady method, is presented for the calculation of rock temperatures in that plane. The algorithm is used in the computation of heat and moisture transfer rates from the rock to the ventilating air for an airway that is wet on part of its circumference and dry elsewhere. The speed and accuracy of the new method are demonstrated on a microcomputer, and it is argued that this method offers a considerably more versatile and physically meaningful alternative to previous methods for the prediction of increases in air temperature along mine airways. The algorithm is also used to explore the concept of a uniformly wet airway that is equivalent to a partly wet airway in terms of its effect on the ventilating air. The concept is shown to be reasonable, but more complex than one might have anticipated. Finally, several useful extensions and applications of the new method are suggested.

Jan 1, 1983

By George P. Demopoulos, Vladimiros G. Papangelakis, Dimitrios Filippou, A. J. Monhemius, G. W. Warren, E. Peters

A new method developed for the estimation of the activity of Ht in mixed sulfate solutions is described and examples of application of this method to the system H2SO4-ZnSO4-FeSO4-Fe2(SO4)3 from 298 to 473 K are offered. The method makes use of an "extended Debye-Hiickel" type of equation that was originally put forth by Das for pure H2SO4 solutions at ambient temperature. The treatment of mixed sulfate solutions was made possible by combining that equation of Das with a speciation algorithm which calculates the abundance of all species formed. The developed method, which also takes into account ionic strength and temperature effects, was used to generate hydrogen ion activity and speciation data for all possible acid/metal sulfate pairs of the system H2SO4-ZnSO4-FeSO4-Fe2(SO4)3. Finally, under the light of the reported data, specific examples of hydrometallurgical reaction systems are analyzed in terms of thermodynamics or kinetics. In particular, the systems discussed are: hydrometallurgical precipitation of hematite, solvent extraction of Fe(III), acid leaching of zinc ferrite, and oxidation of Fe(II) to Fe(III) by O2(aq).

Jan 1, 1993