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By William G. Ryan, David S. Graham, Dan A. Brown, Rich A. Lamb, Paul J. Axtell

"The St. Croix River Crossing project on the Minnesota-Wisconsin border has been in the process of planning and public debate for two decades, with several changes in alignment. During the course of the earlier planning process in 1995, a drilled shaft load test was performed to obtain preliminary design information. There were some difficulties in maintaining stability within the weak sandstone bearing formation, and the measured axial resistance was relatively low. Subsequent experience by the Minnesota Department of Transportation with similar weak sandstones on the I-35W project suggests that improved construction techniques using modern drilling fluids may offer opportunities for improved performance. During final design in 2012 a second load test program was performed of a full scale test shaft constructed using polymer drilling fluids. The stability of the socket excavation in the weak sandstone appeared to be greatly improved and the measured axial resistance significantly higher.This case history illustrates the excellent performance that drilled shafts can provide in even relatively weak sandstone bedrock as well as the profound influence on axial resistance associated with the construction techniques used. The improved resistance values obtained by the new load test with more recent construction technology allowed the foundation scheme to be substantially optimized with respect to the number and size of required drilled shafts, reducing the size, cost, and risk of the coffercells and footings.IntroductionThe Minnesota Department of Transportation (MnDOT) has awarded the first phase of a bridge construction project that will cross the St. Croix River between Oak Park Heights, MN and St Joseph, WI. The first phase construction contract involves building the river pier substructures including groups of drilled shafts beneath each tower leg. A general location of the bridge project is provided in Figure 1.Prior to award of the construction contract, two separate design-phase axial load tests were performed on non-production drilled shafts with rock sockets. Both tests were static, bottom-up tests using the Osterberg Cell (O-cell). The first test was performed in 1995 when final design and construction was thought to be imminent. After years of public debate and literally, an act of Congress, design of the project was finally restarted and a second load test performed in 2012. The 1995 test was conducted on the Minnesota bank approximately 900 ft southwest of the St. Croix River bank. The 2012 test was conducted in the river about 2,100 ft northeast of the1995 test location. A plan-view of the project indicating the test program locations relative to the bridge alignment is provided in Figure 2."

Jan 1, 2015

By Swaminathan Srinivasan, Aaron J. Muck

"When an opportunity arises to combine state-of-the-art concepts with advanced modeling tools, engineers need to take what they know and apply forward thinking to geotechnical solutions to promote the state-ofpractice. Such an opportunity was seized during the design and construction of the Great American Tower in Cincinnati, Ohio. The forty-one story Great American Tower at Queen City Square – currently the tallest building in Cincinnati – has not only changed the downtown skyline, it is also contributing to the advancement of the state-of-the-art use of auger cast-in-place (ACIP) piles as settlement reducers. Predicted settlements of a traditional mat foundation were excessive, and the costs and construction time associated with traditional ACIP piles extending to bedrock were not preferred. A mat supported on a limited number of ACIP piles, with the piles primarily acting as settlement reducers, was evaluated as the preferred foundation type.Promoting the unique soil-structure interaction of the foundation system with confidence required the use of sophisticated numerical modeling tools. Traditional standard penetration test boring data (SPT) was initially used to develop a numerical analysis of the soil-structure interaction using FLAC 3D software. The model was further modified with cone penetration (CPT) and pressuremeter testing (PMT), along with actual load test results on several ACIP pile elements of varying lengths, but all tipping above bedrock. Through a combined design team effort, and detailed numerical modeling analysis, ACIP piles were recommended for reducing mat foundation settlement. Instrumentation during and post-construction confirmed design assumptions and predictions. Integrating sound geotechnical concepts, and using advanced geotechnical analysis and design methods, traditional mat and ACIP pile foundations were successfully integrated into a unique foundation support system.INTRODUCTIONThe Great American Tower at Queen City Square in Cincinnati, Ohio is located within a region dissected by historical geologic deviances associated with the meander of the Ohio River and glacial progression/recession. Combining a challenging geology, with the development of a high-rise office building afforded the design team an opportunity to combine state-of-the-art soil-structure interaction concepts and method with traditional geotechnical engineering concepts. Such a combination required a variety of field tests, collaboration with the design team and owner, and geotechnical-structural modeling during the design phase. During construction, in addition to materials testing and observation, a variety of instrumentation systems were employed. Together, the data was used to corroborate the design model and make adjustments during construction and further substantiate design assumptions following construction."

Jan 1, 2015

By Jiann-Yang Hwang, Ying Qin, Shu-Jing Zhu

Metallurgical Oil Sludge (MOS) is a byproduct created in the process of steelmaking. More than a million tons of MOS are generated each year throughout the world. The material contains hazardous components such as heavy metals and pathogenic organics, which can cause serious environmental problems and health issues. Landfill, combustion, and pyrolysis have been investigated for the disposal of MOS. However, these methods are unsatisfactory since they are unable to reach the clean environment goal. In this study, we investigate the possibility of using MOS as a reductant in a high temperature metallurgical process. The results are reported and discussed.

Jan 1, 2015

By M. Jahazi, P. P. Bhattacharjee, K. Chadha

The present work investigated the effect of strain reversal during high pressure torsion on the evolution of microstructure, texture and hardness properties of two different materials with different dynamic recovery behavior, namely, high purity (99%) Aluminum (2N-Al) and Aluminum-Magnesium (Al-2.5%Mg) alloy. In the two aluminum alloys subjected to different routes, the evolution of the ultrafine structure followed same trend. At lower strain level, sub grains with prominent LAGBs network were observed and at higher strains, ultrafine equiaxed grains separated by HAGBs were observed throughout the disk. The texture evolution in monotonically and strain reversal processed 2N-Al and Al-2.5%Mg showed presence of typical torsion texture components at different strain levels. The strength of the components was observed to follow different trends depending on the processing routes.

Jan 1, 2015

By Guangwei Wang, Changle Zheng, Yifan Chai, Jian Guo, Weiwei Geng, Jianliang Zhang

In this paper, characteristic and kinetics of CO2 reaction with four different kinds of coke such as top-loading coke, dry quenching tamping coke, wet quenching tamping coke and semi-coke were investigated based on isothermal method. Electric resistance reduction furnace was used to heat the sample. Volume Model (VM) and Shrinking Core Model (SCM) were used to calculate the kinetic parameters and to contrast with the experimental results. The results showed that the Volumetric Model (VM) was much suitable for the reaction of top-loading coke, dry quenching tamping coke and wet quenching tamping coke, while Shrinking Core Model (SCM) was much suitable for semi-coke.

Jan 1, 2015

By Manjie Li, Mingrui Yang, Haijun Peng, Shuxing Qiu, Wei Liu, Shengfu Zhang

It is important to produce and utilize highly reactive coke in order to reduce the energy consumption and CO2 emissions through improving shaft efficiency in blast furnace. The present study aimed to investigate the transformation of iron minerals and properties of iron coke (the coke mixed iron ore fines). Along with the increase of iron ore fines, cold strength displayed a slight downtrend and the pore structure wasn’t inferred to be a major factor affected the properties of iron coke. During carbonization, the majority of mixed iron oxides were reduced to metallic iron by CO and H2 and the degree of metallization achieved to approximately 75%. Nevertheless, produced metallic iron was oxidized by pure CO2 during gasification. Iron coke reactivity index (ICRI) was obviously enhanced and the iron coke strength after reaction (ICSR) drastically decreases, which were also significantly influenced by crystal structure of carbon.

Jan 1, 2015

By Jian Li, P. Liu, R. Zhang and J. Lo

In the past decades, focused ion beam (FIB) has evolved into a powerful microscope that provides capabilities that no other microscopes can offer. The combination of high-resolution imaging and stress-free ion beam cross sectioning provides valuable microstructure information both at the specimen surface and beneath. FIB techniques are also the preferred method to prepare site-specific transmission electron microscope (TEM) specimens. CanmetMATERIALS owns a world-class microscopy facility, where advanced microscopy work provides strong supports to research programs that cover a wide range of subject areas. This paper is aimed to provide a few practical examples of FIB applications in microstructure characterizations that include cross-sectioning and imaging, serial sectioning, and advanced TEM specimen preparation in materials research at CanmetMATERIALS.

Jan 1, 2015

By Xu Zhang, Xuewei Lv, Guibao Qiu

Slag foaming phenomenon is of vital importance to the mass and energy transfer in metallurgical processes. A considerable extensively studies carried out via out-gas in the past cannot simulate well the foaming phenomenon formed in the blast furnace where high TiO2 iron ore is used. A gas reaction was designed in the water-glycerol system to simulate the inner-gas system. This study investigated the influences of solution viscosity, particle concentration and particle size on foaming caused by endogenetic gas. The results show that the foaming height decreases with the increase of solution viscosity, which means reduced foaming ability, more difficult foaming elimination process and prolonged time for natural defoaming. With increasing the solid particle content, the foam height presents a trend which increases firstly and then decreases. Under a certain solid particle content, foaming height decreases with the increase of solid particle size, indicating a weak foaming ability.

Jan 1, 2015

By Yongqi Sun, Zuotai Zhang

Our study investigated the influence of P2O5 and B2O3 on the viscosity and crystallization behavior of Ti-bearing blast furnace (Ti-BF) slags for the purpose of Ti extraction. The investigation of the crystallization behaviors were carried out using a single hot thermocouple technique (SHTT) and the viscosity was obtained by rotating cylinder method. For the viscosity, the results showed that P2O5 substantially increased the slag viscosity. P2O5 is a network-forming oxide, which increased the degree of polymerization of slags and accordingly increased the slag viscosity. However, both of slag viscosity and apparent activation energy for viscous flow remarkably decreased with B2O3 addition. As a typical network forming oxide, B2O3 was introduced into the network and existed dominantly as 2-D structure, BO3 triangular, which caused a simpler structure and a decreasing slag viscosity. As for the crystallization behaviors of Ti-BF slags, both P2O5 and B2O3 enhanced the crystallization trend of rod-shape rutile and suppressed the crystallization trend of dendrite CaTiO3. Therefore the added P2O5 and B2O3 caused the primary phase change from CaTiO3 to rutile. Additionally, it was found that the rod-shape rutile showed a 1-D growth, whereas the dendrite CaTiO3 showed a 3-D growth style.

Jan 1, 2015

By Dany Racine, Daniel Marceau, Denis Laroche, Dmitry Lukovnikov

Carbon base materials play a critical role in the performance of Hall-Héroult cell. The determination of their thermo-physical properties is of primary importance for modeling and designing complete cell systems. However, overcoming the associated experimental hurdles is complex and often underestimated. Of them are the Poisson’s ratio measurements and the continuous oxidation/burning of the materials at temperatures above 200°C. The novel procedure developed in this research is based on the Gleeble® 3800 system. Its vacuum chamber allows test with a chosen atmosphere at temperature of more than 1000°C. Young’s modulus, Poisson’s ratio and the coefficient of thermal expansion values can all be adequately measured using a single test. Cylindrical carbon samples (: 50mm, L: 100mm) were tested in the modified system at temperatures ranging from room to 950°C without any trace of oxidation. The resulting values were also in good agreement with literature data for a specific graphite material.

Jan 1, 2015

By Run-sheng xu, Hai-yang WANG, Di ZHAO, Teng-fei SONG, Jian-Liang Zhang

This paper was mainly focused on the different semi-cokes and charcoal which could be new fuels for blast furnace injection. Through the comparative study with bituminous coal and anthracite coal, the properties of semi-cokes and charcoal were presented in this research. 10 indexes of different fuels were obtained by different standard experiment, including proximate analysis, ultimate analysis, igniting point, explosivity, transportation characteristic, ash properties, grindability, calorific value, combustibility and reactivity with CO2. According to the data analysis, it provided a theoretical basis for rational utilization of various blast furnace fuels, and helped to broaden the scope of the blast furnace injection fuels. This research could contribute to energy conservation, emissions reduction, and sustainable development of iron and steel enterprises.

Jan 1, 2015

By Tao Zhang, Wen-tao YU, Hai-bin ZUO, Jian-Liang Zhang

Sintering-pot tests and metallurgical performances of sinter with 4 kind of different Al2O3 contents are experimented in this paper. Results show: when the Al2O3 contents increase from 2.0% to 3.5%, acicular calcium ferrites in mine phase will be gradually replaced by plate-like iron calcium. The increase of Al2O3 contents will lead to the addition of liquid viscosity and the reduction of permeability of sinter bed. Sintering time will be prolonged. The rate of yield is stable basically but production is low; besides, the increase of liquid viscosity will decrease of drum strength. The change of permeability of the material layer will make RDI +3.15 decrease first and then increase when Al2O3 contents changed from 2.0% to 3.5%. RI of sinter shows a contrary trend because many open voids are formed by deterioration of liquidity first and then pores closed.

Jan 1, 2015

By Dietmar Eifler, Marcus Klein, Hendrik Kramer

Conventional methods to characterize the fatigue behavior of metallic materials are very time and cost consuming. That is why the new short-time procedure PHYBALCHT was developed at the Institute of Materials Science and Engineering at the University of Kaiserslautern. This innovative method requires only a planar material surface to perform cyclic force-controlled hardness indentation tests. To characterize the cyclic elastic-plastic behavior of the test material the change of the force-indentation-depth-hysteresis is plotted versus the number of indentation cycles. In accordance to the plastic strain amplitude the indentation-depth width of the hysteresis loop is measured at half minimum force and is called plastic indentation-depth amplitude. Its change as a function of the number of cycles of indentation can be described by power-laws. One of these power-laws contains the hardening-exponentCHT eII, which correlates very well with the amount of cyclic hardening in conventional constant amplitude fatigue tests. To identify heat-treatment-parameters and SAE 52100 TRIP-alloys with high hardening rates as well as their damage tolerance the PHYBALCHT- and PHYBALLIT-method were used. One modified SAE 52100 TRIP-alloy was investigated in detail. The fatigue behavior and the cyclic hardening of the selected SAE 52100 TRIP-alloy was investigated and compared with conventional SAE 52100. Conventional stress-controlled fatigue tests were performed on a servo-hydraulic test system with a frequency of 5 Hz and a load ratio of R = -1. Different rates of cyclic hardening were identified. The size of the nonmetallic inclusions leading to crack initiation and the number of cycles to failure were used to evaluate differences in the damage tolerance capability.

Jan 1, 2015

By Xuling Chen, Zhiyun Ji, Min Gan, Tao Jiang, Liang Yin, Xiaohui Fan

Straw char exhibited considerably faster burning speed than coke breeze for its porosity, which significantly degraded sinter quality when it replacing coke breeze as sintering fuel. In this investigation, preforming technology has been employed to densify raw straw. The properties of straw char preformed show that its density was increased, and the structure was also densified, which made the difference of combustibility between the straw char and coke breeze smaller. The proper preforming temperature, residence time and pressure were 200℃, 1min and 120MPa respectively. Sinter pot trials show that the product carbonized from preformed straw made the proper replacement ratio to coke breeze increase from 20% to 40%, and the emission reduction of SOx, NOx in flue gas increase from 11.50%, 14.15% to 37.85%, 23.60% respectively, compared with non-preformed straw char.

Jan 1, 2015

By C. Pichler, A. Ressler, D. Gregurek, A. Spanring

In order to improve the refractory lining life at one of the RHI key customer test procedures were developed within a two years collaboration project. In the first year of cooperation detailed refractory corrosion work in the rotary kiln with Ca-ferritic slag was performed. The main results of the second year of cooperation, reported in this article, involve a detailed testing work with nickel matte and pre-selected refractory brands which was performed in TBRC. A first part of this work was a complete chemical and mineralogical characterization as well as FactSage calculations carried out on provided matte samples. According to these results testing in the TBRC was realized at different process temperatures with several magnesia-chromite bricks. Based on the mineralogical investigation a high chemothermal load caused by sulfidic matte resulted in a deep reaching infiltration of the brick microstructure and partly corrosion of main brick components.

Jan 1, 2015

By G. Plenge, M. Brittan

"Plant design parameters for gold extraction, leach residence time and cyanide consumption are generally determined from standard bench-scale bottle roll or agitation leach tests. The application of laboratory data to process design has essentially evolved from the testing of oxide or low cyanide-consuming ores. Such scale-up factors may not be appropriate for ores that deplete cyanide and oxygen since this interferes with gold extraction kinetics. High cyanide-consuming ores also exacerbate the differences between the conditions applicable to small batch tests and large continuous operations. Testing a reactive high-sulfide South American ore deposit necessitated the re-evaluation of conventional bench-scale cyanidation procedures. Pulp density can be a major factor affecting the results for plant design purposes and should be treated as a test work variable. As with high clay-bearing ore, where pulp viscosity can hinder mass transfer, minimizing the influence of test equipment on gold extraction kinetics may require low pulp densities. This introduces interpretative complexity since cyanide consumption changes as a function of pulp density. Activated carbon also consumes cyanide, so its effect has to be accounted for in the case of carbon-in-leach (CIL) or carbon-in-pulp (CIP) plant flowsheets. Since cyanide is an expensive reagent, often a major component of plant operating costs, it is important that the scale-up of cyanide consumption from laboratory to plant be representative. The traditional method of reporting cyanide consumption in bench-scale testing is questioned since it takes credit for residual free cyanide in leach tails. The projected plant consumption may be better estimated by using the total cyanide addition in a laboratory test. We propose a test work protocol that categorizes the cyanide consumption into its components but requires more extensive testing to generate design data. The ultimate validation of scale-up factors used by project engineers requires rigorous bench-scale versus commercial plant comparative data. Such data are not readily available.IntroductionMajor factors in the design of a gold processing plant are gold recovery, leach residence time and cyanide consumption. These parameters are important determinants of project revenue and costs and, thereby, potentially of project financial viability. Estimates of the associated design criteria for a commercial plant are normally generated from laboratory cyanidation, carbon-in-leach (CIL) or carbon-in-pulp (CIP) tests using standard procedures (Angove, 2005). The key question is whether the standard laboratory test work procedures developed historically for low reagent consuming ores are appropriate for ores that are highcyanide and oxygen consumers.The present paper examines test procedural factors that can influence the test work results and, therefore, their interpretation for design scale-up purposes. The study refers in particular to a high cyanide-consuming sulfide ore. The ore was being tested to develop scoping level engineering design criteria for a proposed project in South America."

Jan 1, 2015

By K. Bartholomew

The Functional Performance Equation for ball milling circuits provides plant staff with a new means to improve circuit performance. However, successful execution of a plant processing performance improvement project, with verifiable improvements, requires a significant number of accompanying steps beyond using this equation. In order to identify and articulate all these steps, a study was undertaken with the metallurgical staff from two milling operations and process application specialists from a grinding media manufacturing company. “Task analysis” of improving plant grinding performance was carried out. This analysis identified the required steps, and ultimately yielded a “Plant Grinding Circuit Processing Performance Management/ Improvement System.

Jan 1, 2015

By Filippo Maria Leoni, Wesley Schmutzler

"Deep Mixing Method (DMM) for the Rio Puerto Nuevo Project in San Juan was chosen by the Corps of Engineers to improve the soils adjacent to a 90 inch forced sewer main relocation and to improve the soils for the base of a new drainage channel. The project is located just east of San Juan and south of the Horizon Port. The soils to be improved consisted of fill, marine clay, organics (peat) and the foundation clay layer. A preconstruction soil investigation campaign was performed to assess soil properties and to retrieve samples of the different soil layers for the laboratory Bench Scale Testing program (BST). The BST was conducted using various binder contents and water/cement ratios in each of the soil types; the selection of the different combinations and dosages was based on past extensive experiences on similar materials. Following the laboratory program, a full scale Field Test (FT) was done installing several DMM elements to verify the results of the BST and fine tune the construction parameters. Each element consisted of two 5.5 feet diameter overlapping mixing augers installed simultaneously to a depth of approximately 60 feet using a SOILMEC SR-90 dual axis drilling rig. The FT construction and post-construction coring results showed significant differences between the lab study and the actual field conditions. This paper will highlight these differences and the importance of performing both pre-construction laboratory and field tests in order to ascertain the proper mixing parameters in the different soil layers.IntroductionThe Puerto Nuevo project consists of the stabilization of a major drainage channel using Deep Mixing Method (DMM) and the relocation of a 90 inch forced main sanitary sewer outfall. The first portion of this project was a 40 x 16 x 2,000 foot box culvert installed in 2004. In order for the drainage system to be completed and function properly, the 90 inch forced main needed to be lowered about 20 feet to allow for proper drainage.DMM was chosen by the US Army corps of Engineers to stabilize the drainage channel as well as improve the soil under the relocated sewer main. The overall layout of the project is shown in Figure 1. The DMM is arranged in different zones (A through E) with variable top and bottom design elevations as can be seen in the typical cross section for ZONE A and B as an example. (Figure 2) The total amount of soils to be treated by DMM is approximately 84,000 cubic yards up to a maximum depth of 57 feet from ground surface and an Area Replacement Ratio of 100%.The equipment used to perform the DMM is a Soilmec SR90 twin-shaft jet assisted deep mixing rig (Figure 3) coupled with a LODOS 30 grout plant and two Soilmec 7T-500J high pressure pumps."

Jan 1, 2015

By Seth H. Hamblin, John E. Regan, Dimitrios Palantzas

"Through reliability-based calibration of larger pile load test databases, recent developments of the Load Resistance Factor Design (LRFD) methods, which include geotechnical load and resistance factors for deep foundations design, have advanced the state of practice for geotechnical engineering. These load test databases upon which the current geotechnical load and resistance factors have been developed are limited, however, and do not provide sufficient data to support the development of resistance factors for uplift (tension) pile capacity. As such, some recommended resistance factors for uplift capacity estimation methods are simply derived by reducing the recommended resistance factors for piles in compression by a factor of 0.10.The results of three (3) tension loading tests performed to failure on 508 mm (20- in) square precast, prestressed concrete piles, driven though granular soil in southeastern Massachusetts, are presented and compared to static pile capacity calculations and dynamic analyses performed using the Pile Driving Analyzer (PDA) during installation. These results are presented along with current recommended LRFD resistance factors for driven piles under uplift (tension) loading conditions. These comparisons offer an assessment of the applicability and limitations of current resistance factors methods for piles under uplift loading and may be useful additions to the existing database for future calibrations of LRFD resistance factors for driven prestressed concrete piles in sand.IntroductionIn 2010, two (2) natural draft cooling towers were constructed by Kiewit (Kiewit) Construction Company of Woodcliff Lake, New Jersey at the Brayton Point Power Station in Somerset, Massachusetts. These massive 500 foot tall, 400 foot diameter cooling towers were designed to convert the existing “open loop” system into a “closed loop system” thereby dramatically reducing the thermal impact to Mt. Hope Bay.Based on design guidance from the German VBG Design Code and the Massachusetts State Building Code (MSBC), tension (i.e. uplift) and lateral loads due to wind loads and design seismic events represented the critical loading conditions.Weighing approximately 190,000 kips upon completion, the cooling tower loads are transferred to 44 foundation nodes (i.e. pile caps) evenly spaced along ring beams which run the circular perimeter of each tower base. Each pile cap node was designed to resist a 2,000 ton compression load, 200 tons in tension (i.e. uplift), and 600 tons in the lateral direction."

Jan 1, 2015

By Deepak Pappusetty, Miguel A. Pando

This study is motivated from the increased interest in recent years to explore use of Ocean Energy Converters (OEC’s).OEC’s can be tidal or generate electricity from wave or current action. Design of foundation systems for these OEC’s is a key consideration as it can represent about 35% of the initial installation cost. The primary focus of this paper is related to foundation systems involving monopiles where a key design consideration includes gradual accumulation of pile head deformations beyond serviceability limits of the OEC. This design consideration is important since these foundation systems are often subjected to more than 108 low amplitude repetitive dynamic load cycles during a normal 30 year design life. Research on single model piles installed in sand and subjected to over 104 low amplitude lateral load cycles have shown that pile head displacements and rotations tend to increase gradually with increasing load cycles. This gradual development of pile head deformation is related to plastic strain accumulation in the soil in the vicinity of the monopile. Analytical methodologies based on conventional p-y curves typically cannot predict these accumulated pile head rotations and displacements. Even 3D dynamic Finite Element Analyses may not capture this response for several conventionally used soil constitutive models. This manuscript presents predictions using p-y based methods as well as 3D dynamic finite element analyses. The different numerical predictions are compared to available experimental data. Results from this study show that conventional p-y methods do not predict the gradual pile head displacements observed experimentally. Modified p-y curves, developed for cyclic loading, do a better job than conventional p-y curves but tend to greatly under predict deformation. This is believed to be related to the cyclic load test data used to develop these cyclic p-y curves which involved at most up to 500 cycles and did not include high frequency contents or partial unloading cycles. The 3D FEA captured reasonably well the general observed trends of gradual accumulation of pile head rotation and lateral deformation with increasing constant amplitude lateral load cycles.

Jan 1, 2015