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By Andrew Thomson, Peter Wright

"A section of a London Underground expanded segmental lined tunnel constructed in the 1970’s progressively deteriorated after 2001, with extensive radial joint spalling and mid-segment cracking. As part of the PPP contract Tube Lines Ltd and their partners carried out various analyses of the tunnel, including analysis of laser scans of the tunnel, geotechnical testing through the tunnel walls, geotechnical desk studies, real-time monitoring and even full-scale segment testing. This paper discusses the behaviour of the tunnel lining in this setting, the causes of failure and the lessons that can be learnt from this rare example of a tunnel which was progressively failing in service. It is finally noted that a replacement tunnel lining was installed during night-time possessions and completed in 2015. INTRODUCTION In 2003, Tube Lines Ltd. was established under a Public-Private Partnership (PPP) scheme to provide maintenance services and upgrade projects for London Underground (LU). The Deep Tube Tunnel Knowledge and Inspection Programme comprised the assessment of all tunnels, shafts and other underground structures. This included a number of lengths of tunnel constructed using segmental concrete linings. First used by LU in the 1960s, the savings both in cost and speed of construction led to concrete linings replacing cast iron for new tunnel construction in all but a few cases. During the initial scoping phase of this programme, inspections identified potential issues with the expanded concrete segmental linings on the Jubilee line. The inspections found a number of segments with surface spalling (Figure 1a), which did not appear on the post-construction defect records. These were generally relatively shallow, up to 40mm deep, spread over a wide area of segment. These were different to spalls caused by handling damage, which are typically localised at segment corners. Subsequent inspections over the following years identified an increasing number of segments with these types of spalls as well as an increased incidence of longitudinal mid-segment cracking (Figure 1b). The increasing occurrence of these defects was hypothesised to be caused by tensile stresses developing in the vicinity of the joint."

Jan 1, 2016

By Chengcan Wang, Jin-Tae Han, Young-Eun Jang

"The waveform micropile is a newly developed foundation type for increasing the bearing capacity with the created shear keys on the pile’s shaft. Analyzing the increment of resistance at the shear key zone is a crucial factor in the design of the waveform micropile. Hence, centrifuge tests were carried out employing six different models, including a waveform micropile in the axial loading condition. The analysis results of the load-settlement curves showed that the waveform micropile achieved a higher bearing capacity compared to the micropile without shear keys. In addition, the test results revealed that the load-settlement relationship was affected not only by the pile shape but also by the locations of the shear keysINTRODUCTIONA micropile is a small-diameter pile, typically constructed with a less than 300 mm diameter. Generally, the micropile’s construction involves drilling, grouting, and insertion of a reinforcement material, such as a thread bar. The micopile can be utilized in a variety of fields for reinforcing the foundations of existing structures. It also has advantages for accessing challenging areas like limited-access construction sites, including those with a low headroom space and adjacent structures, due to the small size of the construction equipment. Thus, since it was introduced in 1950 in Italy, the micropile has become one of the preferred solutions when other deep-foundation methods are not applicable to the site.Federal Highway Administration (FHWA) gives the micropile design implementation guideline of neglecting the end bearing due to its small diameter but considering the frictional resistance if the bond zone of the pile is in the soil or on a weak rock. The bearing capacity is considered primarily only if the micropile is founded on a high-quality sound rock (FHWA, 2005). Micropile design in South Korea is currently being performed based on the FHWA manual and taking into consideration the frictional resistance for the design as the pile generally sockets into a weak rock or soft rock. Moreover, the frictional resistance within the soil layer has usually been ignored, considering only the shaft resistance of the rocksocketed length in the conservative design. The design concept excluding the frictional resistance in the soil layer, however, may lead to an extension of the pile socket length, which will increase the construction cost. Hence, many researches have attempted to provide better design and construction methods to increase the bearing capacity in a cost-effective way (Juran et al. 2001; Sadek and Isam 2004; Tsukada et al. 2006; Finno 2002; Gomez et al. 2003; Seo et al. 2013)."

Jan 1, 2016

By James F. Davis, Matthew A. Conte, Robert F. Tonning

This is a paper demonstrating the steps taken to combine multiple types of piles for a single site to maximize the benefits and characteristics of each method. We intend to discuss the use of grouted displacement piles in lieu of traditional pile types that were specified on an individual project. We will show how implementing this alternate pile type can both supplement and replace the originally specified pile to increase efficiency and lower costs. We will demonstrate a reduction in spoils, vibration, crew hours, and equipment size while employing methods to overcome unforeseen ground conditions.

By Y. Zedan

In this study, the statistical design of experiments (DOE) was applied to study and regulate the properties of near-eutectic Al-11%Si alloys. Develop regression equations for such response variables as hardness, yield stress, ultimate tensile stress, percent elongation, total cutting force, cutting power, and tool life together with other factors which, include the percentage composition of the alloying elements, and the requisite modification (Sr) level. These equations may be analyzed quantitatively to acquire an understating of the effects which the main variables and their interactions may have on the mechanical behaviour and the machinability of the alloy under investigation. The results reveal that increasing the levels of Cu and Fe content results in an increase in hardness, yield stress, and ultimate tensile strength in both modified and non-modified alloys. On the other hand, both Cu and Fe appear to affect the percentage elongation adversely, whereas the Sr-level has a positive effect on this parameter. It was found that Sr-levels have the most significant effect on the cutting forces and cutting power followed by the content in Fe and Cu. The results also reveal that the interaction coefficients of these variables have a significant effect on tool life compared to the main independent variables. This fact may be attributed to the formation of complex insoluble phases between Cu, Fe, Si, and Al as investigated using Scanning Electron Microscopy (SEM) attached to an EDX analysis system. The accuracy of the regression equations in predicting the expected properties has been verified by carrying out random experiments in the range of variation of these variables.

Jan 1, 2011

By A. Rod Kern, Michael A. McNicholas, Yaser Taheri

Deep foundations were required for construction of an 18,000 ft2 (1,672 m2) 4-story office building and an adjacent 23,750 ft2 (2,206 m2) 5-story parking garage in Queens, New York due to an existing uncontrolled fill layer ranging from 15-20 ft (4.6 - 6.1 m) in thickness beneath the building footprint. The geotechnical engineers for the project initially selected auger cast-in-place (ACIP) piles over driven piles to limit the impact of noise and vibrations on the surrounding neighborhood. Ultimately, drilled displacement piles (DDP) were installed since this method offered a more economical solution that would generate the required pile capacity with shorter drill depths and would also mitigate spoils volume. During installation of test piles by the geotechnical contractor retained for the foundation work, multiple unanticipated soil conditions were encountered that would adversely affect the constructability of the piles. The existing fill contained significantly more natural and manmade obstructions than expected and the underlying glacial soil became too dense to penetrate at shallower depths than anticipated. This paper discusses how these issues were overcome through pre-drilling and the use of detailed instrumented test pile data coupled with in-house engineering capability to proactively re-evaluate minimum pile lengths at any given location and keep the project on track. INTRODUCTION Geotechnical work in the New York City market presents soil conditions that can be highly variable and challenging due to the presence of uncontrolled urban fill placed over the native soils. Construction in this area can therefore pose many unforeseen challenges, even with detailed geotechnical analysis being performed at project sites. A case in point is a construction site in Queens, New York. The proposed site development consisted of construction of a 4-story office building with a footprint of 18,000 ft2 (1672 m2) and a stand-alone 5-level parking garage with a footprint of 23,750 ft2 (2206 m2), together with associated new pavements and utilities. The site is bordered by a mix of commercial buildings and residential properties on all sides. Depth of the uncontrolled nature of the fill extended up to 20 ft (6.1 m) below street grade. Given the significant cost associated with removal and replacement, deep foundations were recommended to bypass the unsuitable soils and support the structures at depth where good bearing material existed.

Jan 1, 2019

By Emad Farouz

This paper presents a case history of a successful construction-phase pile load test program that optimized the pile design in challenging ground conditions at the Great Neck Wastewater Treatment Plant in the Town of North Hempstead in Nassau County, New York. The improvements and expansion of the wastewater treatment plant included the construction of several new structures to comply with new stringent nitrogen discharge requirements and new design flow. The challenging ground conditions included up to 20-ft thick organic deposits with weight of hammer blow counts and up to 14 percent organic content and tidal ground water that was near the ground surface. The foundation design evaluated various deep foundation alternatives and selected driven closed-ended pipe piles then filled with concrete as the most suitable foundation. The selection process included considerations of cost, risk, vibrations, noise, and schedule. The contract documents utilized an innovative approach of performing an optimization load test program that was implemented during construction to optimize pile lengths and reduce potential vibration and construction schedule. This paper discusses the details of the successful load test program including static testing, dynamic testing, and the innovative contracting approach utilized to implement the construction phase load test program. It also discusses the successful development and implementation of driving criteria for production piles and construction challenges. The successful load test program resulted in savings of several hundred thousand dollars, optimized schedule, and lower environmental impacts.

By Stefano Utili, Robert Pell, Nelson Morales, Cristobal Valderrama, Andrea Agosti, Guillermo Albornoz

The overall slope angle (OSA) of pit walls plays a crucial role in the financial return of open pit mines. The work showcases a novel design methodology where non-planar geotechnically optimal pit walls with an OSA steeper than what is used in current design practices are employed without compromising mine safety, i.e. the optimal profiles are featured by the same Factor of Safety (FoS) than their traditional design counterparts. In the current design practice, pit wall profiles are often designed to be planar in cross-section and the profile in between ramps especially tend to be defined by a constant inter-ramp angle.

Sep 30, 2022

By M. M. Kim

Zn-27% Al was pressure infiltrated into a column of 20 micron diameter abrasive grade SiC particles to give billets with particle loading of 50 voli.une %. Some billets were heated to a temperature where they became semi-solid and diluted with liquid Zn-27% Al alloy to give billets with particle loadings of 12 and 16 volume %. Some of these billets were then extruded into wire with an area reduction of approximately 98%. Tensile properties of the as-cast billets were always inferior to those of the matrix alloys; however, the extruded composite samples showed at 37% improvement in ultimate tensile strength compared to their extruded conventional counterparts. The fracture surfaces of these samples are described.

Jan 1, 1990

By C. P. Haller, S. J. Aresco, R. F. Abernethy

The Bureau of Mines has been active in promoting the purchase of coal for Government use under specifications that define the requirements in terms of heating value of the coal, expressed in British thermal units, and the composition as shown by proximate analyses. To these, when required, are added the ash- softening temperature of ash, the free-swelling index, and the hardgrove grind- ability index. Under most of these specification contracts the bidders guarantee the quality of the coal, and that guaranteed by the successful bidder becomes the standard of his contract. The deliveries are sampled in accordance with instruc- tions issued by the Bureau of Mines; the samples are analyzed in the Bureau laboratory to determine whether the coal is of the quality guaranteed by the con- tractor and, if it is not, a price adjustment is made. Analyses of the delivered coal and tipple samples (samples collected at mine tipples as coal is being loaded into railroad cars or trucks) provide valuable data for use in evaluating future bids. In addition, the continuous sampling of coal as delivered is a check on the practical results obtained in burning the coal. The Government purchased approximately 5-1/4 million tons of coal in fiscal year 1953. In connection with these purchases, the Bureau analyzed 11,435 samples. These are published for the use of Government officials and the public. A series of publications has been completed on coal analyses by States, or, where production is small in any one State, by groups of adjacent States. In addition to analytical data showing composition and quality of coals of the States, the publications con- tain brief descriptions of the geological structure of the coal basins, typical mining conditions in the various districts, the principal economic data of the industry, and the relationship of mine or channel samples to delivered and tipple samples. The present publication covers many States but deals only with the analytical data of the coals. Previous publications in this series are: Bulletin 516, Analyses of Tipple and Delivered Samples of Coal (Collected During the Fiscal Years 1948 to 1950 Inclusive); Report of Investigations 4934, Analyses of Tipple and Delivered Samples of Coal (Collected During the Fiscal Year 1951); Report of In- vestigations 4972, Analyses of Tipple and Delivered Samples of Coal (Collected During the Fiscal Year 1952). Following are the Bureau of Mines technical papers published by States, with their numbers: Alabama, 347; Alaska, 682; Arizona, California, Idaho, Nevada, and Oregon, 696; Arkansas, 416; Colorado, 574; Illinois, 641; Indiana, 417; Iowa, 269 and 706; Kansas, 455; Kentucky, 308 and 652; Maryland, 465; Michigan, North Dakota, South Dakota, and Texas, 700; Missouri, 366; Montana, 529; New Mexico, 569; Ohio 344 (and Bulletin 499); Oklahoma, 411; Pennsylvania Bituminous, 590 (Supplement 645); Pennsylvania Anthracite, 659; Tennessee, 356 and 671; Utah, 345; Virginia, 365 and 656; Washington, 491 (Supplement 618); West Virginia, 405 and 626; and Wyoming, 484.

Jan 1, 1955

By Tim Chapman

This general report considers what promoters of deep basement projects want from their teams and whether they get it often enough. Most large projects are based on complex financial models where the funding is related to a future income stream. Project delays and cost over-runs can critically affect the financial model. Too often, delays and cost over-runs originate in the substructure and foundations. We must take positive steps to improve our industry's reputation for reliability.

Jan 1, 2006

One of the earliest and continuing challenges in driving sustainable development in large scale resource industry projects is around the issue of assessment û how do you measure the sustainability of a mineral operation? One of the key road blocks when confronted with this challenge is the temptation of technical folks to reach for a definition of sustainability or sustainable development. But definitions, by definition, have boundaries and limitations that serve to constrain thinking û they limit the thinking of what we can achieve with sustainability (it also acts as a barrier that constrains innovation). Rather than seeking definitions, better understanding of the core perspectives around sustainability and their application to the minerals industry provides a much more powerful platform from which to conduct assessments. But it is only when these perspectives are combined with the right framework and supporting techniques that the complex becomes doable. With the support of the perspectives and the framework, various assessment and measurement methodologies can be used; the challenge is communicating to stakeholders the sustainability character of the project in ways that are meaningful and to which people can connect. Assessment is not about finding the best or most accurate methods that fulfil strictly academic and possibly abstract requirements. The challenge is to help people understand what the impacts are, and what the value contributions will be, in a format and language that make sense in their world-view.

Jan 1, 2009

By H. Kiyama

In order to further elucidate the mechanisms involved in autogenous grinding, the fracture of rock specimens in free-fall impact was studied using the theory of elasticity. Stress distributions in rock specimens under various conditions of impact were analyzed and the conditions for failure were examined in relation to the compressive and tensile strength of rock. The energy equation derived for autogenous grinding coincides basically with Lewis' generalized formula or Oka and Majima's formula, and it is sufficiently general to incorporate all of the three older theories, viz; those of Rittinger, Bond and Kick.

Jan 1, 1972

By Emad Farouz, Francis A. Abreu

"This paper presents a case history of a successful construction-phase pile load test program that optimized the pile design in challenging ground conditions at the Great Neck Wastewater Treatment Plant in the Town of North Hempstead in Nassau County, New York. The improvements and expansion of the wastewater treatment plant included the construction of several new structures to comply with new stringent nitrogen discharge requirements and new design flow. The challenging ground conditions included up to 20-ft thick organic deposits with weight of hammer blow counts and up to 14 percent organic content and tidal ground water that was near the ground surface. The foundation design evaluated various deep foundation alternatives and selected driven closed-ended pipe piles then filled with concrete as the most suitable foundation. The selection process included considerations of cost, risk, vibrations, noise, and schedule. The contract documents utilized an innovative approach of performing an optimization load test program that was implemented during construction to optimize pile lengths and reduce potential vibration and construction schedule.This paper discusses the details of the successful load test program including static testing, dynamic testing, and the innovative contracting approach utilized to implement the construction phase load test program. It also discusses the successful development and implementation of driving criteria for production piles and construction challenges. The successful load test program resulted in savings of several hundred thousand dollars, optimized schedule, and lower environmental impacts.SITE AND PROJECT DESCRIPTIONThe Great Neck Water Pollution Control District (GNWPCD), located in the Town of North Hempstead in Nassau, New York, owns and operates a municipal wastewater treatment plant (WWTP) that discharges treated effluent through an outfall to Manhasset Bay, which is a tributary of the Long Island Sound. The site is located west of Manhasset Bay and is surrounded on three sides by local roads, and commercial, industrial, and recreational properties. The site has a gentle slope ranging from elevation +20 to +7 from west to east, respectively, based on the Nassau County Datum.To comply with new nitrogen discharge requirements and new design flows, the GNWPCD contracted CH2M HILL, Inc. and William F. Cosulich Associates as a Joint- Venture (JV) to design and provide services during construction of eight new advanced nitrogen removal facilities."

Jan 1, 2017

By Scott Webster

Dynamic pile Monitoring Services (DMS) have been used for testing of offshore piles for several decades. However, most of this testing was to measure hammer performance and pile stresses rather than pile capacity or soil resistance. As the need for more economical solutions for foundation support increases, the use of DMS has provided a better means of evaluating in-place pile capacity for offshore structures, and therefore a method of determining pile acceptance. The authors have been involved in several offshore projects where DMS has been the primary source of data for acceptance of the driven pile foundations. The use of DMS for evaluation of offshore foundations requires considerations quite different from land applications and these considerations are often necessary for the careful and thorough analysis of the collected data in nearly real time for determination of pile acceptance. Case Method capacity estimates are often of little use due to the non-uniform cross sections of the foundation piles and their deep penetrations. Therefore, capacity assessments should be made using CAPWAP which is a signal matching program whose utility and reliability has been proven on thousands of projects every year, both on land and offshore. Depending upon the soil conditions at a given location, capacity assessment after soil setup effects may be necessary. In addition, tension capacity is often critical when pile refusal occurs significantly before the design pile penetration depth. Evaluation of uplift capacity can be accomplished by a CAPWAP analysis, which results in a total capacity prediction and its shaft resistance component. The use of hydraulic hammers for driving of these piles also adds the requirement of controlling hammer energy such that over-stressing of the pile is avoided. The calculation of non-axial stresses such as bending or eccentric stresses may also be involved in order to prevent pile damage.

Jan 1, 2010

By Todd W. Armstrong, Michael D. Reader

"INTRODUCTIONThe Playa Vista Development is the largest urban infill development in the history of the United States. Overall, it encompasses about 1100 acres in the City of Los Angeles and is situated north of Los Angeles International Airport near the Pacific Ocean. The development taking place on the project consists primarily of high-density residential condominiums with 1 to 2 levels of subterranean parking . The geotechnical conditions are typified by high groundwater, soft clays, and liquefaction, in addition to environmental issues such as methane.Due to a combination of the geotechnical factors and noise restrictions, both driven and drilled piles were not feasible once the initial phase of the project was occupied. As a result, the project developer undertook a testing program that consisted of the installation and load testing of 9 piles in order to obtain City of Los Angeles acceptance of a pile installation system that met the site constraints. The testing program was divided between two separate contractors operating on sites set on opposite sides on the street (Figure 1 ). Contractors working in Test Areas A & B employed the ""dry dip"" and ""wet dip"" methods of auger pressure grouted displacement (APGD) pile installation, respectively.This paper summarizes the extraordinary program undertaken to install, document, test, and examine auger pressure grouted displacement piles at this site. The program ultimately resulted in City acceptance of auger pressure grouted displacement piles, a historically difficult challenge given the City's resistance of acceptance of ""new"" technologies.A summary of elements included in the test program are: (1) quality control; (2) load testing; (3) long-term testing; (4) non-destructive testing; and (5) pile exhumation."

Jan 1, 2005

By A. Davis

Pit lake chemistry depends on the lithology and hydrologic characteristics of the ultimate pit surface, the availability of buffering capacity in the wall rock versus oxidizable sulfide content, and the alkalinity of recharging ground water. In this paper, we assess the geochemistry of 11 existing pit lakes, ranging from the acidic Red Hill and Berkeley pit lakes (pH 2.6 to 2.8) to the alkaline Yerington Pit lake (pH 8.45). Predicted pit lake chemistry is similar to that in existing pits with the long-term pit lake chemistry lying on a geochemical continuum between end members consisting of influent calcium bicarbonate ground water, and naturally occurring sulfate-rich evaporite playa lakes.

Jan 1, 1996

By Abid O. Adekunte, David Greentree, David Hilton

"The construction industry is witnessing an upsurge in demand by property developers to have basements incorporated into their residential and commercial development schemes. This is attributable to perceived improvement to aesthetic and commercial values of buildings by underground space, amongst property owners. This trend is compelling more owners of buildings with no basements to explore the possibility of creating underground additional space beneath their existing buildings. The creation of a basement beneath an existing building entails the installation of a reinforced concrete (RC) underpinning system, temporary works, bulk excavation to basement formation level and construction of the basement structure, with associated aesthetic finishes.The L-shaped segmental RC underpins are a common system of choice for such underpinning works. They are multi-functional; providing vertical support to the existing superstructure, providing lateral support to earth and groundwater, supporting temporary and permanent surcharge loads from adjacent structures and services, whilst also forming part of the basement slab. This paper focuses on the first function of the Lshaped RC underpins; capacity under vertical compressive loading from the superstructure. The most common industry approach for the prediction of vertical capacities of L-shaped underpins is the oldfashioned Meyerhof’s (1953, 1963) effective width method, which is based on the traditional bearing capacity theory, whilst accounting for correction factors for eccentricity and foundation depth.The traditional bearing capacity formula is surrounded by a significant degree of uncertainty; estimates are highly user-dependent, as capacity prediction is sensitive to the chosen angle of shearing resistance (?), while there are difficulties in accurately measuring the in-situ ??value of cohesionless soils. In addition, the effective width approach has been shown to be very conservative by many research workers. The segmental RC underpins presented in this paper have been designed with an alternative less conservative method, which involves the use of a recently proposed consistent work-hardening plasticity model calibrated with field-based tests on footings of various aspect ratios and relative embedment in sand. The paper highlights the principles behind underpinning works for urban basement construction, the design of L-shaped RC underpins with the recently proposed plasticity model and the advantages of the method over traditional bearing capacity solutions and pre-existing plasticity models."

Jan 1, 2016

By R. Uwaoma, A. Goosen, R. Matjie, K. Mphahlele, J. Bunt

Coal properties that are associated with wear and damage of grinding equipment during pulverization prior to combustion were investigated. A South African Highveld feed coal and its beneficiated fractions were crushed to <1 >0.25 mm particles for the grindability tests. These particles were milled and screened into <75 μm and >75 μm fractions, which were analysed by different techniques to establish a correlation with the conventional Hardgrove Grindability Index (HGI). The <1.5 g.cm-3 float fraction, which contained 93 vol.% (mineral matter free) total -macerals,9% kaolinite, and had the lowest HGI (57) (hardest to grind) was pulverized for 15, 30, 60, and 120 minutes for particle size distribution analysis. This analysis indicated that the content of <75 μm particles increases with increased grinding time. The >1.9 g.cm-3 sink fraction, with the highest HGI (76), 44% kaolinite, and 20 vol.% total macerals, was ground easily to generate the highest proportion of <75 μm particles. Based on higher correlation coefficients (R2 = 0.77–0.91), the ash yield, mineral matter, petrographic composition, and fixed-carbon have significant effects on the HGI. Conversely, the inherent moisture and total sulphur (R2 = 0.48–0.62) have only minor effects on the HGI. Results from this investigation could be implemented in the preparation of a suitable pulverized fuel with little equipment wear, as well as utilizing mineralogical and petrographic compositions. Finally, the effect of microlithotypes and maceral types in South African feed coals on the HGI should be investigated in further pulverization and grindability studies.

Jul 5, 2023

By CHARLES L. WRIGHT

Previous work.-The general plan of work outlined for the Government fuel-testing plant erected at the Louisiana Purchase Exposition, at St. Louis, Mo., in 1904, included investigations relative to the briquetting of coals found in the United States. These investigations embraced the possibility of making satisfactory commercial fuels from lignite or low-grade coals which do not stand shipment well; of benefiting culm or slack coals that are wasted or sold at unremunerative prices; and of improving the furnace efficiency or ability to withstand transportation of good coals. This work was begun in 1904 and was continued in 1905, 1906, and 1907 as an essential part of investigations looking to the determination of methods for reducing waste and increasing efficiency in the utilization of the fuel resources in the United States. The initial briquetting tests at St. Louis, which included examination into the behavior of different coals or mixtures of coals in the briquetting press, experimental study of the merits of various substances used as binders, and consideration of the physical properties and resistance to weather and abrasion of the briquets, have been described.a They demonstrated that satisfactory briquets could be made from most coals, and that by briquetting the commercial value of many low-grade coals and lignites could be raised enough to more than cover the cost of manufacture. Norfolk plant.-The briquetting plant of the Geological Survey was moved from St. Louis, Mo., to Norfolk, Va., in 1907, along with the steam boiler and producer-gas equipment of the fuel-testing plant, as the closing out of the affairs of the Louisiana Purchase Exposition and the consequent removal of the buildings from Forest Park made a change of location necessary. Norfolk was selected largely with a view to the testing of coals for naval purposes, and because of facilities in the way of buildings and materials offered by the Jamestown Exposition Company. The work at Norfolk was chiefly devoted to making steaming and briquet tests of coals which reach the Atlantic seaboard at Norfolk and Newport News and are used by the navy and merchant marine. Two briquet machines were installed at the Norfolk plant, one being the English machine used in briquetting tests by the Geological Survey at St. Louis in 1905 and 1906, and the other an American machine. The briquets made at this plant were tested on locomotives of several railroads entering Norfolk and on the United States torpedo boat Buldle in comparison with the run-of-mine coal used in making them. Some of the tests were conducted by the railroads on their own locomotives, but those on the Biddle and on the locomotive of the Seaboard Air Line Railway were carried on by W. T. Ray and Henry Kreisinger, of the United States Geological Survey. Personnel.-Charles T. Malcolmson continued in general charge of the briquetting section after the removal to Norfolk until January 1, 1908. Walter J. Chapman continued in charge of operation of the briquet machines and of the observations reported under the heading "Details of manufacture." Charles L. Wright supervised the installation of the English briquet machine and later in the year continued the physical tests of briquets and the analyses in the chemical laboratory of the section until January 1, 1908, on which date he was placed in general charge of the work of the section. G. E. Ryder and Ralph Galt also continued with the staff, but the former was obliged to resign soon after the plant was in operation on account of ill health; the latter continued with the section as computer until the close of work on December 1, 1908.

Jan 1, 1911

The ever increasing demand for energy and the progressive depletion of crude oil resources, have renewed interest in oil shale as an alternative fuel resource. Weathered oil shale samples were assembled from El-Nakheil phosphate mine in Quseir area, Eastern desert, Egypt. The oil shale samples were prepared and analyzed by XRD (X-ray diffraction), XRF (X-ray fluorescence spectrometry), and optical microscopic techniques. Rock-Eval pyrolysis and total organic carbon were used to study shale hydrocarbon potential. A leaching procedure using inorganic and organic acids was used to selectively dissolve the oil shale associated ash forming minerals. XRD results showed that calcite is the dominant carbonate mineral, whereas primary silicate minerals are quartz and montmorillonite. SEM (Scanning Electron Microscopy) observations indicated that the organic matter is dispersed throughout the rock matrix. The acid soluble fraction upon leaching was determined to be 37.59 and 42.74 wt% by using 5% HCl and 10% HCl, respectively. The TOC was increased from 20.78 to 29.88 and 34.09 wt% by using 5% HCl and 10% HCl, respectively. Keywords: el nakheil oil shale, characterization, xrd, xrf, sem, elemental analysis, proximate analysis, ultimate analysis, thin section, rock eval pyrolysis, acid leaching

Sep 1, 2012