Search Documents

The acid plant consists of the following units: 1. Glover tower. 6. Mills-Packard type chambers. 3. Reaction towers. 6. Gay-Lussac towers.The sulphur dioxide bearing gases, used in the manufacture of the acid, are obtained from the roasting of zinc concentrate. Six Herreshoff type furnaces are available, each with an effective hearth area of 520 sq. ft.The concentrate contains approximately 30% sulphur, of which about 72 is ultimately recovered as acid. The oxides of nitrogen are added to the gases in the requisite proportions partly from nitrous vitriol and from nitric acid in the Glover tower, and partly from nitrous vitriol in some of the chambers and connecting flues.The acid leaving the Glover tower is cooled by the ordinary water-cooling coils, while the cooling of the chamber gases is effected by circulating water over the outer surface of the chambers, and by spraying nitrous vitriol and weak acid into them.Flow of gases throughout the plant is regulated and controlled by means of regulus metal fans, fitted with variable speed gears.

Jan 1, 1934

This paper forms the second of a series, in which it is proposed to communicate the results of an extensive research into the influence of alloying elements on the physical properties of lead, now being carried out in the Metallurgy School of the University of Melbourne.Some general comments on this research were made by the present writer as an introduction to the first contribution by R. S. Russell*: It was there pointed out that it was the intention to prepare lead as pure as possible, to determine its properties and then to make alloys with the various elements added singly, and in various combinations, in order to determine the effect of each. This line of action is still being pursued.It occurred to the writer, however, that this fundamental attack might, with advantage, be accompanied by a parallel investigation in which lead of commercial purity would form the basis material. In this way, using a standard *Professor of Metallurgy, University of Melbourne.

Jan 1, 1934

Ore samples from the South, Central and North ore-bodies of the King Cassilis Mine, near Omeo, Victoria, were broken and transported to Melbourne for experimental metallurgical treatment. A microscopical examination of individual unoxidised specimens, selected from these samples, was undertaken in order to thro'w as much light as possible on the occurrence of the gold which forms the valuable economic mineral in the ore.The following descriptions are the outcome' of this examination and show that very minute particles of free gold are mechanically associated with the sulphides. While the gold may be separated from the transparent gangue minerals by the flotation of the sulphides, the, actual size of the particles indicates that it is impossible to separate all the gold from the sulphides by grinding the ore to pass through a screen of 200 mesh in which the average width of the holes is 0.063 mm. Chemical disintegration of the sulphides is essential to free all the gold particles and render them available to the attack of chlorine or of a solvent.It is interesting to recall that a metallurgical investigation on the Cassilis ore in the same district by K. A. Mickle in...

Jan 1, 1933

The sulphide ore occurring in the North Mine at Broken Hill is of a complex nature, consisting of an intimate mixture of argentiferous galena, marmatite (zinc-iron sulphide), and gangue minerals. A typical analysis of the ore is:Lead 15.2%Zinc 12.0%Iron 5.3%Manganese 0.8%Copper 0.1%Alumina 0.3%Lime 0.9%Sulphur 11.1%Insoluble 53.8%Carbon dioxide 0.3%Undetermined 0.2%Silver 9 oz. per tonTotal 100.0%The metallurgical practice for the recovery of the lead concentrate and zinc concentrate from the crude ore is briefly described in the following pages.(1) COARSE CRUSHING AND FINE GRINDING OF THE CRUDE OREThe crude ore from the mine, containing lumps to the size of, roughly, 10 in. x 8 in., is tipped over grizzlies with the bars spaced 3 in. apart; the oversize gravitating to a...

Jan 1, 1933

LOCATIONThe property of the Mount Isa Mines Ltd. is situated in Western Queensland, 603 miles by rail west of Townsville, the nearest seaport. All supplies and the bullion are railed between Mt. Isa and Townsville. The climate is semiarid, and operations are conducted throughout the year without difficulty.WATER SUPPLYThe mill make-up water is obtained from the mine, and also from Rifle Creek reservoir, which is situated 20 miles from Mount Isa. The domestic supply of water is obtained from a series of bores on the company's leases.POWER SUPPLYElectric power at 3300 volts, 3-phase, 50 cycles, is supplied from the company's steam power plant, consisting of two units, each unit comprising one Babcock & Wilcox boiler, supplying steam at 300 lb. pressure per sq: in. to one 5000 kW. turbo-alternator. Pulverized coal is used as fuel, and power is being generated at a cost of 0.45d. per kilowatt hour. The coal used is supplied from the State Coal Mine, Bowen, costing 42/- per ton delivered at Mt. Isa.

Jan 1, 1933

Bakelite is fairly widely known as a suitable material for the mounting of ore specimens, concentrates and tailings for microscopical study, but has not as yet had extensive application. It is the most suitable mount for specimens which are to be held in the mechanical holder of a polishing machine, based on that described by J. W. Vanderbilt*, which is installed in the Geological Department of the Melbourne University.Bakelite products are prepared by subjecting bakelite powder to a temperature of about 1600 C. under a pressure of approximately two tons per square inch for a period of four minutes. The shape and size of the products are governed by the use of suitably constructed dies. When the concentrate or tailing is mixed with the bakelite powder, a briquette is produced which can be polished so that the opaque minerals in the sample can be examined microscopically in the same way as in a piece of solid ore. A simple machine for the construction of these briquettes has been described by Head and Slavin. It consists of a small four-pillar press in which the pressure is supplied by...

Jan 1, 1933

By Morley I. W

In the year 1926, Edie Creek, in the Morobe District of the Mandated Territory of New Guinea, saw the greatest gold rush of recent years. Situated 35 miles inland from the coast, and at an altitude of over 6000 feet, Edie Creek presented to the original prospectors a wet, jungle-clad uninhabited, and inhospitable region. There were no roads; and the only means of approach from the equally inhospitable coast was by an eight to ten days' tramp through coastal swamps and gorge-scarred mountains. All food supplies and equipment had to be carried on the backs of "kanakas," and in many cases through country occupied by hostile natives.Since the first discovery of payable gold at Edie Creek, mining on the Morobe Goldfield has shown remarkable progress, and in spite of the tremendous natural difficulties, the field today ranks as one of the most important in Australasia.Aeroplanes, more than any other factor, have been responsible for this rapid development. They provide the only means of transport from the coast, and at present serve the needs of over 600 Europeans and 3000 indentured native labourers engaged in the industry.

Jan 1, 1933

The treatment of mixed lead carbonate and lead sulphide concentrates at Mount Isa presents a problem which is unique ,in the lead smelting world; a problem whose solution is far from simple, and is not yet complete. Two years of study under plant conditions have definitely proved, however, that a most satisfactory sinter can be made in a single-pass roast.The object of this paper is to present a brief record of the development of the single-pass roast and a resume of current practice in the smelting plant. The sintering operation is discussed in greater detail, as it is upon this phase of the work that every item in the smelter operating programme depends.The smelter, to-day, presents a very much simplified layout, equipped for economical, straightforward operation, requiring, however, very careful and constant supervision, due to the extreme delicacy of the sintering operation and to the rapid and wide variati9n in the nature of the concentrates which are to be handled.

Jan 1, 1933

By Rose W. J

Geophysical prospecting was first recognized in Australia as an important aid to mining enterprises in 1927, when, on the suggestion of Sir Herbert Gepp, the "Imperial Geophysical Experimental Survey" was organized. The function of this survey was to carry out investigations on the applicability and efficacy of the most important geophysical methods under Australian conditions. The survey was formed under the joint auspices of the British Empire Marketing Board and Australian Commonwealth Government, and the investigations were carried out in Australia under the leadership of Mr. A. Broughton Edge, B.Sc., A.R.S.M., F.G.S., M.Inst.M.M., during the years 1928 and 1929. A description of the work performed, the apparatus used, the principles of the methods, and the results and conclusions of the survey are included in a report published by the Cambridge University Press in 1931.In 1932 Sir Herbert Gepp became interested in some gold mines in Eastern Victoria, in the Cassilis and Bethanga districts, and realizing that the lodes in these areas would be favorabIe for a geophysical examination, he arranged for a series of tests to be carried out. This work was performed by Mr. E. L. Blazey, B.E.E., a former member of the staff of the Imperial Geophysical Experimental, Survey, under the general direction of, and in consultation with, Mr. W. J. Rose, B.M.E.The work was commenced in October, 1932, at Cassilis, Vie., continued at Talgarno, Vie., .and concluded at...

Jan 1, 1933

DR. WARK, said: I have not come to Broken Hill to tell you how to conduct flotation operations; indeed, during my short stay here I have already learned much concerning the process, of the many difficulties which have been overcome, and of those still awaiting solution. My purpose to-night is rather different. All who have been concerned with the operation...

Jan 1, 1933

By Dunstan N, Valentine C

Gas power was first used on the Sons of Gwalia mine in January 1911, when a twin-cylinder Crossley engine of 167 hp was installed to belt-drive a 112 kw 550-volt ac generator. This engine was connected with a No 8 Crossley up-draught suction gas producer, using mulga charcoal as fuel.A second Crossley engine, of 400 hp direct-coupled to a 550-volt ac generator, was installed in 1912, and operated by a down-draught wood producer.This was followed by a large Kynoch twin tandem four-cylinder engine, rated at 660 hp, sea level, with a rope drive to the crushing and treatment sections of the plant.These engines operated until January 1921, when the plant and power house were destroyed by fire. After the fire, both Kynoch and second Crossley engines were salvaged and reconditioned and they continued to give useful service for some years.

Jan 1, 1932

In another paper the author described the electrolytic preparation of highly-purified lead. One of the most difficult parts, yet perhaps the most essential part, of that research was to ensure, firstly, that the purification process should be effective; secondly, that it should remain effective; thirdly, that the lead should not be contaminated during the tests that were done on it. All this necessitated periodic analyses of the lead.The purpose of this paper is to describe the work done by the author to check the accuracy of some known rapid methods for the estimation of impurities in highly-purified lead, with the intention of applying them to the control of the electrolytic process above-mentioned.METHODS ALREADY IN USEThe literature sets out accurate methods for the estimation of impurities in lead, but these methods are both lengthy and expensive. For example, the method described by Hemingway is used in the Port Pirie laboratory of the Broken Hill Associated Smelters Pty. Ltd., but it requires a sample as large as 1000 grm., and the time required to analyse a sample extends over days, and is too long to allow of quick control over a running process. This method was used by the Associated Smelters to obtain the analyses quoted in another paper by the author.

Jan 1, 1932

From time to time failures occur in structures made of lead, and the failure may be due to corrosion involving a definite thinning of the lead sheet, or it may be of such a nature that cracks develop and the lead appears to disintegrate. The idea of lead cracking will at once suggest something abnormal, for common experience shows that this metal is very ductile and will withstand considerable bending without showing any sign of fracture. Cracking, on the other hand, is usually associated with brittleness.Fig. 1 is a natural-size photograph of a cracked sheet of lead. Prior to photographing, the sheet was etched byimmersion in a solution of ammonium molybdate. Several characteristics of this crack will be evident. First of all it is distinctly a zigzag crack, and secondly it passes between, rather than through, certain well-defined areas which appear bright in the photograph. This is particularly noticeable at the lower end where the crack appears to terminate.

Jan 1, 1932

The Mount Lyell Company's concentrating mill is situated about a quarter of a mile westward of the portal of the North Lyell tunnel, which serves the North Lyell, Royal Tharsis and Crown Lyell mines, being on the 1100-ft. level of the first named. The Comstock mine is connected with the tram system at this level by five and a half miles of steam tramway, two-foot gauge being standard throughout.The plant is well placed with regard to all essential services and has an excellent water-supply from a series of three dams on the West Queen river.MILLING ORESThe mill feed is a mixture of the outputs from the foUr mines mentioned, each of which has its characteristic ore, but, generally speaking, about half of the ore consists of siliceous schists and the other half of hard grey quartzite. The schisty ores are easy to crush, but, on grinding, while the schist slimes readily, the quartz granules are hard, resulting in the handling of heavy loads on the secondary classifiers. The quartzite ores are both hard to crush and difficultto grind.The principal sulphide materials are bornite, chalcopyrite, and pyrite, chalcopyrite being the main copper-bearing mineral.The crystallization is coarse in the schisty ores, but it has been shown that even the 200 mesh (Tyler) material contains included sulphide particles. At the present time the sizing of the final tailing averages 80% through 200 mesh.

Jan 1, 1932

The Black Star lead and zinc ore-bodies, situated in the western zone of mineralisation at Mount Isa occupy an area 2000 ft. long with varying widths from 100 ft. to 300 ft. The strike is N5°W, and the average dip 60° West.To test at depth the potentialities of this area, an extensive diamond drilling campaign was commenced on 16th October 1927. It was continued, with from one to six machines working, until the end of 1931. During this period, 26 inclined holes, with an average depth of 1224 ft, and a total footage of 31,828 ft. were completed. A vertical hole, 2452 ft. deep, for comparative purposes, has been omitted.These drilling operations came directly under the charge of G J Gray, General Superintendent of Mount Isa Mines, and, in the early stages were supervised by E. D. McDermott, of the Mining Trust, London. The foremen, who were in charge of various sections of the drilling operations, were: H Vale, F Bray, J Winston and A A Sanstedt.

Jan 1, 1932

The discussion which followed the publication of my paper by the formert has, I think, enhanced its value. It may therefore be of interest to members of our Australasian Institute, who are not members of the Institution of Mining and Metallurgy, if I give a synopsis of the discussion.My attention was drawn to the fact that my paper did not make clear the extent of the improvement in furnace operations, which followed the use of coke of high quality; this comment applied more particularly to the lead content of slag. My failure to supply comparative figures in regard to the lead content of slag was governed by a condition which, I think, is of interest to metallurgists. As a result of industrial...

Jan 1, 1932

Around no subject of technical )uterest have prejudice and wrong-thinking in the past so wrapped a web of obscurity as that of the corrosion of metals.It is a matter which has primarily concerned the engineer, but the paucity of his training in chemistry and electrochemistry has been the stumbling block to a better understanding of its mechanism.Now that the more important conditions controlling corrosion have been scientifically.established, it can be seen that, with the exception of but a few of the minor points, the electrochemical laws enunciated by Faraday, Helmholtz; Nernst, and others, are sufficient to include all the facts of the process.The word corrosion (derived from the Latin rodere-to gnaw) is so often wrongly applied that a definition at this stage would be useful. As now understood, it means the dispersion and waste of the useful solid metal by conversion into a useless compound which mayor may not be retained on or near the metal remaining.Commonly the presence of these compounds is regarded as evidence of corrosion, but the converse is not necessarily true; the lack of visible corrosion products on a clean surface of metal is no criterion of the absence of this change. It may be difficult to prove that the erosion of such a surface has been caused by chemical and not by mechanical effects alone.

Jan 1, 1932

By Evans A. F

Arising out of the increasing demands for efficiency in modern ore-dressing operations has grown a requirement for fuller knowledge of the characteristics of the ore treated. In part, this is being met by improved methods of study of the mode of occurrence of the constituent minerals, and of the intricacies of their physical relationships.A typical instance of the need for such a study is the presence of some undesired mineral in a flotation concentrate or tailing, which may be due either to mechanical association through insufficient grinding, or to incomplete separation in the flotation operation.Again, with modern practice in fine grinding, which often requires that from 70% upwards of the ground ore shall pass a 200-mesh screen, it is obviously impossible to obtain data on comparative grinding efficiencies, for instance, unless there is adequate knowledge of the size-composition of the material passing the finest available screen.Studies like these can be made satisfactorily only after size-separation (which may be carried out conveniently by elutriation) and by actual visual examination with the aid of a microscope, and the minute size of the mineral grains to be examined has necessitated the development of a new technique of sizing and microscopic examination.

Jan 1, 1932

The resistance of lead to chemical attack and the ease of its fabrication has made it one of the most useful of the metals available to the chemical engineer and the electrometallurgist. It has proved to be of particular value in the manufacture of sulphuric acid, and since the conversion of the sulphur of pyritic ores into sulphuric acid is becoming the duty of the metallurgist, the corrosion resistance of this metal will be a matter of considerable interest to him from the standpoints of both producer and user. He realises that there is little to be gained in carrying the process of purification past the ordinary economic limit if little or nothing is to be added to its corrosion resistance, and he as user would not be willing to pay a premium for such purification if it can be shown that its reputed value has no scientific foundation.The metallurgist is well acquainted with the trouble and expense of meeting demands which have nothing torecommend them but prejudice and fancy. The valuable anti-corrosive properties of lead are very commonly ascribed to its forming insoluble compounds with the acids sulphuric, hydrochloric, carbonic, etc. If we trusted superficial visual evidence alone, such a view would receive strong support, but in the light of what we know of the mechanism of corrosion we must attribute its resistance to other factors much less obvious to casual inspection. Certainly there may be some mechanical obstruction set up to diffusion of the liquids towards the surface of the metal.

Jan 1, 1932

Owing to the 'creeps' and consequent movements in the mines, followed by the recent fire in the southern workings, the whole of the orebody above the 800 ft. level is now very much crushed and broken. The same applies to the hanging wall or overwall coutrny, which has subsided towards the workings, so that for some years past all development work within the lode has had to be carried out with extreme care.The continual but slow subsidence of the overburden into the stopes necessitates a periodical renewal of all gangways in the lode, and, as the subsidence amounts to as much as 60 ft. in places, these new gangways must necessarily pass through the mullock-filling of old stopes in addition to broken ore. They at times pass into the broken ground of the hanging-wall for some distance, where the orebody has widened underneath by the original folding and puckering.

Jan 1, 1932