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By R. J. SHAW

Oil shale has been defined as, "a compact, laminated rock of sedimentary origin yielding over 35 percent of ash and containing organic matter that yields oil when distilled but not appreciably when extracted with the ordinary solvents for petroleum." The oil-yielding organic matter in oil shale, commonly called kerogen, decomposes upon application of heat to form bituminous materials that are soluble in organic solvents and may be extracted from the inorganic residue. However, separation usually is accomplished by continuing the heating and thereby cracking the primary bitumens to gas and oil, which distill, leaving a carbonaceous material on the mineral residue. It has been suggested that this conversion takes place only at relatively high temperatures - 750°F or higher. On the other hand, other workers have found that transformation may take place to some extent at temperatures as low as 400°F. In either a solvent extraction or a destructive distillation process for separating organic material from the inorganic portion of oil shale, the quantity of heat required to raise the temperature of the oil shale sufficiently to induce a satisfactory rate of conversion of kerogen to oil is important in determining the design of an economical process. Likewise, the quantity of heat recoverable from a spent shale is important in determining the overall heat balance of the process. Published data on the specific heat of American oil shales are meager. Gavin and Sharp present data for two samples of Colorado oil shale, one from near DeBeque and one from Parachute Creek, and for a sample of spent shale over a temperature range of 68°F to 1940°F. McKee and Lydor present data on the specific heat of two samples of oil shale from near DeBeque, Colorado. Additional thermal data on various grades of oil shale over a wider range of temperature are needed in order to apply sound engineering practices to the design of equipment for processing oil shale.

Nov 1, 1947

By Victor J. Lynch

The Andover-Sulphur Hill mines are 12 miles northeast of Andover and 5 miles southeast of Newton, in Sussex County, N.J. The property is situated on the Lehigh Valley and Hudson River Railroad and half a mile east of U.S. Highway 206. It is connected with the main highway by a hard-surfaced county road. (See fig. 1.) Howard J. Hewitt of Lafayette, N.J., has under lease the Sulphur Hill tract, consisting of 28 acres, and has an option on the Tar Hill tract of 106 acres. The Tar Hill property adjoins the Sulphur Hill on the northeast. (See fig. 2.) The Andover-Sulphur Hill property is owned by the Lenape Corp. of Andover, N.J., while the Tar Hill tract is owned by the Crane Iron Co. of Phillipsburg, N.J. These mines produced iron ore during a period of about 100 years but have not been operated since 1880. Zinc and lead sulfides occur mixed with iron ores in the lower workings of the old mines. A diamond-drilling program was recommended to determine the extent of the sulfide mineralization in depth and also to explore further the iron-ore deposits on the property. The project was started October 6, 1942, and finished November 25, 1942.

Dec 1, 1947

By S. L. Windes

"INTRODUCTION For a number of years the bureau of Mines has been engaged in the detection, recording and interpretation of earth- and air-transmitted disturbances, man-made and natural, related to mining operations. For the measure¬ment of such disturbances, special equipment was developed (1, 2, 3, 4, 8) 3/ and results of the measurements have been reported (5, 6; 7,9).In general, the ranges of amplitude end frequency of vibration encountered and recorded in the earth-transmitted disturbances were 0.00005 to 0.1 inch and 5 to 5,000 cycles per second; in the air-transmitted disturbances, pressures ranging from 0.001 to 100 pounds per square inch and 0 to 20,000 cycles per second were recorded.One characteristic of the earlier tests was that either the arrival time of the disturbance to be recorded was predictable or the recording speed was slow enough so that the record covered extended periods of time (for example, 4 hours). As the investigations continued, it became apparent that a recording device was required that would respond to transient vibrations arriving at indeterminate times and at the same time provide a permanent record of displacement or acceleration versus time on a scale that would permit the analysis of waves having frequency components up to 10,000 cycles per second. A film or paper speed of 720 inches per second was found to be adequate, as this provides approximately 3/4 inch of record for each 0.001 second."

Dec 1, 1947

By Clyde L. Holmberg, Paul Zinner

"INTRODUCTION In view of the large tonnage of low-grade iron ore and iron-bearing material known to exist at the western limits of the Gogebic range, the Bureau of Mines undertook an investigation of the area for the purpose of evaluating the iron-bearing formations as sources of iron for possible future utilization.After 6o years of exploration an, development on the Gogebic range, the area investigated by the Bureau represents the known western limit of direct-shipping ore mined from operations on the Gogebic range.An area about 2 miles in length between the villages of Pence and Iron Bolt in Iron County, Vic., was selected for investigation, and trenches wore excavated through the overburden and fully across the iron-bearing formation to obtain 108 bulk samples for beneficiation tests. Exhaustive tests involving gravity and flotation methods, magnetic separation, and magnetizing roasts followed by magnetic separation were conducted on the samples to determine the ammability of the individual formations and the entire iron-bearing zone to beneficiation.Empirical data on the character and mineral content of the formations arc tabulated herein, as well as the results of the beneficiation tests."

Dec 1, 1947

By F. K. McIntosh, A. F. Robertson, T. J. Ballard

"INTRODUCTION Molybdenum deposits occur in Halifax County, N. C., near the eastern border of the Piedmont province. The deposits are associated with a small granite body about 2 miles long and half a mile wide. Molybdenite is the principal ore mineral and is found as disseminations or thin stringers in quartz veins and occasionally in the enclosing granite or schist wall rock.The deposits were investigated by Almon F. Robertson and Charles J. Cohen, engineers of the Bureau of Mines, in 1942 and 1943, who recommended that the deposits be explored to supplement reserves of critical war minerals.The Bureau made the initial exploration of the deposits in July 1943 and continued its work to January 1944. Drilling was resumed from July to December 1946 to test the deposits at &eater depth than had been attempted during the previous exploration."

Dec 1, 1947

By M. M. Fine

"INTRODUCTION One of the principal activities of the Bureau of Mines during the recent war was to help to increase the supply of strategic and critical minerals. Fluorite was one of the most critical of the nonmetallic minerals because of the increased demand for it as a flux in basic open-hearth and electric steel furnaces and as a raw material for the production of artificial cryolite used in the aluminum industry. Wartime developments in the technology of hydro-fluoric acid, such as the use of the anhydrous acid as a catalyst in high-octane-gasoline production and the use of organic fluorides as carriers for insecticides, also increased the demand for acid-grade fluorspar. 2/ In 1943 the consumption of acid-grade fluorspar was advancing at a more rapid rate than production and was only slightly less than production during the latter half of the year.The outlook for the postwar market for fluorspar is encouraging. Steel production is expected to remain high until the domestic demand for commodities not manufactured during the war is satisfied. The uses for hydrofluoric acid also are expected to increase under the impetus of war-initiated research. In consideration of these and other factors some authorities predict a new peacetime demand for fluorspar equal to 60 to 75 percent of the war production, 5/ 6/ and others believe that the fluorspar industry will be permanently expanded. 7/"

Dec 1, 1947

By T. F. Mitchell, B. K. Shibler, J. V. Batty, W. G. Sandell, G. M. Potter

"INTRODUCTION The Park City district, situated 30 miles east of Salt Lake City, Utah, in the Wasatch Mountains, Is a well-known producer of lead, zinc, and precious metals. Nearly continuous production has been maintained from the dis¬trict since its early discovery about 1870. For approximately 50 years, gravity milling methods were employed to beneficiate Park City ore, and during that time tailings from the mills were sluiced down Silver Creek and deposited on lands below the camp for 7 miles.Owing to the large tonnage of tailings deposited along Silver Creek, considerable work was done in the past in the attempt to develop a low-cost concentration method for re-treating this material, but no-method was found that was economically feasible. The Bureau of Mines was asked to conduct beneficiation tests on Park City tailings in November 1944, and metallurgical studies were initiated at that time. This report summarizes the results of laboratory ore-dressing studies made on samples from the Grasselli deposit."

Dec 1, 1947

By H. L. Riley, B. W. Gandrud

"INTRODUCTION The Bureau of Mines, United States Department of the Interior, with the cooperation of the University of Alabama and coal producers, has made a series of washability studies to obtain technically and commercially important data regarding the productive coal beds of the State. Based on the system followed in these studies, this report consists principally of screen-sizing and float-and-sink data on the Clark and Gholson beds at Boothton, Ala. A previous washability study 4/ has been made on the Clark bed at Marvel, Ala.SAMPLING AT MINESThe coal from the Gholson and the Clark beds was sampled at the tipple which receives the output,the Boothten No. 3 and No. 4 mines. These two mines are on the Gholson and Clark beds, respectively, but the coal. from both mines is mixed on the tipple and washed in the same washery. The samples taken were minus 4-inch raw coal. The plus 4-inch raw coal is hand¬picked and not washed. AS the 4-inch screen had a capacity in excess of the output of the mines, it was stopped at the end of each mine-car trip. By Observing from which mine incline each trip was hoisted, a separate sample from each bed was cut from the discharge stream of an endless belt which conveys the through 4-inch raw coal to the bin ahead of the washer. The output from each bed was sampled uniformly over the period of a working shift. The two washability samples weighed approximately 3,000 pounds each."

Dec 1, 1947

By W. A. Calhoun

"INTRODUCTION A letter from S. D. Strauss, vice president of Metals Reserve Company, Washington, D.C., dated May 22, 1945, to the chief of the Metallurgical Branch, Bureau of Mines, in Washington; includes the following: Because of the present critical shortage that exists in the supply of corundum required by certain industries in war production, the Reconstruction Finance Corporation, Mr. W. C. Keeley, Vice Chairman for Metals and Minerals, War Production Board, has recommended that the Reconstruction Finance Corporation though Metals Reserve Company, proceed with preliminary mill testing of the corundum ore in Gallatin County, Montana, and that the results of that testing be transmitted to the War Production Board. If the results of the testing work are considered satisfactory, Metals Reserve Company will then provide for the actual mining and milling of the ore for the production of corundum concentrates.Pursuant to the above stated recommendation by the War Production Board, Metals Reserve Company desires to make -use of the facilities of the Bureau of Mines testing plant at Rolla, Missouri, for conducting sink and float and other concentration tests on representative samples of the Montana corundum ore. Two, and possibly three samples of ore are to be tested which will have an aggregate weight of approximately 50 tons."

Dec 1, 1947

By E. O. Binyon

"INTRODUCTION The Gibellini manganese—zinc-nickel deposits, are in southeastern Eureka County, Nev, T. 15 N., R. 53 E. M.D.B.M. 27.5 miles south of Eureka, the county seat.The partly explored deposits, locally known as the Black Iron or Gibellini property, were examined in May 1944 by an engineer 3/ of the Bureau of Mines, who recommended that the deposits be explored further by means of core drilling. The proposed program called for drilling six diamond—drill holes, or eight if necessary, and for trenching at two places — 200 feet northeast and 280 feet west of the shaft on the main deposit.In 1946 the project was set up, and In July, of that year diamond drilling as started. Six holes were drilled for a total length of 1,198.5 feet. No trenching or other exploratory work as done. Work on the project was stooped. October 30, 1946.OWNERSHIPAccording to county records, the property comprises a group of 13 unpatented lode claims, and ownership is divided among Louis P. Gibellini,Louis P. Gibellini and wife (both of Eureka, Nev.), and the International Smelting & Refining Co., of Salt Lake City, Utah. Five claims of the group - the Black Iron No. 1, Black Hill No. 2, Manganese No. 3, Flat No. 1, and Flat No. 2 - are owned by Gibellini. Three claims - the Black Hill No. 1, Black Iron No. 3, and Manganese No. 4 are owned jointly by Mr. and Mrs. Gibellini, and the International Smelting & Refining Co. owns the remaining five - the Black Iron No. 4 and No. 5, and Black Hill Nos. 4, 7, and. 9."

Jan 1, 1948

By J. H. Jacobs

The first authorization, in November 1940, was for a plant of only several hundred pounds capacity at Boulder City, Nev. Improvements in the process and subsequent additions to some sections have enabled the plant to produce more than 2,000 pounds of manganese per day for substantial periods. By the time pilot-plant operations were suspended in June 1945, over 1,500,000 pounds of metal had been produced. The future of electrolytic manganese production obviously depends not only on satisfactory development of methods but on availability of raw material and demonstration of valuable uses. Investigations of manganese-ore deposits in this country, made since 1938 by the Bureau of Mines, have revealed large amounts of ore suitable for making electrolytic manganese. At first the pilot plant was operated on ore from the Three Kids mine near Las Vegas, Nev. After practical features of the process had been worked out, other ores from throughout the United States were tested in the pilot plant. The purpose of this paper is to compare the results obtained on the following ores: Three Kids; Ladd mine, Tracy, Calif.; Chamberlain, S. Dak., nodules; and ore from Metals Reserve stockpiles at Deming, N. Mex.; Cushman, Ark.; and Philipsburg, Mont.

Dec 1, 1947

By James L. Elder, J. P. Capp, James J. Dowd

The Bureau of Mines and the Alabama Power Co., jointly, conducted the first experiment undertaken in the United States in underground gasification of coal in place, at Gorgas, Ala. Milton H. Fies, manager of coal operations, Alabama Power Co., proposed the cooperative investigation to Arno C. Fieldner, chief, Fuels and Explosives Branch, Bureau of Mines; and assisted in supervising the experiment. The objectives of the experiment were to determine whether coal in place could be burned successfully and whether the burning could be controlled; the effect of the fire on the coal bed and the overlying strata; and the yield and quality of gas that could be obtained.

Aug 1, 1947

By G. E. McElroy

This report discusses the construction and use of an all-pressure psychrometric chart in which the requirements of simplicity of appearance and absolute accuracy have been waived, to a certain extent, to provide for the rapid determination of psychrometric data and for the rapid solution of air-conditioning problems of major interest to the mining industry. Many mines in which air-conditioning problems are important are situated at elevations far above sea level and embrace great differences in elevation - in excess of 8,000 feet in certain mines - throughout their airflow circuits. Under these conditions, the effects of variations in the pressure of the atmosphere upon the physical properties of the mixture of air and water vapor of which it is composed are considerable and should be taken into account in the solution of problems. The simple types of psychrometric charts in common use, such as the Carrier, Bulkeley, Hill, and Goff (American Society of Heating and Ventilating Engineers Guide), are not generally suitable, in that they are drawn for a single barometric pressure - 29.92 inches mercury.

Dec 1, 1947

By J. S. Kennedy, R. G. Omeara

Beryllium is a strategic metal of ever-increasing peacetime importance because of the unusual properties of beryllium-copper alloys. These unusual characteristics are the combination of high strength and hardness, high fatigue resistance, and high wear resistance in alloys that have the corrosion resistance of copper. The principal industrial source of beryllium is the mineral beryl, a beryllium-aluminum silicate that occurs in pegmatites associated with quartz, feldspar, mica, and smaller amounts of various accessory minerals. The beryl is usually recovered in processing the pegmatites for the recovery of some of the other mineral constituents. Pegmatite deposits are found in various parts of the United States, but those in the Black Hills of South Dakota are the source of most of domestic production. The beryl marketed from the South Dakota pegmatite deposits occurs as coarse crystals, which are obtained by hand sorting. These pegmatites also contain other valuable minerals.

Jan 1, 1948

By Thomas Fraser, William L. Crentz

"INTRODUCTION Sulfur is a most damaging impurity in many of our American coals. From the older coal industry of Europe and Britain we can apparently learn but little about the problem of preparing and using high-sulfur coal. Although washing has long been established there for controlling ash content, sulfur is referred to rarely, as the important deposits are singularly low in sulfur.On the other hand, widely distributed coal deposits of America differ tremendously in sulfur content. Many of the more extensive beds contain too much sulfur for metallurgical use, and almost everywhere except in the Rocky Mountain and Pacific coast regions sulfur control is at least a potential problem. American coal-preparation engineers are confronted not only with great variations in the total quantity of sulfur in coal but with an intricately varying pattern of the physical and chemical forms in which the sulfur occurs. It must be conceded that the baffling problem of sulfur reduction in coal is as yet substantially unsolved, for there are but few isolated instances in which we have been able to prepare a satisfactory metallurgical fuel from coals containing as much as 2.0 percent sulfur in the raw state.It has been assumed generally that organic sulfur, being chemically combined with carbonaceous matter, is distributed throughout the coal matter and that it remains unchanged in the clean-coal part of the product during washing.Sulfur that may be washed out of the coal is that part that is combined with the iron in pyrite lenticles associated with the coal. In most of our coals it has been found that, besides the visible bands, lenses, and flakes of pyrite, extremely small and even microscopic particles of pyrite 4/ are distributed through the coal matter. Only the free, relatively coarse pyrite particles .are removed by conventional coal-washing devices, and usually most of the sulfur is still left in the product."

Dec 1, 1947

By W. M. Traver

As a direct result of the second World War, consumption of nickel in the United States has increased to such an extent that it has been considered timely to investigate undeveloped deposits of the nickel minerals. Funds were made available to the Bureau of lines in 1941 to investigate the extent, occurrence, and quality of nickel ores in the Mirror Harbor area. The Federal Geological Survey mapped' and studied the area during the summer of 1941 and Robert S. Sanford, an engineer of the Bureau of lines, made a preliminary examination in June 1942. A contract for drilling the deposits under the direction of the author was let in July 1942.

Jan 1, 1948

By M. A. Elliott, F. W. Brown

"INTRODUCTION During the recent war the Bureau of Mines, at the request of one of the armed services, investigated the hazards that night be encountered 5n handling perchloric acid, particularly if spilled on certain materials. The hazardous nature of perchloric acid when mixed with reducing agents had been known qualitatively, but it was desired to obtain quantitative data on the explosion hazards of such materials. Accordingly, tests were made to determine the sensitivity of mixtures of perchloric acid and oxidizable materials to initiation by heat, impact, sparks, flame, and explosive impulses. This report summarizes the results of those tests.PROPERTIES OF PERCELORIC ACIDAnhydrous perchloric acid is a colorless,hygroscopic, volatile, mobile liquid that fumes in the air. The anhydrous acid is unstable at ordinary temperatures, and therefore the commercial acid is a water solution containing either 60 percent or 70 percent by weight of the anhydrous acid. The commercial acid is widely used in chemical analysis, frequently to oxidize organic material. If proper precautions are not observed, such an oxidixation may become exceedingly rapid and result in an explosion. Several such explosions involving the acid are mentioned in the literature. 4, 5, 6/"

Jan 1, 1948

By John I. Kasteler, John H. Hild

"INTRODUCTION The South Hecla mine, one of the principal mines of the Alta United Mines Co., is situated at Alta in thee Little Cottonwood mining district, about 30 miles southeasterly from Salt Lake City, Utah. The mine has produced copper, lead, zinc, gold, and silver, and is reported to have been one 'of the principal sources of this country's bismuth from 1912 to 1925. The tungsten mineral, scheelite, has been found but has not been recovered. The extreme need for these minerals during World War II prompted an examination of the property by the Bureau of Mines and resulted in an unpublished report entitled ""The South Hecla Mine, Salt Lake County, Utah"" (fig. 1).A Bureau of Mines project 3301 was initiated, and operations were started early in 1943. The primary purpose of the project was to increase substantially the reserves of bismuth and tungsten ores. The critical situation in regard to lead, copper, and zinc developed during the early stages of the operation, and the work was expanded to include the development of ores 'of these metals.An investigation of 'the Albion, Rustler, and Greeley workings adjoining the South Hecla mine was made, and this work is also described (fig. 2); ACKNOWLEDGEMENTSIn Its program of investigation of mineral deposits, the Bureau of Mines has as its primary objective the more effective utilization of our mineral resources to the end that they make the greatest possible contribution to national security and economy. It is the policy of the Bureau to publish the facts developed by each investigative project as soon as practicable after its conclusion. The Mining Branch, Lowell B. Moon, chief, conducts preliminary examinations, performs the actual investigative work, and prepares the final report. The Metallurgical Branch, O. C. Ralston, chief, analyzes samples and performs beneficiation tests."

Jan 1, 1948

By V. F. Parry

"INTRODUCTION During the war period the Bureau of Mines expanded its investigations on western coals principally in connection with Investigations of raw material resources for western steel production. Owing to the expansion of the steel industry, there was some concern regarding the availability of suitable coking coals; end because of the potential steel shortage, the production of sponge iron, using the lower-rank fuels, was considered. Work was conducted by the Bureau of Mines on exploration projects and on testing of coals both at the Central Experiment. Station at Pittsburgh, Pa., and at the Bureau of Mines Station at Golden, Cole.The results of these investigations are being published by the Bureau in several reports of investigations and technical papers. In making this resume of coal investigations, the work done by the Bureau of Mines at Pittsburgh in the Mining and Coal Carbonization Sections will be discussed and the investigations at Golden described in greater detail.INVESTIGATIONS OF WESTERN COALSThe Mining and Coal Carbonization Sections of the Coal Division, Bureau of Mines, under the supervision of A. L. Teeny es and J. D. Davis, respec¬tively, conducted many field investigations to locate and evaluate new sources of coking coals. Drilling explorations were made in Colorado, Wyoming, Utah, New Mexico, and Washington and revealed two important new reserves of coking coal. The first one studied was the Willow Creek bed at Kemmerer, Wyo., which was reported in 1945.3/ A recoverable reserve estimated at 11,200,000 tons was blocked out, and samples of coal were extracted for coking tests. The coking properties of the coal were not quite equal to those of Sunnyside coal, but it was indicated that a 50-percent blend of the Willow Creek with Lower Sunnyside will produce a satisfactory metallurgical coke based on Columbia steel standards."

Jan 1, 1948

By F. K. Shelton, J. C. Stah, Ruth E. Churchward

A study of the hydrometallurgy and electrowinning of cobalt from various domestic ores has been in progress at the Boulder City, Nevada, Experiment Station since February 1940. Previous reports covering certain phases of this investigation have been published. This report covers the research and pilot-plant work on the production of cobalt metal from cobalt-copper ores from the initial experimental work on crude ore through continuous operation. The ore types were from the Blackbird District, Lemhi County, Idaho. The initial tests were made with concentrated ore which was received by air mail and these experiments were expanded both in size and scope. After the laboratory was continued, improved, and extended tests were reported. Sufficiently advanced, a continuously operated plant producing 250 pounds of electrolytic cobalt per day was operated from June 15 through July 15, 1944.

Jan 1, 1948