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The present study investigates the nature of gold mineralogical distribution and association in a Cu-Au flotation circuit (1.6 g/t Au, feed head grade). The approach used in this study involves a combination of bulk gold assay and quantitative X-ray diffraction (QXRD), on a size-by-size basis, followed by QEMSCAN analysis on the -75+53 µm, -53+38 µm and -38+20 µm size fractions. The QXRD and QEMSCAN analysis showed that gold mineralogy is complex and fine-grained in the flotation feed, particularly in the -38+20 µm size fraction. Gold and pyrite concentration follow each other closely, suggesting gold-pyrite association. Quartz as the major gangue mineral shows a bi-modal distribution with respect to particle size. The identified gold particles were completely locked (~94 %) in pyrite as fine inclusions and 6 % locked as complex aggregates (-75+53 µm size fraction) whereas in the -38+20 µm size fraction, the identified gold grains occur as fine inclusions (~1-3 µm) within pyrite and silicates. However, in the intermediate size fraction (-53+38 µm), 75 % of the identified gold grains (10-22 µm) were over 90 % liberated and 25 % associated and locked in pyrite and complex aggregates (~2-4 µm). The identified gold grains in the -53+38 µm size fraction occurred as native and electrum with varying silver concentration between 8 and 20 % by weight. In the -38+20 µm size fraction, a gold telluride was also identified. Based on the mineralogical analysis of the feed, possible flotation strategies are discussed. Optimizing the flotation of pyrite is suggested as the primary Au recovery strategy. Keywords: flotation, pyrite, gold, liberation, QXRD, QEMSCAN

Sep 1, 2012

By J. Masinja

The mining industry is known to be a potential major contributor to the industrial development of any economy. Large-scale mining has been going on in Zambia for the last 100 years. The impact of mining in Zambia has been to create a development corridor along the line of rail to the Copperbelt Province, where hitherto, mining was concentrated, and then to develop a large consolidated high-density economic zone covering an area of about 72 km by 60km. This area is home to a number of very large integrated copper/cobalt mining complexes. The mining zone has expanded to the Northwestern Province in the last 10 years, where the largest copper mine in Africa now exists, having produced about 300 000 tonnes of copper in 2011. The total output of the Zambian mining industry is now about 820 000 tonnes per annum with projections of reaching 1.5 million by 2015, due to new Greenfield investments expected to come online by then. These new mining industry developments have come on the back of strong and sustained high base metal prices, in the last 10 years or so, due to demand mainly from China and India. This new lease of life has increased the contribution of the sector to the national treasury. The mining industry in Zambia has undergone a very important ownership restructuring with the sale of the previously Government owned parastatal, Zambia Consolidated Copper Mines (ZCCM) which dominated the sector, to allow for private sector participation. The privatization process lasted from about 1995 to about 2002. The recent growth of the mining sector has unfortunately not been matched by an adequate supply of skilled manpower for various reasons. These include: (i) A lack of strong in-house training strategies by the new mine owners (ii) Decrease in industry support to the training institutions (iii) The demise of and restructuring of ZCCM which has consequently limited the Government human resources planning tools for the mining sector (iv) The cyclic nature for the fortunes of the sector has lead to fluctuating interest of student recruitment into training institutions (v) Limitations, both staff and equipment, in the training institutions (vi) A re-structuring of the training institutions This paper examines the current status, and student output from tertiary training institutions for the mining sector in Zambia. This is then compared to the skilled labour demands of the sector. The various cause and effect issues are considered and a proposal on how this skills gap could be addressed sustainably is proposed. Keywords: skills gap, graduate training, quality of graduates

Sep 1, 2012

By V. Hema

Granular materials are widely used in process industries, such as chemical, pharmaceutical, cement, food, detergents, and fertilizers. Mixing, blending, calcining, reduction, heating, and granulation of these materials are frequently carried out in rotating cylinders. In all of these processes, the mixing and segregation of these granular materials is important as this controls the secondary phenomena in the rotating kiln such as heat transfer to the material. A significant amount of work is available in the literature but to date these efforts have not been able to capture the important parameters affecting the mixing and segregation in rotating kilns. In addition, the range of parameter values studied so far is rather limited. Simulations of granular materials are based on either discrete elements or continuum models. The discrete element methods (DEM) combine semi-empirical models for the inter particle interactions with the equations of motion from classical mechanics to simulate the explicit paths of all granules in a rotary kiln, thus yielding realistic predictions of the mixing process. This approach is very demanding computationally, which strongly limits the number of granules and the number of revolutions in a simulation. Continuum models dispense with the discrete particles and can therefore be scaled up more easily. But the constitutive relations that serve as the foundation for continuum modeling are difficult to come by, and often only applicable to specific systems and conditions. Here we have chosen DEM simulation for investigating the mixing and segregation behavior of granular materials in a rotating cylinder. This work is directed towards demonstrating the capability of the prediction of the mixing and segregation behavior of granular materials in a horizontal rotating cylinder through discrete element simulation. Further the effect of particle size and rotational velocity on the mixing and segregation behavior is investigated. The simulation results are quantified in terms of mixing index, mixing rate, segregation index and percolation index. Keywords: DEM simulation, granular mixing

Sep 1, 2012

The status of utilization of copper ore resources, and the application and development of biohydrometallury technology in the world is reviewed. Based on the characterization of Zambia?s copper resources, biohydrometallurgy technology is shown to be a practical approach to extract and utilize the enormous low grade copper resource, such as ore tailings and low grade copper ore in this country. Through the cooperation of CSU, China and MMMD, Zambia, ?CNMC-CSU Demonstration Base of Biohydrometallurgy Technology in Zambia? was launched and several biohydrometallurgy plants are being constructed. This indicates that the biohdyrometallurgy technology would be applied soon in Zambia and in the whole Africa. Biohydrometallurgy technology stands as an efficient alternative to the traditional pyrometallurgy process and it can be the key to unlock mineral resources value. Keywords: biohydrometallurgy, low grade copper ore, Zambia, Central South University

Sep 1, 2012

By M. Naymanbayev

The characteristics of the mineral composition of ores and valuable set of components: the technology of processing depending on the type of mineralization, the nature of the impregnation of ore minerals and their composition have been considered. There have been given technological schemes for processing concrete objects. The analysis of fitness fields for industrial development (degree of scrutiny, the effectiveness of developed enrichment and hydrometallurgy technology) has been provided.

Sep 1, 2012

By J. Leite

In a small-scale mining in Brazil?s northeast, scheelite were exploited since 1940?s using a traditional gravity concentration flowchart (composed by jigs and shacking tables) that operates with low efficient for fine particles. Tailing of this plant was submitted to chemical, mineralogical and size characterization. Results pointed 50% smaller than 74µm with a grade of 0.11% WO3. The particle?s size is an important operational variable to heighten recuperation by shacking tables. Tests using Falcon SB40 centrifuge concentrators and shacking table were realized, optimizing their operational variables. Based on the tests results a new flowchart was proposed for concentrating and tailings recovery.

Sep 1, 2012

By M. Maldonado

A flotation bank is a serial arrangement of cells. How to optimally operate a bank remains a challenge. This article reviews three reported strategies: air profiling, mass-pull (froth velocity) profiling and Peak Air Recovery (PAR) profiling. These are all ways of manipulating the recovery profile down a bank, which may be the property being exploited. Mathematical analysis has shown that a flat cell-by-cell recovery profile maximizes the separation of two floatable minerals for a given target bank recovery when the relative floatability is constant down the bank. Available bank survey data are analyzed with respect to recovery profiling. Possible variations on recovery profile to minimize entrainment are discussed.

Sep 1, 2012

By B. K. Gorain

Mining of low grade deposits along with the necessity to design and operate flotation plants with high throughput presents unique metallurgical and environmental challenges that need to be addressed to reduce project risks, improve project economics and to sustain the profitability of operations over the life of a mine. Some of the key challenges include poor recovery of valuables and concentrate quality issues due to complex mineralogy, the need to use poor quality water such as brackish or sea water, reduce environmental impact from the process, integrate flotation with hydrometallurgy to maximize precious metals recovery, escalation of capital and operating costs, use of unproven technology and constant use of larger equipment, high ore variability, worldwide constraints on resource availability and an ever increasing need for reliable metallurgical input to financial models to evaluate economic viability of projects. The need to develop effective solutions to these problems in a short time frame is becoming a key to the success of any new project and for sustaining the profitability of a mining operation. An integrated multi-disciplinary approach to problem solving is crucial with the need for a more lateral thinking along with strategic partnerships and collaboration involving the right players. This paper presents some of the key findings based on experiences from a large number of challenging projects and operations focused on solving complex flotation problems Keywords: mineral processing, flotation, flotation problem solving, flotation optimization, plant design, innovation

Sep 1, 2012

By Cagri Emer

In conventional mechanical flotation cells, when the size of particles exceed a particular value, that is of the order of 100 µm for metal sulphides, the recovery of particles decline rapidly. It appears that the turbulence in the agitated vessel is sufficiently intense to rupture the forces of attraction between the particles and the bubbles, so the large particles are flung off the bubbles in the turbulent field. It has recently been suggested, that a fluidized bed would be a very favorable environment in which to contact bubbles and the particles. In a fluidized bed, particles are supported by rising flow of fluid, which separates them from each other and allows them to move freely while remaining close together. In this novel method, bubbles injected into the fluidized bed are able to rise through it, colliding with hydrophobic particles, transporting them to the top of the column where they can form a froth layer that overflows into a launder. The flow in a fluidized bed is generally slow and nonturbulent, and preliminary experiments have shown, that it is possible to collect mineral particles as large as 1 mm and coal particles as large as 5.5 mm. If the upper particle size limit can be extended, there could be significant reductions in the overall energy consumption in concentrators. Calculations show for example that if the top size for flotation could be increased from 100 µm to 400 µm, there would be a reduction in grinding energy of the order of 40%. It is therefore, important to study the mechanism of coarse particle capture in fluidized beds. In this work, the factors governing the capture rate of particles, particularly the particle and bubble size, the fluidization velocity and the superficial gas velocity have been investigated, and the results will be presented.

Sep 1, 2012

By A. Gülmez

The complex ore deposit containing fluorite, barite and bastnaesite minerals is located in Beylikova Region of Sivrihisar town of Eskisehir Province of Turkey. The ore contains 40.80% CaF2; 35.35% BaSO4; 2.01%Ce; 1.5% La; 0.39% Nd and 0.1% Th. Barite recovery from this ore by flotation of the HCl leached tailings is presented in this paper. Rare earths are recovered by leaching. The leached residue (tailings) containing fluorite and barite is subjected to froth flotation to recover barite. The effect of pH and collector concentration on the flotation of barite have been studied in this work.

Sep 1, 2012

By Fangming Liu

The key problems of current flowsheets and equipments are analyzed. A new steel slag's crushing flowsheet whose key equipments are the improved inertia cone crusher and inertia vibrating jaw crusher is proposed. An advanced two stage open-circuit crushing method is adopted in the flowsheet, with 90% of particle size crushing under 6mm. Using inertia vibrating technology and selective crushing principle the crushers can realize steel slag separating fully into steel and slag and with flexible transmission mechanism the crusher can be protected when iron lump is passing. The flowsheets can enhance the recovery of metal greatly, and expand the application range of tail slag and added value.

Sep 1, 2012

By S Brochot

During the development of a mining project, samples are taken for metallurgical tests. The sample can be a composite sample made of material coming from a selection of various drilling products or a sample coming from a mining test. This sample can represent several tonnes of material which are analysed and split to be used in various tests.In the current case, a composite sample is dedicated to semi-autogenous grinding (SAG) pilot plant tests. The property of interest is then the size distribution of the material. The sample is mixed and a subsample is taken to measure the size distribution which is considered as the feed size distribution. Then the remaining material of the sample is divided in several subsamples for batch grinding tests at different operating conditions. The product of each grinding test is then analysed to measure its size distribution.The grinding performances are analysed at the light of the measured size distributions for feed and product. But what is the accuracy of the measurement of these size distributions? What is the variability of the feed knowing each feed is just a subsample of the initial sample?The Pierre Gy theory of sampling answers these questions.The current paper presents, through a real example, the calculation of the measurement error of the size distributions and the variability of the feed between the different tests. The uncertainties of the grinding performances are then calculated and their impact on the results interpretation is then analysed.CITATION:Brochot, S, 2012. Sampling for grinding pilot plant test - the effect of size distribution variability, in Proceedings Sampling 2012 , pp 127-134 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 21, 2012

By D M. Marques, J F. C L Costa

The estimation of process plant head grade is not trivial and is a source of constant dispute within the mining industry. Grade estimates informed by the short term mine planning are frequently not reproduced by sampling the continuous flow of ore at the plant. Head grades are normally obtained by periodically sampling the continuous flow during a day or shift, and taking the average of the multiple increments collected. The standard error of this mean grade depends on the ore variability and the frequency (number) of aliquots extracted. The more increments are taken the higher is the precision on the calculated mean. Variographic experiments are normally used to map grade variability along a certain period of time and the extension variance is derived from this variogram. This experiment is time consuming, expensive and cumbersome. Mining industry personnel rarely apply this approach. Additionally, a temporal variogram can vary from day to day as different ores are mined along the life of the mine. This paper investigates a novel approach based on simulating the grades feeding the processing plant. In situ 3D grade models are built using geostatistical simulations. Grade spatial continuity and variability are reproduced in models that mimic the real deposit. These models are used in mine planning and scheduling transforming a 3D block model into an one dimensional string of values feeding the plant (one dimension flow). These grades have the statistical characteristics of the unknown real grades and can be sampled to emulate a variographic experiment. The results showed consistency and adequacy to estimate the sampling error (Gy, 1998 p 31) for various sampling intervals using the simulated grades. Also the results show a variographic experiment can change significantly from time to time, as ore changes and a selected sampling protocol can become obsolete if not adjusted for ore variability.CITATION:Costa, J F C L and Marques, D M, 2012. Defining a sampling strategy for a continuous flow supported by geostatistical simulations, in Proceedings Sampling 2012 , pp 3-8 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 21, 2012

By B W. Atkinson

Full-stream mechanised sampling apparatus, that collect a full cross-sectional increment from the complete screen discharge, will always be the preferred option for sampling screen overflows. However, the reality is that provisions for automated sampling are rarely, if ever, provided at the discharges of individual screens within beneficiation plants.Sampling from the discharge of high capacity vibrating screens, especially multi-slope screens, is subject to sampling bias, due to the stratification of the ore that occurs on the vibrating screen deck. The stratification in the vibrating bed translates to a stratified falling stream at the discharge end of the screen, typically with smaller particles at the back of the falling stream and large particles at the front of the falling stream (Figure 1).The chemical and physical characteristics of heterogeneous ore (mineral or coal) particles vary significantly with particle size. If samples do not correctly reflect the source material size distribution, they will be biased and the resulting analytical/assay data will not reflect the actual physical nor chemical characteristics of the source material.Prior published data for coal preparation research (Australian Coal Association Research Program) has demonstrated that a bias appears to exist for samples collected from high capacity multi-slope screens.A new form of sampling scoop has been developed with the aim of overcoming this issue.Bias was evaluated at a coal preparation plant by comparing the desliming screen overflow size distribution to that for æreferenceÆ coal preparation plant feed samples collected using the recognised stopped-belt technique. The study procured 20 sets of comparison samples in order to ensure statistical relevance.Two forms of sampling device were employed for the multislope screen discharge.A conventional square aperture scoop was demonstrated to exhibit a significant coarse bias, in that the resulting samples exhibited a significantly coarser size distribution compared to the reference samples. In other words it was evident that the conventional scoop æfavouredÆ material from the front of the falling stream.A new æcollapsibleÆ sample scoop was evaluated in parallel, and its samples were found to exhibit no relevant bias.CITATION:Atkinson, B W and Swanson, A R, 2012. A new method for sampling from high capacity screens, in Proceedings Sampling 2012 , pp 89-94 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 21, 2012

By K H. Esbensen

The critical role of representative sampling is featured and illustrated by selected examples from the geosciences and beyond. As there already are many demonstrations of the potential (and potentially large) economic consequences of ignoring proper standards with respect to representativity, eg for mining and minerals processing companies, which æstand to lose millions of dollars by failing to optimise exploitation of their mineral resourcesÆ, such need no further iteration here.This keynote lecture, rather, takes a point of departure from the opposite perspective: what is to be gained by a scrupulous stand for representativity? Honesty, reputation, credibility, market advantage - is what!CITATION:Esbensen, K H, 2012. The critical role of representative sampling, in Proceedings Sampling 2012 , pp 9-12 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 21, 2012

By E du Plessis, M Rowley, M Fallon, F Golenya, R Swanson, I Robertson

"Check sampling programs were undertaken at Barrick Australia Pacific LimitedÆs Lawlers and Plutonic mine sites in Western Australia. The programs identified that the sampling, sample preparation and assaying protocols required modification to ensure acceptable precision (reproducibility) for each gold mineralisation type. These case studies describe the processes used to identify the: inconsistent precision different types of test work programs that were conducted to quantify the appropriateness for each mineralisation type steps used to modify the protocols.The type of test work conducted included: a duplicate series heterogeneity test for particulate gold mineralisation in the Lawlers gold deposit screen fire assay test work on duplicate subsamples for arsenopyrite associated mineralisation at the Plutonic gold deposit.Each test work program required a detailed scope specifying the sample selection criteria, sample preparation and assaying steps. The aim of the test work flow chart design was to ensure the assay precision between the different particle sizes or duplicate sample pairs could be measured and calculated. In the screen fire test work the true grade of the primary sample was calculated and compared against each subsample.A high quality assay laboratory was utilised for the test work. All samples were fire assayed and the gold grade determined using a gravimetric finish. The assay results were validated and the data was analysed using tables and graphs in spreadsheets. Following data analysis a modified sample preparation and assaying protocol for each mineralisation type was designed for use by the principal assay laboratories. Following implementation of the new protocols, routine check samples were collected during the sample preparation and assaying stages to monitor the performance of the new protocol.CITATION:Fallon, M, Rowley, M, Du Plessis, E, Golenya, F, Robertson, I and Swanson, R, 2012. Confirming the sampling, sample preparation and assaying protocols used at two Yilgarn gold deposits, in Proceedings Sampling 2012, pp 47-62 (The Australasian Institute of Mining and Metallurgy: Melbourne)."

Aug 21, 2012

By R Steinhaus, D M. Frantois-Bongarton, P W. Cleary, G K. Robinson, M D. Sinnott

Multotec Process Equipment and Dominique Frantois-Bongarton have a patent for a mineral sampling device, which they call a æTrue-Belt SamplerÆ. This uses a plough, which is rotated about an axis parallel to a conveyor belt to throw material off the belt. A fixed sample cutter takes a sample from the material thrown off the belt.Discrete element modelling has been used to consider a range of plough designs, plough speeds, positions for the cutter relative to the plough, cutter apertures, cutter designs and frictional properties, prior to the building of a physical prototype. This modelling work will be discussed, both as an illustration of the role of modelling in the development of new materials-handling devices and in order to explain the likely strengths and weaknesses of this new type of sampling device.CITATION:Robinson, G K, Sinnott, M D, Cleary, P W, Steinhaus, R and Frantois-Bongarton, D M, 2012. Modelling of a ætrue-belt samplerÆ - A new device for sampling from a conveyor belt, in Proceedings Sampling 2012 , pp 33-40 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 21, 2012

By M Goers, M Almond

"The use of reverse circulation (RC) drilling for grade control sample collection was selected by the Pueblo Viejo Mine Geology department at the recommencement of the operation in 2010. This method was selected because it allows: for multi-bench drilling (60 m hole depth, four benches of mining) to aid mine planning and provide a detailed close spaced drill data comparison with the reserve model angled drill holes to optimise the drill hole interception of the vertically controlled mineralisation dry sample collection in areas of excessive surface and groundwater mining operations to commence with the long assay return period (due to the need for the samples to be shipped overseas for analysis) until the on-site laboratory is operational.To date, 118 302 m of drilling has been completed throughout the operations of two open pits: Monte Negro and Moore. Two drill rigs (contractor and site-owned and operated) with three generations of sampling systems have been used to date. Throughout the drilling a 20 per cent quality assurance, quality control (QAQC) sample check (blanks, field duplicates and standards) have been used to check the drilling and laboratories performance. In addition, a total of 1104 fines samples were collected to compare the drill chip samples collected and the fines lost with two of the sample systems used.The drilling to date has highlighted the need for a complete and coordinated system to be used before sufficient confidence in the quality of the samples collected is achieved.The complete system must be set-up and coordinated to obtain the best quality sample possible. This complete package includes: drill bit size and shape for the rock being drilled and mineralisation targeted face sampling hammers with the correctly sized hammer shrouds sample hose routing to reduce sample flow turbulence and choking blow-down valves to eliminate drill hole water that has entered the drill string during rod changes correct drilling techniques targeting sample quality a sample system that captures the fines for inclusion into the sample.These improvements can be obtained without reducing the drilling rates.The measurements required to demonstrate the improvement in the sample quality will be the focus of future work within the department.CITATION:Goers, M and Almond, M, 2012. Bit to bag - The importance of a total coordinated system in reverse circulation drilling, in Proceedings Sampling 2012, pp 65-72 (The Australasian Institute of Mining and Metallurgy: Melbourne)."

Aug 21, 2012

By V Rasouli, G Cavanough, A Mokaramian

The sampling time, the costs and its quality are the three factors that determine the best method of drilling in mineral exploration. The two principal methods of reverse circulation (RC) and diamond core drilling are often used in combination by mine operators. RC is used for drilling shallow holes and in-pit grade control, and core drilling for deeper holes to identify future resources. The RC method is faster and more flexible than coring and provides virtually uncontaminated cuttings (ranges from dust to 25 mm chips) to the surface cyclone suitable for geochemical anomalies. The diamond coring produces core samples to increase the level of geological knowledge and the 3D extension and distribution of the orebody. However, both of these methods are subjected to certain limitations and inefficiencies in reaching deeper depths and drilling complex hole geometries. Examples of such shortcomings include the inability to provide enough air pressure for RC drilling and high friction between drill pipe and the hole wall in diamond core drilling.Considering that delivering large volume of reliable samples from deep zones to the surface in shortest possible time is of paramount importance in mineral exploration, and assuming that obtaining core samples over whole overburden is not always essential, then drilling small size holes as fast as possible and delivering the small chip samples to the surface would be a good alternative with several advantages over conventional drilling methods for deep hard rocks mineral exploration. As a result, the use of coiled tube (CT) drilling technology has been proposed recently for such applications. CT is a continuous length of ductile steel or composite tube stored and transported on a large reel; and allows fast drilling by eliminating the connection time and providing continuous circulation during drilling. This enables quick access to the zone of interest to collect the cuttings or obtain core samples. CT is advantageous particularly in drilling directional boreholes and multi-laterals. In this paper, feasibility of using CT delivering reliable samples is discussed for deep mineral exploration. In addition, recent developments and practices are presented that make CT a reliable drilling technology to drill cheaper, faster and deeper and to deliver more continuous and reliable data and samples from deep formations.CITATION:Mokaramian, A, Rasouli, V and Cavanough, G, 2012. Quality sampling using coiled tubing drilling in deep mineral exploration, in Proceedings Sampling 2012 , pp 73-80 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 21, 2012

By D M. Frantois-Bongarton

Variograms can be powerful tools for the analysis and control of process streams and their sampling. Their uses and proper utilisation have been described somewhat unclearly to date, and their limitations and precautions of use are too rarely mentioned. The general meaning and properties of the variogram tool and its use in geostatistics are therefore reviewed in details to derive a critical view of its proper use for process control: what to expect from it and what it cannot deliver and which uses are illusory or potentially misleading. A summary of GyÆs seminal work accompanies this essay to put the concepts into historical perspective.CITATION:Frantois-Bongarton, D M, 2012. Review of variogram properties and remarks on its use in process control, in Proceedings Sampling 2012 , pp 175-180 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 21, 2012