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By Thomas H. Dubaniewicz, Gerald R. Cucci, Gregory M. Green, Kenneth L. Cashdollar

New types of industrial instruments use fiber-coupled law energy to power remote serum. Fiber-optic based instruments are useful in classified (hazardous) locations found in many industrial plants because the fiber provides a natural barrier against accidental electrical discharge into potentially explosive atmospheres. However, current safety standards do not cover the use of laser-powered fiber-optic instruments in potentially explosive environments such as found in coal mines. The U. S. Bureau of Mines began an investigation of laser-powered fiber-optic instruments in explosive atmospheres in support of the standards-making process. A commercial fiber-optic interface system, modified to sin relate several worst-case operating conditions, ignited explosive hydrogen-air mixtures. Worst-am simulations consisted of disabling a safety shutoff feature, operating the laser at significantly higher powers than intended for normal operations, and cleaving fiber-optic connections to direct laser energy onto selected absorptive materials. At the highest power level available, the fiber-optic interface system did not ignite selected methane-air mixtures. The obtained data should prove useful in establishing appropriate safety standards.

By W. P. Yant

A previous report of the Bureau of Mines dealt with the toxicity of dichlorodifluoromethane, a new refrigerant that has a remarkably low toxicity. Continued research by the Frigidaire Corporation and toxicological experiments performed in the Laboratory of Applied Physiology of the University of Cincinnati revealed another organic fluoride, dichlorotetrafluoroethane, whose toxicity also appeared to be of a very low order and whose physical and chemical properties make it suitable for refrigeration purposes. In addition to low toxicity, safety in its use is further enhanced by its physical properties, which permit the design of equipment that operates at comparatively low pressures and hence mitigates the dangers and problems of leakage. The investigation described in this report was performed by the Bureau of Mines at the request and with the cooperation of the Frigidaire Corporation.

Jan 1, 1932

By C. G. Kirkpatrick

Analysis of the data produced by a wide-band, sensitive, horizontal, biaxial motion sensor has revealed several distinctive patterns before, during, and after a roof fall. The signals prior to the roof fall are similar in spectra, but one thousand times larger in amplitude, than those after the roof fall. Immediately preceding the roof fall, by two to twelve hours, five events occurred which were larger in amplitude and lower in frequency than even the large pre-roof fall background signals. An interpretation of these events is offered.

Jan 1, 1979

By James P. Ulery, Stephen J. Kravits, William P. Diamond

This report presents results of a cooperative research project between the U.S. Bureau of Mines and Beth Energy Mines, Inc. Four coreholes (two before mining and two after mining) were drilled at a longwall mine operating in the Lower Kittanning Coalbed to obtain coal and rock samples from overlying strata to determine their gas content at various times in the mining cycle. The results of those tests indicate that 91 pct of the gas removed from the overlying strata came from coalbeds. Material balance calculations were made to compare the volume of gas produced both from gob gas vent holes drilled on the panel and gas removed by the mine's ventilation system with the volume of gas removed from strata directly overlying the panel to a height of 275 ft. This analysis indicates that only 40 pct of the total gas produced from the panel actually came from the strata directly overlying the panel. The remaining volume of gas production probably migrated to the Iongwall gob from overlying, and perhaps underlying, strata immediately adjacent to the panel and perhaps from greater distances downdip because of the establishment of a long-term pressure gradient in the study area.

Jan 1, 1992

By J. D. Corrick

Research was conducted to develop operating techniques and define some of the limiting parameters for microbially converting hydrous calcium sulfate to hydrogen sulfide. The work was carried out in either glass stoppered flasks or anaerobic fermentors. Using the criteria of pH, temperature, number of bacteria per milliliter of test solution, and hydrogen sulfide produced, it was shown that hydrous calcium sulfate could be microbially converted to hydrogen sulfide at a rate of 7.3 g H2S/1 of fermentor volume per 24 hours. The various parameters defined were pH, temperature, and medium exchange rate. These were shown to be a pH range of 7.2 to 8.8, a temperature range of 30° to 35° C, and a medium exchange rate of 70 percent of the ferment or volume per 24 hours. It was also shown that a daily waste was between 50 and 77 percent as effective as sodium lactate in supporting the production of hydrogen sulfide and that by utilizing a gas to purge the fermentation system, a 1.7-fold increase in hydrogen sulfide was obtained.

Jan 1, 1970

Detect hazards associated with abandoned mine openings through the use of integrated geophysical technology. Background Many abandoned mines in the U.S. present hazards to the public. The first step in abatement of these hazards usually requires locating the abandoned workings. Recent Colorado legislation resulted in a concerted effort aimed at mitigating the hazards associated with abandoned mine workings. The Colorado Department of Natural Resources-Mine Land Reclamation Division (CDNRMLRD) is responsible for locating and backfilling abandoned mine openings such as shafts, adits and collapsed features. Many shafts and adits can be located by inspection, other openings give little or no surface expression and must be located by drilling, or through the use of geophysical methods. A common method used for locating underground mine workings is to drill throughout the suspected area. However, it is prohibitively expensive to drill holes at the spacing needed to detect backlilled shafts and small voids associated with caving and/or chimneying. It may also be dangerous to move heavy equipment over shallow mined-out workings. Geophysical investigations that employ only a single method have had mixed success in detecting hazardous abandoned mine land cavities.

Jan 1, 1991

By R D. Fleming

A single-cylinder research engine was operated on pure hydrocarbons and simple (two-component) mixtures of pure hydrocarbons to study the effect of fuel composition on exhaust emissions from a spark-ignition engine. Used as fuels were three pure hydrocarbons that represented the primary hydrocarbon types present in commercial motor fuels: A paraffin (2,2,4-trimethylpentane), an olefin (2,4,4-trimethylpentene-2), and an aromatic (meta-xylene). The engine was operated at the same equivalence ratio for all of the fuels used in the experiment. Exhaust gas samples were collected and quantitatively analyzed for carbon monoxide, carbon dioxide, hydrogen, nitrogen oxides, aldehydes, and hydrocarbons. Exhaust hydrocarbons were separated and quantitatively measured with a chromatographic system employing a flame-ionization detector. Unknown hydrocarbons and oxygenated materials in the exhaust were identified with a Time-of-Flight mass spectrometer coupled to a chromatographic system. The results of the exhaust gas analyses showed that ethylbenzene, l-methyl-3-ethylbenzene, and l-methyl-3-vinylbenzene were more abundant in the exhausts from either 2,2,4-trimethylpentane--m-xylene or 2,4,4-trimethylpentene-2--m-xylene fuel mixtures than in exhaust produced from m-xylene. Also, the pure 2,4,4-trimethylpentene-2 fuel produced smaller amounts of C2 to C7 olefins in the exhaust than that produced by the pure 2,2,4-trimethylpentane fuel. The exhaust from pure m-xylene fuel contained aromatic hydrocarbons of higher molecular weight than the parent fuel. The amount of total hydrocarbon (moles of exhaust hydrocarbon per mole of fuel used) in the exhaust from the three pure fuels decreased in the following order: 2,2,4-trimethylpentane > 2,4,4-trimethylpentene-2 > m-xylene. The hydrocarbon mole-fractions of unreacted fuel in the exhausts produced from each of the pure fuels were 0.20 for 2,2,4-trimethylpentane, 0.13 for 2,4,4-trimethylpentene-2, and 0.66 for m-xylene.

Jan 1, 1970

By M. Beus, R. Iverson, A. Dreschler, V. Scott

This paper describes research to improve safety during transport of ore and waste in underground mines. Field tests are underway in mines in Idaho and Montana. Strains measured on structural support members in an ore pass provided information about total forces acting on the structure as material was dumped into it. Results show that measured static loads were considerably less than actual total weight of the material dumped and that dynamic loads were subject to many factors, such as effects of blasting to remove hang-ups. Comparisons of measurements and computer results using a particle flow code indicated that several difficulties remain before achieving realistic determinations and models of the dynamic effects of particle flow in ort: passes and impact loads on the gates. Impact loads were overestimated in computer analyses as compared to loads measured in field tests. An alternative design approach based on softening the chute and control gate assembly is being proposed.

By C. M. K. Boldt, R. L. Levens, A. D. Marcy

Researchers at the U. S. Bureau of Mines conducted investigations to evaluate the potential for ground water contamination by mine waste used as backfill. Samples of cemented waste backfill and water discharging from drillholes and seeps were collected to use in chemical analyses and laboratory tests to determine the physical and chemical factors that control release of heavy metals to ground water. Greater water retention by cemented backfill (as compared to uncemented sandfill) reduces the surface are aexposed to oxidation, which in turn reduces the amount of acid produced. The acid is neutralized by the cement and minerals contained in the backfill. The grain-size distribution of tailings used for backfill affects the structural integrity of cemented backfill under attack by acidic water; breakdown of the backfill structure releases neutralizing materials faster. Backfilled stopes in rock with low hydraulic conductivities will constitute preferential flow paths after mine flooding; however, the rate of flow through backfill will be much slower than when the stope is partially saturated during mine operation. Considering all factors, acid generation and release of metal ions from cemented backfill should be less than in uncemented sandfill.

Jan 1, 1995

Control the release of ground-water into active underground coal workings by short-term pumping from dewatering wells sited on fractures. Approach The sudden release of fracture-stored groundwater into underground coal workings often occurs when mine workings are developed beneath fracture valleys, Pumping from fracture trace-sited dewatering wells, prior to development of the underlying workings, can be an efficient means of intercepting fracture-stored groundwater before it is released into the mine. Dewatering operations are discontinued once the underlying mine workings have been fully developed, and the maximum possible reduction in fracture storage has been achieved through pumping. How It Works An aerial photographic technique known as fracture trace analysis is used to site dewatering wells on rock fractures in a valley bottom. Downhole caliper and temperature logs are used to assess the fracture flow potential of each dewatering well drilled.

Jan 1, 1987

By F. J. Gallagher

The purpose of this circular is to present information on the construction and use of reinforced rubber-jacketed tubing and insulating air-line couplings in coal mines where Airdox is used for breaking coal in order to eliminate, insofar as possible, arcing at the face between Airdox tubing and the track or other face equipment.

Sep 1, 1949

By John Gross

The Alaska Station of the Bureau of Mines has recently conducted tests on two tailings from black sand which had been treated previously at the Station. The results of this previous treatment have be on given in a paper entitled "Recovery of Gold from Black Sand by Classifier Concentration." The gold in these tailings was intimately united with quartz, and was so finely divided that it could not be detected with the naked eye, nor even by P&nn ing unless the material was ground. Its fineness is further shown by the assºy result, which reported only lz per cent of the gold content as "metallics", Wºorea's the assay of the original sand reported 36 per cent of the gold as "metallics." The fact that the gold was in such fine particles, closely united with quartz, precluded further recovery by amalgamation without grinding. On the other hand, the small content present, as well as the lack of grinding appliances at the placer mines of Alasia, made it necessary that the material be cheaply handled if at all. With these facts in mind the experiments described below were undertake.n.

Oct 1, 1920

By Frank Ruskey

This report describes a computer program devised by the Bureau of Mines to model coal-mining situations where one or more panels encounter oil or gas wells. The program seeks in several hundred trials to evade the wells if possible or to minimize their influence by shifting or skewing the mine plan and/or adjusting the centerline dimensions of the entryways. Upon completion of computations, the program sorts the hundreds of models which have been tested, and lists the 10 best with their associated parameters. It also draws a mine plan of the best configuration, showing the entryways and crosscuts along with the "lost" coal remaining in the barrier pillars surrounding the various wells.

Jan 1, 1972

By J. B. Gayle

A 1/2-ton experimental coke oven was installed ac the Bureau of Mines Southern Experiment Station, Tuscaloosa, Ala., in 1948. Designated as the Tuscaloosa oven, this unit features a 17-inch carbonizing chamber, globar heating elements, and silica-brick walls designed to simulate as closely as possible the carbonizing conditions for commercial slot-type ovens. Because of the small force exerted on the oven walls in most tests conducted to date (probably owing to the practice of charging coals and blends at a moisture content approximating that normal to commercial plants operating in this district), little information has been obtained about expansion properties. Two sole-heated ovens have therefore been constructed and used as supplementary equipment for determining the expansion properties of coals tested in the Tuscaloosa oven. The reasons for constructing the Tuscaloosa oven, the details of design, the operating, characteristics of the oven and the reproducibility of results have been discussed in previous publications. 3 4 5/ The present report deals with the effects of substituting various high- and low-volatile coals for components of a selected base blend carbonized under conditions similar to those normally used for producing foundry coke. Results of tests of 11 coals and 14 blends indicate that several blends tested rave cokes having physical properties very similar to those produced from the reference blend.

Jan 1, 1957

By J. B. Zadra, S. M. Shelton, M. M. Fine

"Ferrograde manganese ore or its equivalent is essential to the manufacture of every ton of steel produced; although it is well known that there are large deposits of low-grade ore in the United States, the production of substantial amounts of ferrograde material from domestic sources presents a problem that becomes more and more critical as the stockpiled ore is depleted through inability to procure adequate supplies from foreign sources. Consequently, a program of laboratory and pilot-plant investigation designed to solve the problem of obtaining a domestic supply of manganese has been undertaken by the Metallurgical Division, Bureau of Mines.This paper is one of a new series that will include reports of results obtained in the various investigations conducted under the manganese program. The scope of the program and the organization that woo set up to direct and supervise the work were discussed in the foreword of the first paper of this series, Report of Investigations 3606, Manganese Investigations. 1. Concentration of Manganese Ores from the Drum Mountain District, Utah, by S. R. Zimmerley, J. D. Vincent, and C. R. Schack. Other reports will be published as the work progresses."

Mar 1, 1942

By L. J. Prosser, G. Esterhuizen, A. T. Iannacchione

The potential for roof fails in underground mines remains a clear and present danger for mine workers An investigation of ground conditions in nearly 50 percent of the nation’s underground stone mines fold that the slate of roof stability is primarily determined in a limited and subjective manner. These large-opening mines with roof heights typically 7 m (23 ft) or more, make physical observation difficult. Although some mines use monitoring techniques to gain additional information an roof stability, this practice is usually short term and localized to address ground conditions in a particular section or part of the mine. A roof-fall hazard-assessment techniques was development based on engineering judgment acquired from extensive underground stone mine experience and on exanimation of the related literature. This technique utilizes observational processes to determine roof fall likelihood Case-study scenarios offer a realistic picture of model implementation. Providing the mine level decision-maker with an accurate assessment tool to ascertain the level of ground fall hazards is expected to reduce mint worker injuries and fatalities Moreover; the presences of danger can be overcome with a clear picture of quantified ground conditions.

By V. A. Nieberlein

An extractive process was developed applicable to submarginal titanium deposits containing valuable minor constituents; such as columbium (niobium) and iron. The process consisted of reducing the mineral concentrate with coke at high temperature to form a carbide-suboxide sinter, chlorination in the 400° -500° C. range, and fractional condensation of the chlorides. The chlorination procedure recovered 97, 83, and 87 percent of the titanium from brookite, rutile, and ilmenite sinters, respectively, while simultaneous columbium recoveries on the same materials were 85, 50, and 87 percent.

Jan 1, 1957

Provide longwall operators with practical information and guidelines concerning mine design to reduce problems associated with the interaction of adjacent workings in multiple-scam longwall mines. Background The high productivity achieved by longwall mining demonstrates its potential to provide a substantial segment of underground coal production. Longwall mines produce more than 30 pct of underground coal, up from pct just 15 years ago. However, the continued growth of this mining method without appropriate multiple-seam planning may increase the cost and risk of mining. Research by the U.S. Bureau of Mines (USBM) indicates that 25 longwall mines (32 pct of the total number in the United States) have mining in adjacent coalbeds either above or below. About half of these longwall mines report some type of interaction problem with the adjacent workings, such as caving due to subsidence. Optimization of mine design factors is the best means for controlling interactions between operations in adjacent scams. To avoid higher mining costs, operators should focus on adopting practices and procedures that prevent and control interactions in multiple scams. The USBM, in an effort to improve longwall mine planning, has been investigating multiple-seam longwall design and development.

Jan 1, 1994

By John C. Edwards, Gerald S. Morrow

The U.S. Bureau of Mines has constructed a smoke chamber and developed sensitivity tests for smoke detectors. Response of ionization- and optical-type commercially available smoke detectors have been investigated. Six smoke detectors were measured with respect to visually obscuring smoke characterized by a corresponding optical density for smoldering and flaming coal combustion in the smoke chamber. It was determined that for one type of ionization smoke detector the alarm time was nearly equivalent to that of an odor monitor's alarm for smoldering coal combustion experiments and earlier for flaming coal combustion experiments. The experiments showed that an average CO concentration of 5 ppm corresponded to an optical density of 0.022 m for smoldering and flaming-1coal combustion. Two of the commercially available ionization-type smoke detectors were more responsive to flaming than smoldering coal combustion at an optical density of 0.022 m, whereas the optical smoke detectors-1showed the opposite trend. The responsive characteristics of the detectors evaluated with respect to known smoke conditions in the smoke chamber shows their potential for use as mine fire sensors or part of a mine atmospheric monitoring system to improve mine safety.

Jan 1, 1995

By J. C. Edwards

To have the capability to predict the development of localized spontaneous heating within a porous coalbed that is subjected to forced air ventilation or in an otherwise quiescent environment in which buoyancy develops, the Bureau of Mines developed three time-dependent mathematical models, which were used to calculate the temperature increase associated with chemisorption of oxygen by the coal. In each model, spontaneous heating is driven by an Arrhenius first-order reaction between the oxygen and coal. Two models are two-dimensional, and one is one-dimensional. In the first two-dimensional model, a constant-velocity forced convection airflow is specified; and in the other, buoyant flow is allowed to develop in the absence of forced convection. The third model evaluates the airflow from Darcy's law and a specification of the pressure at the surface of a one-dimensional porous coalbed. Numerical computations demonstrated how each model could be used to predict the onset of spontaneous heating when the porous coalbed was subjected to constraints of an imposed internal heat source or a high temperature airflow. The effects of particle size and coalbed compaction upon spontaneous heating were examined with the third model.

Jan 1, 1990