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A study was made of zircon powders bonded with phosphoric acid or aluminium orthophosphate. The influence of strength of solution of the phosphatic binders on the modulus of rupture over a temperature range was investigated. Physical properties of three grades of zircon powder bonded with phosphatic binders were studied at various temperatures. Examination of x-ray diffraction data indicated that phosphates ofzirconia are preferentially formed to phosphates of silica. However, zircon in the presence of excess phosphoric acid also forms phosphates of silica upon heating.Resistance to attack by slags from blast and open hearth furnaces was determined on phosphate-bonded zircon mortars in a cup test with industrially made ladle bricks. Zircon powders bonded with phosphates proved to have high P.C.E. values. The first satisfactory results of a plant trial with phosphate-bonded zircon mortar, used in a steel ladle, are now being assessed in larger scale industrial tests prior to accepting the mortar as a steel plant refractory.

Jan 1, 1972

The Auscoke project has reached-a stage where a pilot plant nominally able to produce 100 t.p.d. of coked briquettes is being brought on stream during Nov. 1971 . The targets for this stage of the project are to establish the technological and economic value of Auscoke for the iron blast furnace, and to verify the commercial feasibility of large scale plants. The project originated at the B.H.P. Central Research Laboratories (C.R.L.) and work to date has shown that using a two stage contin- uous process, strong large coke can be produced at good productivities from medium or low volatile poorly caking coals. General features of the pilot plant and processing are discussed.

Jan 1, 1972

The facilities used and techniques employed in the manufacture of steel and iron rolls at the Steel Foundry, B.H.P., Iron & Steel Works, Newcastle are described.

Jan 1, 1972

By Still RF

Sintering of lead and zinc concentrates is practised by Sulphide Corporation Pty. Limited to provide both desuiphurised lump sinter feed, for simultaneous reduction to zinc and lead in the Imperial Smelting Process blast furnace, and sulphur dioxide gas for sulphuric acid manufacture. From November, 1969 a 20 percent increase in production rate has been obtained through improvements in operating technique. A gradual increase in bed permeability was achieved by modifications to the feed mix conditioning equipment and by improving moisture control. However advantage could not be taken of the higher permeability to increase sulphur elimination because the hardness of the lump sinter decreased. Higher throughput, better quality sinter and more stable sintering conditions were however made possible by simultaneously: 1. reducing segregation and compaction in the sinter bed, by narrowing the discharge opening of the main layer feed hopper, 2. reducing the sizing of sinter returns to give a closer size spectrum of particles in the feed mix, and 3. increasing the sulphide sulphur content of the feed mix to give higher bed Temperatures.

Jan 1, 1972

Laboratory high tension roll separation and the commercial machines available for this purpose are discussed. The shortcomings of these machines are indicated and a machine that overcomes some of these undesirable character- istics is described. A procedure for evaluating laboratory high tension roll separation is described. The use of this evaluation procedure in conjunction with the laboratory separation is described with examples taken from the Dunwich and Hexham processing plants of Associated Minerals Consolidated Limited. Evidence that laboratory testwork results may be directly transposed to operating plants is given. A discussion of the effects of variables in high tension roll separation of mineral sand concentrates concludes the paper, and uses in support results obtained in the metallurgical laboratories of Associated Minerals Consolidated Limited, Southport, Queensland.

Jan 1, 1972

Subsurface information from the "Upper Coal Measures" of the Sydney Basin is interpreted by means of structure contour maps, isopach maps and geological cross- sections. Particular reference is made to recent coal drilling operations by the New South Wales Department of Mines. The study is restricted to the onshore portion of the Sydney Basin.

Jan 1, 1972

By Duncan B

Shortwall continuous mining as first introduced at Burwood colliery, and currently being used at John Darling, Lambton, and Corrimal collieries, is a method of coal winning which was pioneered in the Newcastle district. The system uses individual hydraulic self-advancing chocks for roof support and the coal winning operation is by continuous miners and shuttle cars. Where physical conditions are suitable the system provides a safe, efficient and economically viable basis for pillar extraction. Shortwall operations have been conducted successfully in the Victoria and Dudley seam, near the coastal fringe of the Newcastle district and are now being tried out in the more difficult conditions of the Bulli seam in the Illawarra district.

Jan 1, 1972

The history of the down draught Dwight- Lloyd system of iron ore sintering in Australia is developed. Characterisation of the broad process is given for one plant, and regional divergences from the reference practice are noted and briefly analysed. The subject of the development of high basicity sinters is introduced, and regional differences in approach and results are Examined.

Jan 1, 1972

By Ritchie AS

The principles of chromatographic and electrophoretic separations are described in simple non-mathematical language. Brief details of the analytical procedures and of equipment are given. Partial analyses of rare earth elements in monazites from four localit- ies in New South Wales are compared with analyses from other localities. The presence of uranium in two of the monazites is recorded. The occurrence of rare earths in nature is outlined and its geological significance is indicated, A low capital cost method of analysis of rare earths in monazites is Introduced.

Jan 1, 1972

A brief review of currently available "commercial" information on methods of treating ilmenite s to produce high titanium content "upgrades" is made. In this back- ground the CSIRO/Murphyores Process is described and its relationship to other methods Discussed.

Jan 1, 1972

Exploration for economic nickel sulphide mineralisation has often been directed by rationalisations based on poorly understood genetic models. Among those that have enjoyed popularity over the past decade are the "layered gabbro" model and the "basal ultramafic" or Kambalda model. The new discoveries in the Mt Keith-Agnew area could well become a model for future nickel search. Exploration based on even the crudest state- ment of the Kambalda model - prospect the basal contact of Archaean ultramafic complexes for gossanous expressions of sulphide mineralisa- tion - has met with remarkable success. Refine- ments to this model, besides satisfying the geology of any particular deposit, have the major virtue that many of the genetic options - magmatic segregation, hydrothermal transport, sulphurisation, replacement sedimentary, structural control, etc. - are still open. Recent descriptions of highly magnesian silicate melts associated with the ultramafic rocks, do however, place some constraints on the formation of these deposits. Further evidence, from experimental studies on sulphide-silicate and sulphide-oxide phase relationships, and nickel-iron exchange in pyrrhotite, is taken with descriptions of sulphide nickel occurrences in Western Australia to examine genetic models for existing ore bodies.

Jan 1, 1972

A continuous casting machine, of the Concast curved mould design casting billets in four strands, was commissioned at the Newcastle Works of The Broken Hill Proprietary Co. Ltd., in November, 1967. Quality assessment of early casts from this plant indicated that steel cleanliness was sometimes inferior to that of equival- ent ingot cast steel. Extensive trials to develop a modified deoxidation technique were not successful in improving clean- liness to the desired level. A "contra-flow" gas shroud, to cover the steel stream between the tundish and the mould, was developed, and proved successful in achieving the required levels of product cleanliness. The inclusion content of six grades of steel ranging in carbon content from 0.10 to 0.70 per cent is examined, and an attempt is made to explain theoretically some of the results obtained.

Jan 1, 1972

The published liquidus data on the Pb-PbS system have been correlated on the basis of one-coefficient Margules equations. Thermodynamic properties of the components of this system have been obtained, and it has also been found that the calculated miscibility gap of this system exists over a very narrow range of temperature (1041 to 1058°C).

Jan 1, 1972

Drilling has disclosed a sequence of Cainozoic sediments immediately to the west of the Ediacara mineral field containing little or no dolomitic debris in the lower and middle sections, but with gravel beds of dolomite derived from local rocks in the upper part. It is suggested that the lower and middle sequence of Cainozoic strata was deposited over the area of the Ediacara Range, and that this range was uplifted, probably as a horst block, during Quaternary times and was first exposed to subaerial erosion during the upper Pleistocene epoch.Lower Cambrian dolomites with associated stratiform lead mineralization, which formed the target of drilling on the western downthrown block of the Ediacara Fault, were eroded before deposition of Cainozoic sediments.Intense leaching of basal Cambrian dolomites around the periphery of the Ediacara Basin took place during Mesozoic and Tertiary times. This leaching process has resulted in enrichment of copper and lead mineralization in a thick marginal zone of residual clayey material overlain by dolomitic collapse breccia. These zones of leaching and enrichment were preserved under Cainozoic sediments which have subsequently been eroded. The Ediacara Fault appears to have been a major conduit for mineralizing fluids and is the main lineament of the Torrens Hinge Zone. Contemporaneous movements on this fault have controlled rates of depositionand thickness of sediments across the fault during Adelaidean and Cainozoic times. Though latest movements of this fault have been west block down, the predominant movement has been east block down with associated thickening of sediments to the east in the Adelaide Geosync1ine.

Jan 1, 1972

A detailed study of the capital investment and production cost for copper electrowinning plants shows that significant savings in both can be achieved by increasing the current density. From the economic analysis it is determined that the optimum current density which will result in lowest capital investment and lowest operating cost is between 60 A/sq. ft. and 70 A/sq. ft., or at least three times as high as the Conventionally employed current density. The specific investment, expressed as $/ton-year, is found to be a function of both the current density and plant capacity and has a minimum value at the optimum current density. Empirical equations are developed for the purpose of estimating the capital investment and operating cost for plants of any production capacity operating at any current density.

Jan 1, 1972

The use of black and white and colour infrared film in remote sensing of natural resources is reviewed. In heavlly-forested areas such as New Zealand, the main value of the method is in surveying the vegetation cover to detect the existence of plant communities characteristic of specific geological formations. By contrast in arid areas of Australia where the vegetation cover is sparse and where rocks and soils are well exposed, the method can be used in detecting different rock types or other geological differences.

Jan 1, 1972

The flotation circuit handling Peko ore at Peko Mines N.L. was examined in July 1970 with a view to determining simple changes in circuitry or reagents which could improve the grade and recovery of the final copper concentrates. The investigation included sampling over one shift followed by detailed testing of the samples by sizing-assays, sizing-mineralogy and sizing-liberation. Mass balances were carried out over total streams, the component minerals and the copper contents. Some laboratory work was carried out to assess the effect of salinity on flotation. In order to handle the sizing-mineralogy calculations a computer programme was set up. The raw data were corrected for locking factors, then mineral and elemental distributions cal- culated for each screen fraction and the total sample. Calculated assays from grain counting were compared with chemical assays. Recoveries through the size-ranges re- vealed very rapid flotation of copper minerals at sizes below 350 mesh. This pointed to a possible circuit improvement by desliming rougher tailings ahead of the scavenger stage. A strong correlation was found between water in concentrates and gangue recovery for the subsieve sizes. This pointed to clean water additions to the cleaner circuit as a way to 1 Project Consultant, The Australian Mineral Development Laboratories, Adelaide, South Australia.

Jan 1, 1972

The uptake of nickel into the lattice of pyrrhotite, Fe1 _1J S was studied experimentally in the temperature range 200°C to 760°C. Nickel from both aqueous solutions and salt melts diffuses rapidly into the sulphidelattice with an accompanying release of iron into the solution or melt. The rate of uptake of nickel and its diffusion into the sulphide lattice were followed by optical microscopy and by analysis with an electron probe microanalyser. Some geological consequences of this phenomenon affecting the distribution of nickel in rocks associated with nickel-iron sulphide ores are discussed.

Jan 1, 1972

By Coppock BW

Sintering of lead and zinc concentrates is practised by Sulphide Corporation Pty. Limited to provide both desuiphurised lump sinter feed, for simultaneous reduction to zinc and lead in the Imperial Smelting Process blast furnace, and sulphur dioxide gas for sulphuric acid manufacture. From November, 1969 a 20 percent increase in production rate has been obtained through improvements in operating technique. A gradual increase in bed permeability was achieved by modifications to the feed mix conditioning equipment and by improving moisture control. However advantage could not be taken of the higher permeability to increase sulphur elimination because the hardness of the lump sinter decreased. Higher throughput, better quality sinter and more stable sintering conditions were however made possible by simultaneously: 1. reducing segregation and compaction in the sinter bed, by narrowing the discharge opening of the main layer feed hopper, 2. reducing the sizing of sinter returns to give a closer size spectrum of particles in the feed mix, and 3. increasing the sulphide sulphur content of the feed mix to give higher bed Temperatures.

Jan 1, 1972

By Williams RC

Overlying the coal deposits of the Sydney Basin are several lakes and other bodies of water. These include the Pacific Ocean, Lake Macquarie, the Tuggerah Lakes and the stored waters of the dams of the New South Wales Metropolitan Water Sewerage and Drainage Board. The coal beneath these bodies of water amounts to hundreds of millions of tons. Colliery workings have approached these areas of water and in some instances first 1"orkings of bord and pillar have taken place oi_eshh the water. he problem which now faces mine manage- and other interested authorities involves the determination of the maximum ;mount of coal which can be safely extracted from beneath the water. There are many factors to be considered including the depth of cover, seam thickness, geological details and strata movements.

Jan 1, 1972