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By B. J. CROSS., Henry Kreisinger, John Blizard, C. E. Augustine

This bulletin presents the results of 36 tests made on a 468-horsepower Edge Moor boiler fired with pulverized coal at the Oneida Street Station of the Milwaukee Electric Railway & Light Co., Milwaukee, Wis. The tests were made by the fuel section of the United States Bureau of Mines in cooperation with the research department of the Combustion Engineering Corporation. Illinois coal was used as fuel; the furnace, burners, and feeders were designed by the Locomotive Pulverized Fuel Co. The object of the tests was to determine what over-all boiler efficiency could he obtained with pulverized coal under various conditions of furnace operation and with coal of different fineness and moisture content. The investigation was thorough. The pulverized coal, as it was supplied to the furnace, was weighed in specially designed tanks placed on platform scales. Twenty-nine of the tests were of 24 hours duration, three of 16 to 18 hours, and four of 12 hours. All tests are reported excepting two-8 and 20-which had to be stopped abruptly, No.8 because a motor actuating the coal-feed screw burned out and No. 20 because of trouble with the feed pump. Tests 1 to 27, inclusive, were made with round burners and tests 28 to 3Rwith spreading burners. In the first nine tests a large excess of air was supplied in an effort to prevent the ash fusing at the bottom of the furnace. In tests 10 to 16 the supply of excess air was reduced in order to get a high efficiency, regardless of the slagging of ash at the furnace bottom. Tests 17 to 27 were made with a water screen about 10 inches above the bottom of the furnace, to make possible the burning of coal with a small supply of excess air without the ash fusing at the bottom of the furnace. Tests 28,29, and 30 were made without the water screen and with a small supply of excess air, and tests 31 to 38 with a water screen around the walls near the bottom of the furnace. Tests 32, 33, 34, and 35 were run with coarser coal than that used ordinarily at the plant. Tests 36,37, and 38 were made with undried coal.

Jan 1, 1923

By William W. Adams

Reports for the calendar year 1923 that have been transmitted to the Bureau of Mines of the Department of the Interior by mine officials of the various coal-producing States show that accidents in and around the coal mines resulted in the death of 2,452 men. The output of coal during the year, as reported to the United States Geo- logical Survey, was 641,476,000 tons; hence the fatality rate per million tons was 3.82 as compared with 4.15 for 1922, a decline of about 8 per cent. The average rate for the decade ending with 1922 was 4.11. This reduction of 8 per cent in the fatal-accident rate per million tons is equivalent to the saving of 210 lives--that is, had the fatality rate of 1922 continued through 1923 the number of lives lost would have been 210 more than they actually were. Not only was there a net reduction in the fatality rate from all causes combined, but each of the main causes of coal-mine fatalities also showed a decline. Falls of roof and coal, which generally account for nearly half of all deaths in coal mines, were responsible for 1,158 fatalities in 1923, which represents a rate of 1.81 per million tons as compared with 1.90 in 1922. (See Table 2.) Haulage accidents underground usually cause about 17 per cent of all fatalities, and the reports for 1923 show that 413 deaths were due to this cause, indi- cating a rate of 0.64 per million tons, as against 0.71 for the previous year. Gas and dust explosions killed 372 men, the fatality rate being 0.58; the rate for 1922 was 0.65. Seventy-five deaths were due to electricity, for which class of accidents the fatality rate per million tons was 0.12 as compared with 0.16 the year before. Powder and other explosives caused 114 deaths, representing a rate of 0.18 as compared with 0.19 for 1922. Of the 2,452 fatal accidents during the year, 2,249 occurred under- ground, 46 in shafts, and 157 on the surface. At bituminous coal mines the number of deaths was 1,943, of which 1,816 were under- ground, 31 in shafts, and 96 on the surface. At the anthracite mines

Jan 1, 1923

By E. D. Gordner

Irrespira ble gutses issuing from the rock fofflb tions ere tJ source of expense ond danger in some metGLl mines. There is a great Variation in the compos i-· tion of such gdses and, os shown 'by recent sampling by the Bureau of ines, the gas rr;;,.y consi$t mostly ct carbon dioxide, (Rocle Strata Gtsses in the Mines of the East Tintic Mining District, by G. E. McElroy, Bu.retau of Mines Serial 2Z75) or f methone (Metruine in Ccalifornia C.old Mines, by B. 0. Picl-Q:lrd i:lnd !.. D. ("iordner, Bure, cf Mines Serial 2303), or nitrogen, sin the present instonce. A nl.liilber of unventilated rt:t.ises in some of the mine of l:l Neva&. district conuin «i'ccumulCltions of l;i hih-nitrogen gas the1t will not supi:ort life or combus­tion. The rdises ore in different geologiecil formations and in widely sep1:1rated. loecslities in the mining district. One ot" two ri::lises in the sme fc.rtr.ation may be full of the gos cand einother nec-r'by be t'ree ot· it. Lives have been lost t:lnd a number of men heave been overcome on enteing unvetilated rtsises in which their­respircable tss hcsd c1ccuni..1.l1::1ted between sldfts. Gener1:1lly, however, the gas see:ns to noozett from the .t'onrbtio:1 ond to ecc1: .. ,i.-1,;.1:.1te so slowly tMt its presence is not suspected t the tfr.1e, bu.t discovered. ed:'t&.c' the raise is t)band.oned. OcCE.isionelly 1 t issues from a ne•.,ly cut cre·tice or fissure under considerca ble pressure and in lar!?e enough '3.'16ntities to overcome or drive 011t men working in unventilated places.

Dec 1, 1922

By J. D. Davis

"Introduction.Sixty years ago, M. Berthelot found that ethylene could be selectively absorbed from gaseous mixtures by concentrated sulphuric acid, and that the compound formed by the chemical union of the gas and acid was readily decomposed by heating with water, yielding ethyl alcohol. Only within the last few years has there been any attempt to make use of this discovery technically.Bury*, working in England at the Skinningrove Iron Works and on a commercial scale, developed a technical method for converting, the ethylene of coke-oven as into alcohol. With a gas containing less than 3 per cent of ethylene, he obtained a yield of 1.6 gallons of alcohol per ton of coal carbonized.De Loisy** perfected a technical method for treatment of coke-oven as for alcohol. Evidently this work was carried out on a semi-commercial scale. His method is based on the use of catalytic agents for hastening the absorption of ethylene by sulphuric acid. He uses part of the spent acid for drying the gases and pact for the manufacture of ammonium sulphate. Excess acid is reconcentrated by waste heat. Others have worked on the problem, but so far there has been no large recovery of ethylene from coke-oven gases. The chief difficulty seems to lie in the low efficiency (about 50% of methods and tae relatively low concentrations of ethylene in the gases treated. Gas from Trent amalgam*** contains much larger percantages of ethylene than does coke-oven gas, as Will presently be shown, and if it should ever prove practIcal to treat industrial ;as for alcohol, this gas would offer attractive possibilities,* Bury, Ernest, Ethylene as Alcohol from Coke-Oven Gas: Gas Journal' Vol. 148, D. 30, 1919, pp. 718.** DC Loisy, M.E., Sur un procede' industrial de fabrication syntlotique de l'alcool et de l'ether a partir des gaz de distillation de la houil Comp Rend, vol. 170, Jan. 1920, p. 50-3.*** A paste consisting of approximately part oil such as that obtained as for cleaning coal. See Perrott. in cleaning coal, Chem 3 parts finely pulvarized coal and 1 final product in the Trent, process StJ, and Kinney, S.P. The use of oil Vol. 35 August 3, 1921, p, 183.. & Met."

Nov 1, 1922

By H. B. Freaman, C. L. Colburn, C. M. Bouton

"The mine telephone has been perfected to such an extent that it is giving satisfaction in most mines were the wiring is well insulated. Very often the telephone cannot be depended upon on account of falls of rock, grounding due to worn insulation or extreme dampness. In the event of a disaster it frequently happens that the mine telephone system is put out of commission by the agency that causes the disaster, at the time when it is most urgently needed. On this account the mining industry is interested in any kind of telephone system that can be counted upon in an emergency. Many requests have been received by the Bureau of Mines to devise means of utilizing wireless methods for this purpose.The results of some preliminary experiments conducted by the writers at the Bureau of Mines experimental mine at Bruceton, Pennsylvania, in the ordinary sending and receiving of radio waves through earth strata are described below. The experiments were made in cooperation with the Westinghouse Electric end Manufacturing Co., which assigned to this work three of its radio engineers, C. A, Boddie, E. C. Douglas, and F. D. Fessler,The preliminary experiments consisted first in receiving signals from without the mine by means of a receiver located inside the mina, and second, both sending and receiving messages underground through the strata. It was found that with a receiving instrument set at a point 100 feet underground, signals from KDKA station, of the Westinghouse Electric and Manufacturing Co. East Pittsburgh, Pa., could be heard distinctly. Station KDKA is at a distance of about 18 miles from the experimental mine. About 50 feet from the receiving station used in this test was a 6-inch bore-hole from the surface, lined with iron pipe and containing electric light wires which extended therefrom through-out the mine. The presence of these wires evidently assisted greatly in the reception, for when the receiving set was carried to another point in the mine removed from wires and tracks the signals were barely audible through 50 feet of cover. The fact that signals were detected, however, even though faintly, is sufficient evidence of transmission through the ground to encourage further experimenting.In sending waves underground the Westinghouse 20-watt B.T. model T.F. transmitter was used in such a manner as to send out continuous waves of 200 to 300 meters length."

Oct 1, 1922

By L. C. IlsLey

Minin,g Qr col-cu.ttint till:I chines are 1?;\i9ng the _m9t wideiy .used de1sses ()f mining equipment.· These 1T:.i:1Chines ,.--re practicaily t-tl\·operc1_ted eiyher_by compressed .iir or by electric. ·motors. According to &.ta• compiled _ from the 122. issue COAL CATALOG\JE. OJMEINED WITH; OOAL "FIELD 'pf!:fC'TOTl1, bf 7,088. mnes from which reports were obttiined there -are 3895 mines that u.se coal-cutting eql;lipmen:ts,, 'f'hi report lists 20,031: r.ct:lchines, 17,&75 being operated by·elct:i.c.m<;>_tors··:r;id :the remtiinder by compressed i.r motors,· ,-. · ', .. . · .. ··, .. _ ,· .,, .. .. . . . . . : ; "'l t:: On tl.Ccou-nt .. of the wide· use of coc:11-cutting -.:i"cliine_- any Stat!;ls have issued regulationa as "to their operation dnd be to safety precautions that.should be observed J especially in gaseous mines.

Oct 1, 1922

By Robert J. Anderso

Few elements have received more attention and developed greater interest in the last ten years than titanium. The substantially pure metal has been din...ie. cult to isolate, and so far has been little employed oommercially, but the use af alloys and chemical compounds of titanium has increased markedly in recent years. The earlier attempts at preparing pure titanium resulted in various impure forme which, from their metallic appearance, were always mistaken for the metal. Hunter in 1910 isolated pure titanium by the reduction of titanium tetrachloride with sodium. This brief statement is issued by the Bureau of Mines in response to numerous inquiries which have been received concerning titanium. More complete in. formation on the metal may be had by consulting the referenpes appended. The Literature is voluminous and only the more important references are Riven. It has been drawn upon freely in preparing this report; also information was supplied by M. g. Hunter, Arthur Braid, M 1. Schmid, C. M. Johnson, N. B. Hoffman, and de Courny Browne. The pioneer investigator in titanium is A. IL Rossi.

Oct 1, 1922

By Rudolf Kudlich

"During the coming winter, it is probable that many householders who have habitually been users of anthracite coal will be obliged to turn to some other fuel for heating purposes, because of the limited supply of anthracite. The next best fuel, from a standpoint of cleanliness and ease of operation, is coke, but here again the supply is inadequate and the householder will have to fall back on bituminous coal. Though bituminous coal has the dis¬advantage of being dirty to handle, requiring more care in firing, and of giving off considerable smoke, it will be more generally available, costs less, and in the better grades which will naturally find their way to the domestic market, is higher in heat value, and contains less ash than anthracite.Choice of CoalThere a variety of bituminous coals are available, the householder should choose a low volatile coal, such as New River, Pocahontas, or some other ""smokeless"" coal, or the British coal now being offered in the markets along the Atlantic seaboard. Though not necessary to have the coal sized, as is the case with anthracite, it will be found cleaner to use coal from which the fine dirt has been screened. If it is found that excessive dust is caused when firing the coal, this can be reduced by slightly wetting the coal at the front of the bin, as it is being used.Method of Firingusing bituminous coal instead of anthracite in the domestic furnace, it will be necessary to use an entirely different method of fir Instead of leveling the fuel bed and putting on fresh coal in an even layer over the entire fire box, the coked and partly burned coal remaining from the previous firing should be pushed as much as possible to one side of the box, and the fresh coal thrown into the empty side so as to leave some burning coal exposed. In this way the green coal is heated slowly, the volatile gases are given off gradually, and are ignited by the burninggoing to waste up the chimney unburned."

Oct 1, 1922

By L. C. IlsLey

A n'Ulllber or operators have installed f'lBJ!le-proot or so-called exploaion­ proot electrical outfits, under the impression that such equipments met· all of the reqiirements of the Bureau of Mines as regards safety, There a.re todq in gaseous mines a large nwnber of euipments that have not been approved by the Bureau ot Mines, and unless mod1f'iecl could not receive sucl1 approval.. These e qu.ipments represent in pa.rt the product of manufacturers whil ha.ve never submitted. equipments for insri?ction or tests. and iri pat types developed. previous to the safety work or the bureau. Sometiu.es saleimen advocate the use of unapproved. types in gaseous mines in place of Bureau of Mines approved outfits, the purchase price beini slightly less than approved types,

Sep 1, 1922

By Raymond B. Ladoo

Cne of t·: . .:: i::,portt recent developrr.ents in the feldspar industcy l:.a.s beer. tl:.e r,:ipid. rise of Ne·N H.v-:psr.ire as a. feldspar producing State. Tl:.e unusual size and purity of t: e deposit now 'being worked ne3.r Keene, and tr.a i.nproved metl:.ods ot:' rr.ining srd ir,illing used l:.ave been responsible foe tt.is situation. ti'eldsp'.:l. w'ls occ':tsiona.lly produced sorr.e ye1rs ago in srr.a.ll (tuantities in New Hrunpshi :e, but t::.e State had not been considered a producer of" feldspar ui til lS3l. In the s::ring of tr .. at yea!', t:.e '[eane iic Products co. of Keene, N.H., beg3Il in a srr.9.ll way tl:e production of feldspar fro:n t1eir property in Gilsum, H.H., whicr. l-.a.d long been opera.tei a.s a :tl.ca mine. The purity of the feldspar at enoe '\ttracted f''.lvorai)le attention. and tt.e production of crude ore rapidly in­ cre'.\sed. Early in 1922, a new company, t'he Golding-Keene Co,

Sep 1, 1922

By Byron O. Pickard

With table of bibliography

Sep 1, 1922

By Byron. O. Pickard

"An Arizona mining company recently demonstrated a new use for the geophone by successfully locating leaks in compressed-air lines which were buried under from 1-1/2 to 2-1/2 feet of fine rock fill. The following information is abstracted from data sent to the Bureau of Mines by the superintendent of the mine.The company has two parallel main compressed-air lines, about one and one-half miles long, buried under an average of two feet of fine rock fill. One of the lines is a four-inch high-pressure (1000 pounds) main, and the other line a ten-inch low pressure (90 pounds) main. The two mains are separated by a 10 to 3C foot interval, and run from the compressor plant to the No. 2 shaft, where they are taken underground. A pump line is also buried in the immediate vicinity.Several leaks, not audible enough to be located, were developed in the Alms. Various =Abode were suggested that did not seem practicable to the management. Finally, the company obtained a Bureau of Mines' geophone and experimented with it. The first test& were conducted while the pumps were running, and while there was noise on the concrete pavement, all of Which caused so much vibration in the geophone that it was impossible to detect the leaks.The second attempt was made at the close of the day shift when the compressors were not operating and when the pumps could be shut down. The valves in the far end of the surface lines were closed, and the lines were pumped to full pressure (90 and 1,000 pounds respectively).Geophone readings were then taken at 7 or 8 foot intervals directly see the lines. Several leaks some very large in the high-pressure line were audible with the geophone at distances varying from 15 to 30 feet. A con-le leak in the low-pressure line was found at a distance of 10 feet. detecting the leaks, no difficulty was found in locating them exactly. ""At this time"", laid the superintendent of the mine, are unable to large a leak must be in order to be located under two feet of loose geophone. The fill we worked over was quite loose and dry and unfavorable for the work in question. However, we have no that the instrument is a valuable adjunct to our business""."

Aug 1, 1922

By W. M. Weigel

Langley is about nine miles north of Augusta, Georgia., on the Sou them :l;.ilv1ay. According to the South Carolina. Geological Survey, tr.e district is known a.s tr. Horse Creek and Town Creek sub-areas of the Aileen or Savannah River Area f the South Ciil.Z'olina Coastal Plains. The geology and origin of the clays 3l"e Jscribea in a bulletin of the South Carolina Geological Survey (Series 4, Bull, l; "A Preliminary Report on Cl.:.ws of South Carolina.-), According to this report, i.he clays are sedimentary kaolins, in the Mid.dendor! and Hamburg series of the Cretaceous Age.

Aug 1, 1922

By C. E. Munroe

In order to meet the emergencies of the world wr, tne quantities of explosivea produced in the Unitecl States, and the number of explosives plants were onti:.1.1.:l,lly ncreased so that when the armistice was declared the Government had on hand larg ..mounts oi militazy explosives in excess of existing military needs. Tle stor3.gs of these explosives entailed a liirge expense and their protection neessitatei the employment of m'3.l'lY men who could be better employed otherwise in the military estlish.11ent. Moreover, mar.y ex.ploives, like QJ.l other material, deteriorate on prolonged storage, They lose tht precise definiteness of properties and behavior on which reliance· is placed in military operations, The continued expen3e and d3.nger ttending storage of theae explosives might be diminished by dcst1et1on of the surplus beyond immediate needs, but such·deetniction is danger• ou5 qnd coetly. Hence, the evident solution o! the problem was the salvage d prompt ut111zation of the ru.rplua •

Aug 1, 1922

By A. B. Hooker, L. C. IlsLey

Several ignitions or mine pa, which might have led to explosions, and at least ona mine fire attributed to heated leg wires of electric detonators, have occm.rred. at rn1::.es in which outside shot firing is practiced. Photographs taken at one mine ind.la.ted. that the wires became red hot during firing. These results having been --i·-led. to the .Lttention of the electrical section of the Bureau of the Mines, ignitions the tests and to reportd aid in herein preventing were made future to trouble determine of if this possible kind, the cause of The investigation, which 1• considered preliminary, included tests to determine the conditions tha.t cause gas ignitions from heated. leg wires of electric and. of detonators, copper leg possible wires, remedies The tor samples such of heating, wire used. and in the the relative test were behavior the of reg\llar ironDa. Pont iron and copper leg wires (No, 22 A,W,G.) C\1t from Du. Pont electric detonators.

Aug 1, 1922

By H. A. Doerner

Tellurium is a silver white solid with metallic luster, the e17atal.line torm being ver., brittle aud e.g,s!ly powdered. It has a specific gravity of 6,27, melta at 45a0c. and boils at red het, giving off a. golden 1ellow vapor when air 11 excludei. When heated in air, telluri'UiD burns with a bl\te name tinged with green, and evolves wh1 te vapors ot tellurium dioxide. An amorphous form of tel­lurium, obtained by red.uction and precipi ta.tion from so).ution, haa II specific gr1.vity ot 6,015, and when heated ia cho.nged to the cry:.,talline variety. Telluri,a 11 insoluble in water, c&rbon diaiJ.phido, or h;rd.rochl oric acids, but it 11 41a-1olved bJ nitric or concen t1·ated. sulphi.U·ic acid. It 1..oea not tamiah in moiet ah•• 11 ree11tant to alkaline solutions, e,;:ctpt concentrated KOB, but it 11 cliaaolvecl by tuaed. &lkl 1••. I ts 11.to!!lic weight h..'l.a been the "J.Ubject ot mch controverq, bu\ t.he value 137 .5 :.a bl!ten generally accepted, Tho chflmietr:, of tellurium ia eim1lar to that ot IUlphur. It tonne throo xid.ee TeO, To02, and Te0 , al10 tellur14ea, t•llurite,, and. tellur1.t11, A number of halide compoWld.1, a 3iulph1de, and. a .ulpbat.e are known.

Aug 1, 1922

By Leonard Greenburg

The analytical procedure necessary when using this new impinger•bubbler eil)paratus is almost identical with that em:r;,loyed with the Palm0r a:pp8.ratua. As sugar is not employei, the new apparatus por.;sesses the advantage over the eug.r tube method in having vsry low control errors, being, therefore, much simple in laboratory manipulation during analysis.

Aug 1, 1922

By Clyde E. Eilliams

In recent ye.ars much intere,t has been centered on the possibility of pro­ducing alumina from clq, a.nd proposed methods tor the recove:r,v of alumina are appearing constantly in parent lit,erature, As a good· grade of clay contains from 30 t<> 40 per cent of al"WDina, the prospect of tecovering it is alluring, al though obviously ditfieul t. A patent typical of m projected thermal processes is that 0£ Paul Migu.et, (U, S, Patent No, l,376,563) entitled nprocess for the preparation of pure alkaline alu:ninates.'' Re proposes to prepare alkaline a.luminate by fusing clay, lime, and acrap iron with a reducing aget in the electric furnAce, thereby reducing the silica a.r.d formin1s calcium alumina.te and ferrostlicon, The calcium aluminate, being lighter, would. float on top substantially free from foreign oxides, It could. then be tapped ott, cooledf ana later crushed and leached with aodium carbonate solution to torm, by double decomposition, sodium aluminate, and calcium carbonte. The fonMr is soluble and yields readily aluminum hydroxicie. 'l'he ferrosilicon wo'Uld be r,covered as such and sold at a profit.

Aug 1, 1922

By A. B. Hooker, L. C. IlsLey

In lare-scal e blasting, it is customary to fire me.l'\Y shot.!:l simu1. taneously. The electric !atonators ara usually conneced in seies, ard are fired either from a power circuit or :from a blasting ma.chine with large capacity, operated by hand. "!hen :'::ri111; with a blasting ca.chine, trouble with missed shots has been freqi.,.ently e>:pert0nced.. Unit1:i:' thes ,:::rcu:ns tances, the shots that fail to fire are often a gr"up in the t.:E"nter r,f t>e series, Various explaz,.a.tions hs.ve been given as to the cause of the failurs. Tis paper covers a few tests made cy the electrical section of tl:.e Dti..'t'cau. cf Mines, wh;.r.;h may be helpful in understanding the -probable cuse of tl1e misfiring of c.:anter shots, Wh3tever th9 source ot the firir. current generator, magneto, or batter, the CUl"rent delivered th:·01.1.gh a shot-f:?·ing circu.it is determined by t.ae total resistance of ,;he clrcili +.; c:1nd all cure:it leaving th9 p,si tive terminal must return to tre negative te1-minal. If a. metallic circuit is well i1,.sul.:tted, praeti­ccl. l;1 a.ll of the t.'Urrent keepo within the circu.it; but in a. shot-!11·.irig ci.rc1li t, Nhere the ·.vires f:ll·e often 1n c.c,i.cact with the eru:"!ih as i11 wet holer., end whero the ins".lla.tion of the leg wires :i. inadecpa.te to prc·,ent lea.l.tage, the current ma.v tu.e v a.r ious pa the: thro-.. .. gh the nr r. earth.

Aug 1, 1922

By John R. Reeves

The principal oil aha.le in Indiana ie known as the New Al'baZ\Y shale. It 11 ot Devonian age, and ia usually correlated with, although not certainly of the 1ame age a,, the Antrim shale of northern Michiga.. the Ohio shale of Ohio, and the Chattanooga shale ot Kentucky. Termescae • a."ld Georgia. The nqtmal thickneaa of the formation 1n Indiana 1e a.bout 100 faet, ltbough 1n the region of its out­ cro;l the tall th!::kne,111 io rarely exposed because cf the general d:.p of the strata, which is 11 about 30 feet per mile to the west. With the exception ot thin local pha1e1, the entire thickness is oil shale,

Aug 1, 1922